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- Couceiro, José, 1983-
(författare)
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X-ray computed tomography to study moisture distribution in wood
- 2019
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- X-ray computed tomography (CT) has been used as an analysing tool for different features in wood research since the beginning of the1980s, but it can also be used to study wood-water interactions in different ways, such as by determining wood moisture content (MC). The determination of wood MC with CT requires two CT images: one at the unknown moisture distribution and a second one at a known reference MC level, usually at oven-dry condition. The two scans are then compared, and the MC is calculated based on the differences between the images. If the goal is to determine the MC in local regions within the wood volume, e.g. when studying moisture gradients in wood drying, wood shrinkage must be taken into account during the data processing of the images. The anisotropy of wood shrinkage creates an obstacle, however, since the shrinkage is not uniform throughout the wood specimen. The technique is thus limited in two ways: it cannot measure MC in local regions and it cannot do it in real time.The objective of this thesis was to study methods to overcome these two limitations. The work explores up to three different methods to estimate local MC from CT images in real time. The first method determines shrinkage for each pixel using digital image correlation (DIC) and is embedded in a broader method to estimate the MC, which verified against a reference. It involves several steps in different pieces of software, making it time-consuming and creating many sources of possible experimental errors. The determination of shrinkage within this method is further explored to enable the implementation of all steps in a unique piece of software. It is shown that it is possible to calculate MC through this method with a root mean square error of prediction of 1.4 percentage points for MC between 6 and 25%.The second method studied succeeds in determining the MC distribution in research applied to wood drying, but the calculation of shrinkage differs from the previous method: instead of calculating shrinkage in the radial and tangential directions, it does so by using the displacement information generated from the spatial alignment of the CT images. Results show that the algorithm can provide consistent data of internal MC distribution of wood at the pixel level that entail continuing researching wood drying processes with an improvement in the accuracy of the MC determination. It represents an improvement regarding the first method because the calculation is fast and highly automatized in a single piece of software.The third method studied is the application of dual energy CT (DECT) to moisture. DECT would provide means for MC calculation at the pixel level and, potentially, in real time, which would mean an important breakthrough in wood drying research. Previous research shows promising results, but its implementation in medical CT, the tool used throughout this work, has shown poor predicting ability. Nevertheless, further research is encouraged.The work done in this thesis proves that it is possible to measure local distribution of MC in wood using CT with accuracy and precision. It also shows that further research could potentially provide a means for MC estimation in real time.
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| 2. |
- Neyses, Benedikt, 1986-
(författare)
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Surface Densification of Solid Wood : Paving the Way Towards Industrial Implementation
- 2019
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Surface densification of a piece of solid wood results in an increase in density and in hardness in the whole or a part of the densified material, and is one of the ways of improving the properties and value of low-density wood species. Despite efforts for many years, mass commercialisation of either bulk- or surface-densified wood products has not yet been achieved. Most of the previously tested densification methods have limitations in terms of processing speed and integration into the largely continuous wood processing chain, which leads to high production costs. Established methods to eliminate the set-recovery rely either on technologically complex close-system methods or on open-system methods that require relatively long periods of high energy input. For this reason, impregnation with adhesives is used in almost all commercially available densified wood products, and none of them have risen above their status of being niche products.Based on this background, three objectives for this project were formulated: (1) the development of a method for selecting the most suitable wood species for surface densification, (2) showing that surface densification can be carried out in a continuous manner at high process speeds, (3) and researching a fast open-system method to reduce the set- recovery.The method developed for selecting the most suitable wood species for surface densification was based on Lean principles, and it confirmed the suitability of previously studied wood species, such as Scots pine, spruce and poplar. In addition, several suitable alternatives from different parts of the world and from different types of forest were identified. This suggests a high potential for establishing such wood products on a global market level.Two studies using a continuous roller press showed that solid wood can be successfully surface-densified at process speeds of up to 80 m min-1, and that some defects, such as knots, are acceptable in the raw material, but the problem of set-recovery could not however be solved.A screening experiment testing different open-system approaches to reduce the set-recovery highlighted the potential of a novel method using ionic liquids as a plasticiser prior to the surface densification of solid Scots pine. The set-recovery could be reduced to 10%, with the time of high energy input being less than 10 minutes. The Brinell hardness was increased by a factor of 2.7 over that of undensified wood. A study with thermo-gravimetric analysis and digital image correlation showed that the set-recovery almost exclusively happens in the transition zone between the densified and undensified wood cells, where there is less penetration of the ionic liquids.The work accomplished in this project has successfully addressed several gaps in the field of wood densification, firstly, by employing a continuous surface densification process using a roller press, and secondly, by developing and studying a fast open-system pre-treatment with ionic liquids, which greatly reduces the set-recovery. Research will continue on a new band press, facilitating a swift transfer of knowledge between small- scale studies and the continuous surface densification of production-size wooden boards.
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