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Optimisation and va...
Optimisation and validation of an automated solid phase extraction technique coupled on-line to enzyme-based biosensor detection for the determination of phenolic compounds in surface water samples
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- Burestedt, E. (author)
- Department of Analytical Chemistry, University of Lund, Lund, Sweden
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- Emnéus, J. (author)
- Department of Analytical Chemistry, University of Lund, Lund, Sweden
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- Gorton, L. (author)
- Department of Analytical Chemistry, University of Lund, Lund, Sweden
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- Marko-Varga, G. (author)
- Department of Analytical Chemistry, University of Lund, Lund, Sweden
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- Domínguez, E. (author)
- Department of Analytical Chemistry, Faculty of Pharmacy, University of Alcalá de Henares, Alcalá de Henares, Spain
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- Ortega, F. (author)
- Department of Analytical Chemistry, Faculty of Pharmacy, University of Alcalá de Henares, Alcalá de Henares, Spain
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- Narváez, A. (author)
- Department of Analytical Chemistry, Faculty of Pharmacy, University of Alcalá de Henares, Alcalá de Henares, Spain
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- Irth, H. (author)
- Division of Analytical Chemistry, Leiden/Amsterdam Center for Drug Research, Leiden, The Netherlands
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- Lutz, Mareike, 1967- (author)
- Division of Analytical Chemistry, Leiden/Amsterdam Center for Drug Research, Leiden, The Netherlands
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- Puig, D. (author)
- Department of Environmental Chemistry, CID-CSIC, Barcelona, Spain
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- Barceló, D. (author)
- Department of Environmental Chemistry, CID-CSIC, Barcelona, Spain
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(creator_code:org_t)
- Heidelberg : Springer Berlin/Heidelberg, 1995
- 1995
- English.
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In: Chromatographia. - Heidelberg : Springer Berlin/Heidelberg. - 0009-5893 .- 1612-1112. ; 41:3-4, s. 207-215
- Related links:
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Subject headings
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- A fully integrated screening system for phenolic compounds was developed incorporating on-line solid phase extraction, fractionation and biosensor detection. Two different types of biosensors, solid graphite and carbon paste electrodes incorporating the enzyme tyrosinase, were compared and used in the screening system. Interfacing of the solid phase extraction and fractionation with the biosensor detection was given special attention since the biosensors were not compatible with the organic modifier used for desorption of phenols from the solid phase extraction step. The system was validated with conventional analytical techniques. Surface water samples from the Ebro river were spiked with 1,10, and 25μg L−1 of catechol, phenol,p-cresol, respectively. Three out of seven samples were spiked and the correct samples were identified, containing phenols equivalent to the spiked concentrations. © 1995 Friedr. Vieweg & Sohn Verlagsgesellschaft mbH.
Subject headings
- NATURVETENSKAP -- Kemi -- Analytisk kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences -- Analytical Chemistry (hsv//eng)
Keyword
- Column liquid chromatography
- Solid phase extraction
- Enzyme-based biosensor detection
- Tyrosinase
- Phenols
Publication and Content Type
- ref (subject category)
- art (subject category)
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- By the author/editor
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Burestedt, E.
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Emnéus, J.
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Gorton, L.
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Marko-Varga, G.
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Domínguez, E.
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Ortega, F.
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show more...
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Narváez, A.
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Irth, H.
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Lutz, Mareike, 1 ...
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Puig, D.
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Barceló, D.
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show less...
- About the subject
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- NATURAL SCIENCES
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NATURAL SCIENCES
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and Chemical Science ...
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and Analytical Chemi ...
- Articles in the publication
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Chromatographia
- By the university
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Halmstad University