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  • Alhashimi, Anas, 1978- (författare)
  • Statistical Sensor Calibration Algorithms
  • 2018
  • Doktorsavhandling (övrigt vetenskapligt)abstract
    • The use of sensors is ubiquitous in our IT-based society; smartphones, consumer electronics, wearable devices, healthcare systems, industries, and autonomous cars, to name but a few, rely on quantitative measurements for their operations. Measurements require sensors, but sensor readings are corrupted not only by noise but also, in almost all cases, by deviations resulting from the fact that the characteristics of the sensors typically deviate from their ideal characteristics.This thesis presents a set of methodologies to solve the problem of calibrating sensors with statistical estimation algorithms. The methods generally start with an initial statistical sensor modeling phase in which the main objective is to propose meaningful models that are capable of simultaneously explaining recorded evidence and the physical principle for the operation of the sensor. The proposed calibration methods then typically use training datasets to find point estimates of the parameters of these models and to select their structure (particularlyin terms of the model order) using suitable criteria borrowed from the system identification literature. Subsequently, the proposed methods suggest how to process the newly arriving measurements through opportune filtering algorithms that leverage the previously learned models to improve the accuracy and/or precision of the sensor readings.This thesis thus presents a set of statistical sensor models and their corresponding model learning strategies, and it specifically discusses two cases: the first case is when we have a complete training dataset (where “complete” refers to having some ground-truth informationin the training set); the second case is where the training set should be considered incomplete (i.e., not containing information that should be considered ground truth, which implies requiring other sources of information to be used for the calibration process). In doing so, we consider a set of statistical models consisting of both the case where the variance of the measurement error is fixed (i.e., homoskedastic models) and the case where the variance changes with the measured quantity (i.e., heteroskedastic models). We further analyzethe possibility of learning the models using closed-form expressions (for example, when statistically meaningful, Maximum Likelihood (ML) and Weighted Least Squares (WLS) estimation schemes) and the possibility of using numerical techniques such as Expectation Maximization (EM) or Markov chain Monte Carlo (MCMC) methods (when closed-form solutions are not available or problematic from an implementation perspective). We finally discuss the problem formulation using classical (frequentist) and Bayesian frameworks, and we present several field examples where the proposed calibration techniques are applied on sensors typically used in robotics applications (specifically, triangulation Light Detection and Rangings (Lidars) and Time of Flight (ToF) Lidars).
  • AlHayali, Amani (författare)
  • In vitro-solubility and supersaturation behavior of supersaturating drug delivery systems
  • 2018
  • Doktorsavhandling (övrigt vetenskapligt)abstract
    • The development of new pharmaceutical products has been challenged by the growing number of poorly water-soluble drugs, which often lead to suboptimal bioavailability. Various approaches, such as the use of amor-phous solid dispersions and cocrystals, have been used to improve the solu-bility, and subsequent bioavailability, of these drug molecules. Supersaturat-ing drug delivery systems (SDDSs) have potential for achieving adequate oral drug bioavailability by increasing the drug solubility and creating a su-persaturated state in the gastrointestinal tract. However, there is a need for better understanding of the supersaturation behavior in SDDSs and of the factors affecting supersaturation. The main objective of this thesis was to improve understanding of the supersaturation solubility behavior in SDDSs with a particular focus on rapidly dissolving solid forms (amorphous forms/cocrystals).In the course of the work, a new formulation for ezetimibe using an amorphous solid dispersion was prepared, cocrystals of tadalafil were pre-pared, and oral films of silodosin were formulated for the first time. These new formulations were thoroughly characterized using a number of solid-state and pharmaceutical characterization techniques.The dissolution and supersaturation behavior of the prepared SDDSs were studied. The effects of various factors on the supersaturation and precipita-tion characteristics were investigated. These factors included the preparation method, the temperature of the dissolution medium, the type of dissolution biorelevant medium (gastric/intestinal) used, the permeability of the relevant gastrointestinal membranes, the addition of polymers, and the addition of surfactants. The amorphous solid dispersions, cocrystals and oral films that were prepared represent new drug formulations that provide significantly higher dissolution rates and supersaturated solubility than crystalline drug forms. Solid dispersions prepared by the melting method had better super-saturation properties than those prepared by spray drying. The precipitation kinetics of the solid dispersion were faster at 37 ̊C than at 25 ̊C in bio-relevant media. Implementation of an absorption tool during in vitro evalua-tion of supersaturation levels could improve the prediction accuracy of su-persaturation and precipitation. A better understanding of the effects of ex-cipients on the supersaturation and precipitation behavior of these types of formulation was obtained in this thesis. The improvement in supersaturation solubility obtained by adding polymers and surfactants was not proportional to the amounts of excipient used.This thesis has made notable contributions to the field of pharmaceutical science by advancing our understanding of the supersaturation solubility behavior of the newly prepared SDDSs.
