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Effects of decompos...
Effects of decomposition route and microstructure on h-AlN formation rate in TiCrAlN alloys
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- Chen, Yu-Hsiang (författare)
- Linköpings universitet,Nanostrukturerade material,Tekniska fakulteten
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- Rongström, L. (författare)
- Linköpings universitet,Nanostrukturerade material,Tekniska fakulteten
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- Ostach, D. (författare)
- HZG, Germany
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- Ghafoor, Naureen (författare)
- Linköpings universitet,Nanostrukturerade material,Tekniska fakulteten
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- Johansson-Jöesaar, Mats P (författare)
- Linköpings universitet,Nanostrukturerade material,Tekniska fakulteten,SECO Tools AB, Sweden
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- Schell, N. (författare)
- HZG, Germany
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- Birch, Jens (författare)
- Linköpings universitet,Tunnfilmsfysik,Tekniska fakulteten
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- Odén, Magnus (författare)
- Linköpings universitet,Nanostrukturerade material,Tekniska fakulteten
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(creator_code:org_t)
- ELSEVIER SCIENCE SA, 2017
- 2017
- Engelska.
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Ingår i: Journal of Alloys and Compounds. - : ELSEVIER SCIENCE SA. - 0925-8388 .- 1873-4669. ; 691, s. 1024-1032
- Relaterad länk:
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https://liu.diva-por... (primary) (Raw object)
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http://liu.diva-port...
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Ämnesord
Stäng
- The phase evolution of cubic (c), solid solution TixCr-0.37Al1-0.37-x N alloys with x = 0.03 and 0.16, and the kinetics of the hexagonal (h)-AlN formation are studied via in situ wide angle x-ray scattering experiments during high temperature (1000-1150 degrees C) annealing. Spinodal decomposition was observed in Ti0.16Cr0.36Al0.48N while Ti0.03Cr0.38Al0.59N decomposes through nucleation and growth of h-AlN, c-TiN and c-CrAlN. h-AlN is formed from c-CrAlN domains in both cases and the formation rate of h-AlN depends on the stability of the c-CrAlN domains. In Ti0.16Cr0.36Al0.48N, the c-CrAlN domains are stabilized by crystallographic coherency with the surrounding c-TiCrN in a microstructure originating from spinodal decomposition. This results in lower formation rates of h-AlN for this composition. These differences are reflected in higher activation energy for h-AlN formation in Ti0.16Cr0.36Al0.48N compared to Ti0.03Cr0.38Al0.59N. It also points out different stabilities of the intermediate phase c-CrAlN during phase decomposition of TiCrAlN alloys. Additional contributions to the low activation energy for formation of h-AlN in Ti0.03Cr0.38Al0.59N stems from precipitation at grain boundaries. (C) 2016 Elsevier B.V. All rights reserved.
Ämnesord
- TEKNIK OCH TEKNOLOGIER -- Materialteknik -- Metallurgi och metalliska material (hsv//swe)
- ENGINEERING AND TECHNOLOGY -- Materials Engineering -- Metallurgy and Metallic Materials (hsv//eng)
Nyckelord
- Coating materials; Phase transitions; Kinetics; Synchrotron radiation
Publikations- och innehållstyp
- ref (ämneskategori)
- art (ämneskategori)
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