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Effect of low-temperature degradation on the mechanical and microstructural properties of tooth-colored 3Y-TZP ceramics

Nakamura, Keisuke (författare)
Gothenburg University,Göteborgs universitet,Institutionen för odontologi,Institute of Odontology,University of Gothenburg, Sweden; Tohoku University, Japan
Harada, A. (författare)
Tohoku University, Japan
Ono, M. (författare)
Japan Fine Ceramics Co. Ltd, Japan
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Shibasaki, H. (författare)
Japan Fine Ceramics Co. Ltd, Japan
Kanno, T. (författare)
Tohoku University, Japan
Niwano, Y. (författare)
Tohoku University, Japan
Adolfsson, Erik (författare)
RISE,IVF
Milleding, Percy, 1942 (författare)
Gothenburg University,Göteborgs universitet,Institutionen för odontologi,Institute of Odontology,University of Gothenburg, Sweden
Örtengren, Ulf, 1959 (författare)
Gothenburg University,Göteborgs universitet,Institutionen för odontologi,Institute of Odontology,University of Gothenburg, Sweden; UiT The Arctic University of Norway, Norway
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 (creator_code:org_t)
Elsevier BV, 2016
2016
Engelska.
Ingår i: Journal of The Mechanical Behavior of Biomedical Materials. - : Elsevier BV. - 1751-6161 .- 1878-0180. ; 53, s. 301-311
  • Tidskriftsartikel (refereegranskat)
Abstract Ämnesord
Stäng  
  • The aim of the present study was to evaluate the effects of low-temperature degradation (LTD) induced by autoclaving on the mechanical and microstructural properties of tooth-colored 3mol% yttria-stabilized tetragonal zirconia polycrystals (3Y-TZP). In total, 162 disc-shaped 3Y-TZP specimens were prepared. Two-thirds of the specimens were shaded by either the infiltration or powder mixing methods while the remaining specimens were used without coloring. The specimens were autoclaved at 134°C for 0, 10, and 100h to induce LTD (n=18 for each group). Chemical compositions were analyzed with X-ray fluorescence spectroscopy. Biaxial flexural strength was measured using a piston-on-three-ball test. The surface fraction and penetration depth of the monoclinic phase were examined using X-ray diffraction and scanning electron microscopy, respectively. The tooth-colored 3Y-TZP specimens contained Fe2O3 and Er2O3 (infiltration technique), and Fe2O3 (powder mixing method) at concentrations of<0.5wt%. The tooth-colored 3Y-TZP had higher strength than the non-colored material after 100h of autoclaving. In terms of surface fraction and penetration depth, the generation of monoclinic phase was significantly lower in the tooth-colored 3Y-TZP than in the non-colored material. The tooth-colored 3Y-TZP possessed equivalent biaxial flexural strength to that of the non-colored material and higher resistance to LTD regardless of the coloring technique (infiltration technique or powder mixing method) when the coloring pigments were contained at concentrations used in the present study. © 2015 Elsevier Ltd.

Ämnesord

MEDICIN OCH HÄLSOVETENSKAP  -- Klinisk medicin -- Odontologi (hsv//swe)
MEDICAL AND HEALTH SCIENCES  -- Clinical Medicine -- Dentistry (hsv//eng)
TEKNIK OCH TEKNOLOGIER  -- Materialteknik (hsv//swe)
ENGINEERING AND TECHNOLOGY  -- Materials Engineering (hsv//eng)

Nyckelord

Coloring
Low-temperature degradation
Phase transformation
Weibull analysis
Zirconia
Bending strength
Chemical analysis
Fluorescence spectroscopy
Mixing
Phase transitions
Scanning electron microscopy
Strength of materials
Temperature
X ray diffraction
Yttria stabilized zirconia
3mol% yttria-stabilized tetragonal zirconia polycrystal (3Y-TZP)
Bi-axial flexural strength
Infiltration techniques
Low-temperature degradations
Micro-structural properties
Powder mixing methods
X ray fluorescence spectroscopy
Yttrium alloys
erbium
ferric oxide
yttrium
zirconium oxide
Article
autoclave
ceramics
chemical composition
chemical structure
color
degradation
low temperature
priority journal
X ray fluorescence
Coloring

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