  • Ali, Ammar (författare)
  • Three Dimensional Hydro-Morphological Modeling of Tigris River
  • 2016
  • Doktorsavhandling (övrigt vetenskapligt)abstract
    • The River Tigris is a major river in Iraq. It divides Baghdad, the capital of Iraq, in two parts. The reach of the river within Baghdad is about 60 km long. The climate change within the region and the construction of hydraulic structures upstream of Baghdad has reduced the water discharge of the river by 44%. Despite the fact that huge volumes of sediment have been trapped in the constructed headwater reservoirs, substantial changes have occurred in the topography of the Tigris River within Baghdad City and the number of depositions is increasing. The debris of the destroyed bridges from the wars of 1991 and 2003 and their subsequent reconstruction have contributed to the development of these depositions. As a consequence, the ability of the river to carry the peak flood waters has been reduced. This has led to a potential increase of flooding in parts of the city. To predict the maximum flood capacity for the river, the bathymetric survey that was conducted for 50 km of the Tigris River by the Ministry of Water Resources in 2008 has been used with the one-dimensional flow model “HEC-RAS”. Calibration of the model was carried out using field measurements for water levels along the last 15 km of the reach, and the water level observations at the Sarai Baghdad gauging station for the last 10 years were used to validate the model. The model showed a significant reduction in the river’s capacity compared with what the river had carried during the floods of 1971 and 1988. This result agrees with previous surveys conducted on the same reach indicating that the ability of the river to convey high water has decreased. To overcome this problem, dredging operations started along most of the Tigris River inside Baghdad City to remove many islands and side bars, as well as cleaning water intakes. An examination for the dredging plan currently in progress and two additional proposed plans was conducted using the ‘HEC-RAS’ model for the 50 km long river reach to investigate whether the designed flooding capacity of the river can be recovered and how much it can be improved. Comparing the historical records of water level and discharge for the last three decades, some improvement of flood capacity was achieved. Cautions about the water intakes should be considered to maintain their functionalities with the expected drop in water levels due to dredging operations. Bathymetric and land surveys were conducted for the northern Tigris River reach (18 km length) in Baghdad, producing 180 cross sections. A riverbed topography map was established from these cross sections. Sediment transport rates and bed composition were investigated by collecting three different types of sediment samples at the quartiles of 16 cross sections along this reach. The Helley-Smith sampler was used to collect 288 bedload samples, a suction pump was used to collect 212 suspended load samples from different depths. The Van Veen grab was used to collect 46 bed material samples. The velocity profiles and the water discharges were measured using ADCP at the sampling sections. Bed sediment compositions were investigated by analysing the collected bed material samples. It was noticed that fine sand dominated the riverbed (90.74%). The average median size within the reach was 2.49 phi (0.177mm) whilst the mean size was 2.58 phi (0.16mm). In addition, the sediments were moderately sorted, fine skewed and leptokurtic. The size of the bed sediment relatively decreased compared to older investigations due to the decrease of the competence of the river. The bed elevation had increased compared to previous surveys. It was noticed that dredging operations and obstacles (e.g. fallen bridges and islands) disturbed the flow of the river and the sediment characteristics in several sites. Bedload rates were computed using the weights of the collected bedload samples. The spatial distribution of sampling cross sections took into consideration the variance of river topography where 7 meanders, 2 islands and several bank depositions characterize the geometry of the river reach. Twenty bedload predictors were applied to the same reach. The annual transported quantities of the bedload were estimated to be 36 and 50 thousand tons in 2009 and 2013 respectively. The total load discharge rate in the northern reach of the Tigris River was computed using the sediment concentrations of the collected suspended load samples after adding the bedload rate at each of the sampling cross sections. The results indicated that the suspended load is the dominant mode in the total load with a minimum percentage of 93.5%. The total load ranged from 29.1 