The first example of sequence-specific non-uniformly C-13(5) labelled RNA: Synthesis of the 29mer HIV-1 TAR RNA with C-13 relaxation window

• A complete synthetic protocol as well as H-1- and C-13-NMR data on the monomer building blocks used for the solid-phase synthesis of specifically C-13-labelled (99 atom % C-13) stem ((27)A and (43)G), bulge (C-24) and loop (U-31) regions of 29mer HIV-1 TA

Nyckelord

SELECTIVELY C-13-ENRICHED DNA; NUCLEAR-MAGNETIC-RESONANCE; RELAYED HMQC EXPERIMENTS; TIN DEUTERIDE REDUCTION; ACID RELATED-COMPOUNDS; SOLID-PHASE SYNTHESIS; ENZYMATIC-SYNTHESIS; CHEMICAL SYNTHESIS; NMR-SPECTROSCOPY; STEREOSELECTIVE SYNTHESIS

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