to 190.3 kg/s. A total load rating curve of the power function was established. The associated errors from using the proposed rating curve are within reassuring levels and less than the errors produced from most of the other twenty-two total load formulas, which were applied to the same reach. The scattering of the results from the other formulas can be attributed to the spatial variance in the topography of the riverbed. According to the final results obtained, it is recommended to use the proposed procedure for establishing a spatial total load rating curve to estimate sediment rates for morphologically complicated rivers. The annual transported quantities of the total load were estimated at 2.47 and 4.23 million tons for 2009 and 2013 respectively. The three-dimensional morphodynamic model (Simulation of Sediment movements In water Intakes with Multiblock option - SSIIM) was used to simulate the velocity field and the water surface profile along the northern reach of the Tigris River using the findings of the current bathymetric survey of the river. The model was calibrated for the water levels, the velocity profiles and the sediment concentration profiles using different combinations of parameters and algorithms, those available in the model. The set of parameters that gave a minimum root mean square error (RMSE) was used for the validation process using another set of field measurements. The calibration and the validation results showed good agreement with field measurements, and the model was used to predict the future changes in river hydro-morphology for a period of 14 months. The results of the future predictions showed increases in depositions on the shallow part of the cross section having lower velocity and, on the other hand, the river deepens the incised route to fit its current hydrologic condition leaving the former wide section as a floodplain for the newer river. The net deposition/erosion rate was 67.44 kg/s in average and the total deposition quantity was 2.12 million tons annually. The locations of depositions are compatible with those of the river in the real world. An expansion in the size of current islands was predicted. An indication of the potential threats of the river banks’ collapse and the bridge piers’ instability was given by high erosion along the thalweg line.Keywords: Flood capacity, Dredging, HEC-RAS, Bathymetric survey, Bed sediment, Bedload, Total load, Helley-Smith sampler, Sediment transport, ADCP, Prediction formulas, 3-D morphodynamic model, Bed changes, SSIIM, underfit river, regulated river, Tigris River, Baghdad.
  • Allali, Naoual (författare)
  • Covalent functionalization of carbon nanomaterials for bioelectrochemical applications
  • 2019
  • Doktorsavhandling (övrigt vetenskapligt)abstract
    • Carbon nanotubes (CTNs) are renowned for their exceptional electronic and mechanical properties. Their structure can be considered as rolling up a graphene sheet along a specific crystallographic direction, leading to a 1D confinement of the electronic wavefunction of the delocalized electrons along the perimeter of the cylindrical structure thus obtained. This confinement produces the existence of defined spikes of high intensity in the electronic density of states, called van Hove singularities. These singularities are primordial to understand both the optical and electronic properties of CNTs through electronphonon coupling processes. If the electronic density of states (DoS) is non zero at the Fermi level the nanotube is metallic, otherwise the nanotube is semiconducting. The synthesis of CNTs always produces a mixture of both metallic and semiconducting nanotubes, and this material can be useful to be incorporated at the surface of electrodes for electrochemical devices. The high specific surface area, the high mechanical and thermal stability of CNTs and the low percolation threshold for electron transport in a mat of CNTs render them very attractive for such kind of applications. There is yet a drawback of using raw CNTs: they are not compatible with solvents and modification of their surfaces by chemistry is required to make good suspensions for easy deposition at the electrode surface and to introduce specific functional groups for promoting electron transfer, called electron shuttles.The final aim of this thesis is therefore the covalent functionalization of CNTs by electron shuttles and their incorporation at the surface of glassy carbon electrodes for electrochemical devices application. A strategy of chemical grafting in three steps has been chosen: i) a controlled oxidation step in acidic media assisted by microwave irradiation in order to keep the structural integrity of CNTs, so as to save their useful electronic properties; ii) a chloration step to produce acid chloride groups and iii) reaction of these groups with electron shuttles modified by specific linkers. The study was first conducted on very clean HiPCO single-walled CNTs (SWCNTs). This enabled to avoid any disturbing effects of carbonaceous impurities or residual catalytic particles, since their possible effects are extremely controversial in the literature. Once validated, this approach was then conducted with cheaper material including few-walls carbon nanotubes (FWCNTs). The use of FWCNTs compared to SWCNTs was not only beneficial for the production of costeffective electrochemical devices but also for a better durability ofthe final device, the inner nanotubes being not functionalized.The challenge was to obtain a functionalization process with enough grafted electron shuttles to obtain a good electrocatalytic activity but maintaining CNTs integrity. The first step is predominant to reach this goal, and requires a very accurate understanding of the nature and the number of defects created in the CNTs structure versus the physico-chemical conditions used. The introduction of defects in the crystallographic structure of CNTs has strong consequences both for the electronic DoS and for the phononic properties of the material. Spectroscopic methods are essential in probing these consequences. UV-visible-near IR absorption spectroscopy is the method of choice to directly probe the existence of van Hove singularities and the oscillator strength associated with the authorized electronic transitions between theses ingularities. Covalent grafting of chemical groups at the surface of CNTs changes both the energy and the intensity of these transitions. However, this spectroscopic method requires solubilizing CNTs in non-absorbing solvents using adequate surfactants. Interactions between surfactant molecules and CNT sidewalls may also alter the position and intensity of electronic transitions between van Hove singularities unrelated to the chemical groups covalently grafted.Raman spectroscopy of CNTs involves the electronphonon coupling processes through the resonant electronic enhancement of Raman modes. Double resonance processes are also observed in Raman spectrum of CNTs, for instance with the D-band mode that is actually related to the existence of defects in the graphene structure of CNTs. Therefore, Raman spectroscopy is a widespread analytical method to characterize the structural defects created by covalent functionalization processes. Indeed, the intensity ratio of the D and G bands in the Raman spectrum is correlated to the number of defects. However, CNTs are used as bundles when chemical functionalization is performed, which produces a heterogeneous distribution of chemical species grafted on CNTs. Therefore, we have developed a new protocol to obtain statistically significant data for most of the samples made in this thesis. Nevertheless, this statistical approach is still limited for samples slightly functionalized, whence the idea to use spectroscopic ellipsometry as an alternative method to characterize these samples.More specifically, ellipsometric data were collected from UV to the IR part of the electromagnetic spectrum for CNTs functionalized in different conditions. The complex dielectric function was retrieved from the experimental data. A Drude model was used to model the infrared part of the data for raw and acid oxidized CNTs. The optical conductivity of the samples was obtained. These results, combined with other information collected using a set of complementary analytical techniques (Raman scattering, UV-visible-NIR absorption, X-ray photoelectron spectroscopy, thermogravimetric analysis coupled to mass spectrometry, transmission electron microscopy and rare gas volumetric adsorption), show that the microwave-assisted oxidation process actually consists in removing amorphous carbon deposits away from the surface of CNTs and transforming the already existing defects in the CNT structure to oxygen-containing groups such as carboxylic acids.Rare gas volumetric adsorption was also used to compare the distribution of chemical groups at the surface of CNT bundles when two different acids are used (HNO3 and H2SO4). The chloration step was also studied by these methods, as well as the final grafting of electron shuttles. Finally, these functionalized CNTs were deposited at the surface of glassy carbon electrodes and used as electron mediators for diaphorase-catalysed oxidation of nicotinamide adenine dinucleotide (NADH). This was a good example of mediated electron transfer for development of electrochemical devices based on NADH recycling and it validated the good electrocatalytic properties of functionalized CNTs for making electrochemical sensors and actuators, opening new perspectives with potential market applications.
  • Allan, Jon, 1972- (författare)
  • Evaluation of Live Loudness Meters
  • 2019
  • Doktorsavhandling (övrigt vetenskapligt)abstract
    • Discrepancies in loudness (i.e. sensation of audio intensity) has been of great concern within the broadcast community. For television broadcast, disparities in audio levels have been rated the number one cause to annoyance by the audience. Another problem area within the broadcast and music industry is the loudness war. The phenomenon is about the strive to produce audio content to be at least as loud or louder to any other audio content that it can easily be compared with. This mindset, when deciding for audio level treatment, inevitably leads to an increase in loudness over time, and also, as a technical consequence, a decrease of utilized dynamics. The effects of the loudness war is present in both terrestrial radio transmissions as well as in music production and in music distribution platforms.The two problems, discrepancies in loudness and the loudness war, both emanate from the same source; regulations of audio levels and the design of measurement gear have not been amended to cope with modern production techniques. At the time when the work on this thesis started, the ruling technical recommendations for audio level alignment were based on peak measurement. This measured entity has poor correspondence to loudness. To counter the above described problems, the European Broadcasting Union (EBU) and the International Telecommunication Union (ITU) has developed new recommendations for audio alignment, EBU R 128 and ITU-R BS.1770. The new definitions for loudness measurement constitutes simplified models on the human perception of audio intensity. When using the new recommendations in production, the problems have been shown to diminish.For an engineer in a live broadcast scenario, measurement equipment also need to be updated in real-time to illustrate a time-variant loudness of the signal. EBU and ITU also has regulated how this type of measurement gear should behave. EBU Tech 3341 and ITU-R BS.1771 define properties for live loudness meters. These recommendations has since the time of publication been implemented in measurement equipment from manufacturers and become available in production facilities.This thesis investigates the conceptions that have led up to the present recommendations for live loudness meters. It maps out the (at the time) present ways to evaluate the same. Emanating from this knowledge, a new methodology to evaluate loudness meters is proposed that combines qualities from former methods to achieve an alternative balance between ecological validity and control in the experiment design. The methodology includes a procedure to capture data from engineers’ actions and the resulting audio levels from simulated broadcast scenarios. The methodology also incorporates a way to process this type of data into different parameters to be more accessible for interpretation. It presents an approach to model the data, by the use of linear mixed models, to describe different effects in the parameters as the result of the meters’ characteristics. In addition, a review on publications that examine the engineers’ own requests for beneficial qualities in a loudness meter has been condensed and revised into a set of meter criteria that specifically is designed to be applied on the outcome of the mixed models. The outcome of the complete evaluation yields statements on meter quality that are different and complementary to formerly proposed methods for meter evaluation.The methodology has been applied in two different studies, which also are accounted for in the thesis. The conclusions from these studies has led to an increased understanding of how to design live loudness meters to be satisfactory tools to the engineer. Examples of findings are: the effect of the speed of the meter, as being controlled by one or several time constants, on the readability of the meter and the dispersion in output levels – some tested candidates, with higher speed than the present recommended ones, has been shown to be adequate as tools; the three-second integration time has been shown to generate a smaller dispersion in output levels than the 400 ms integration time; the effect of the gate in BS.1771 on the resulting output levels– the gate generally leading to an increase in output levels. The acquired knowledge may be used to improve the present recommendations for audio level alignment, from EBU and ITU.
  • Alvarez, Manuel, 1980- (författare)
  • Distribution Network Planning Considering Capacity Mechanisms and Flexibility
  • 2019
  • Doktorsavhandling (övrigt vetenskapligt)abstract
    • The increasing penetration of distributed energy resources (DERs) has posed challenges to the distribution system operator (DSO) from the operation and regulatory point of view. High penetration of DERs could have negative impacts on the performance of the distribution grid, and depending on the regulatory framework, the DSO's remuneration as well. In liberalized electrical systems, the focus on promoting eciency has led to the implementation of an incentive-based regulation that exerts additional pressure on the DSOs to reduce costs. Additionally, the European Parliament Directive 2009/72/EC establishes a regulatory unbundling among the distribution, production, and retailing activities within the same vertically integrated electric utility.A way of helping the DSO to cope with the posed challenges is by providing it with exibility. This exibility can be acquired from the planning stage, and later be used during the system operation. This exibility can stem from the DSO's ability to exert control on the demand and the supply side to balance the system and correct its operational state.Based on the European DSOs' current situation at facing the increasing penetration of DERs, this thesis investigates in non-wired exible grid tools to solve the distribution network expansion problem. The investigation focuses on exibility providers, in particular on energy storage systems and hydropower, and also on capacity mechanisms to translate the capacity from DERs into the grid's capacity for planning purposes.Given that the share of renewable sources among the DERs is increasing, and considering the importance of energy storage systems in providing exibility to balance renewable energy production, the eort has been turned on to developing a hydropower model and a generic storage model that t both planning and operational studies.Given the need for gearing the DERs' behavior into the DSO's decision making process during the planning and operational timescales, the design and implementation of a distribution capacity mechanism have been developed. The design of the capacity mechanism has been conceived considering its integration within the distribution network expansion problem.The outcomes of this thesis can be synthesized as follows: 1) A generic hydraulic/storage model provided with an equivalent marginal cost that aids in considering the impact of present decisions in the future costs. 2) A market oriented distribution capacity mechanism that gears DERs and the DSOs to benefit mutually. 3) A distribution network expansion planning formulation that integrates the capacity resource from DERs through the distribution capacity mechanism.
  • Amiri, Kaveh (författare)
  • Experimental investigation of a Kaplan runner under steady-state and transient operations
  • 2016
  • Doktorsavhandling (övrigt vetenskapligt)abstract
    • Hydropower is a key part in electricity production nowadays. Hydropower electricity production rose to 3579.5 TWh in 2013, ranked as the second source of electricity production in the world after fossil fuels. It is the principle source of renewable electricity production, producing 16.2% of the electricity in 2013, accounting for 78% of the renewable electricity production in the world. Specifically in Sweden, hydropower is the main source of electricity production producing 47.5% of the required electricity. Nuclear, biomass, and wind placed in the following positions in the ranking in 2013 with 38.4%, 6.5%, and 4.3%, respectively.Besides meeting electricity demand with an environmental-friendly method, hydropower has a unique and important role which is grid regulation: balancing electricity production and consumption. Gas turbines and hydraulic turbines called “Primary reserves” are the only electricity production systems that can be used for fast regulations due to their short start-up time from 1 to 60 s. The obvious environmental problems, air pollution, and costs associated with gas turbines make hydropower a prime alternative whenever applicable. In Sweden, the share of fossil fuels in electricity production is small; 2.8% in 2012 with an average annual growth of -0.7% in the period 2002-2012. Hence, hydropower is practically the only available source used to regulate the grid fluctuations resulting from deregulated market and fast growth of intermittent power generation systems, i.e., solar and wind energy. Hydraulic turbines are subject to frequent off-design and transient operations because of their grid regulation responsibility. Such operating conditions decrease turbine’s efficiency and affect its lifetime significantly. Off-design and transient operation of hydraulic turbines may induce unpredicted pressure fluctuations on the stationary and rotating parts of the turbine. Special attention should be dedicated to the effects of such phenomena on the runner blades because of their importance on the efficiency of the turbine, and their vulnerability to the pressure fluctuations.This thesis presents an experimental investigation on the effects of off-design and transient operation of an axial hydraulic turbine on velocity fields and pressure fluctuations exerted on the runner and the draft tube of a turbine. The investigation was performed on a 1:3.1 scaled model of a Kaplan turbine known as Porjus U9. The main objective was to investigate the effect of operating point on pressure and velocity fluctuations in the runner and the draft tube. Another objective was to study the effect of transient operation on pressure fluctuations exerted on the runner and the draft tube, to investigate the formation and mitigation process of a rotating vortex rope (RVR) within the draft tube. Finally, the effect of the swirl leaving the runner and the draft tube bend on the performance of the turbine was investigated. The study involves pressure measurements on the runner blades and draft tube walls of the turbine, laser Doppler anemometry (LDA) measurements within and after the runner, and particle image velocimetry (PIV) measurements within the draft tube.The pressure and LDA results acquired during steady state operation of the turbine showed different sources of fluctuations on the runner at different operating points resulting in symmetric and asymmetric fluctuating forces on the runner. The pressure measurements during transient operating conditions exhibited pressure fluctuations exerted on the runner during load variations and elucidated some aspects of formation and mitigation process of RVR within the draft tube. The PIV measurements performed after the draft tube bend of the turbine focuses on the physical phenomena resulting in flow asymmetry after the draft tube bend of hydraulic turbines affecting their efficiency.
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