| 1. |
- Varna, Janis, et al.
(författare)
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Damage and Failure Analysis for Composites
- 2022. - 2
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Ingår i: Comprehensive Structural Integrity. - : Elsevier. - 9780323919456 ; , s. 225-246
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Bokkapitel (övrigt vetenskapligt/konstnärligt)abstract
- Intralaminar cracking in plies of composite laminates is the first microdamage mode that affects thermo-elastic properties and may trigger local delaminations and final failure of the composite. Intralaminar cracks are like tunnels running along the fiber direction in the ply. The number of cracks increases with the increase of the applied load or with the number of cycles in fatigue loading. In this article, the cracking evolution is analyzed distinguishing two phases in development: initiation and propagation. For laminates with thick plies, the initiation ends with triggering sudden propagation and, therefore, concept of statistical initiation stress distribution in the ply together with Monte Carlo method is used for analysis. For thin-ply laminates, crack initiation does not lead to immediate propagation and the energy release concept is used to analyze crack propagation.
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| 2. |
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| 3. |
- Al-Maqdasi, Zainab, 1986-
(författare)
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Development of Constituents for Multi-functional Composites Reinforced with Cellulosic Fibers
- 2019
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Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Bio-basedcomposites are being increasingly used in applications where weight saving,and environmental friendliness is as important as structural performance. Obviously, bio-based materials have their limitations regarding durability and stability of the properties,but their potential in use for advanced applications can be expanded if they were functionalized and considered beyond their structural performance.Multifunctionalityincomposites can be achieved by modifyingeither of the composite constituents at different levelsso that they can perform energy-associated roles besides their structural reinforcement in the system. For the fibers, this can be done at the microscale by altering theirmicrostructure during spinning process or by applying functional coatings. As for the matrix, it is usually done by incorporating additives that can impart the required characteristics to the matrix. The nano-sized additives that mightbe considered for this objective are graphene and carbon nano-tubes. A big challenge with such materials is the difficulty to reachthe dispersionstate necessary for formation ofstable network to overcome the percolation threshold for conductivity. However, once the network is formed, the composite can have improved mechanical performance together with one or more of the added functionalities such as barrier capabilities,thermal and/or electrical conductivities or electromagnetic interference ability.Enormous work has been done to achieve the functionality incomposites produced with special care in laboratories. However, when it comes to mass production, it is both cost and energy inefficient to use tedious,complex methods for the manufacturing. Hence there is a need to investigate the potential of using scalable and industrial-relevant techniques and materials with acceptable compromise between cost and properties.The work presented in this thesis is performedwithin two projects aiming to achieve functional composites based on natural and man-made cellulosic fibers suitable for industrial upscaling. Conductive Regenerated Cellulose Fibers (RCFs) were produced by coating them with copper by electroless coating process using commercial materials. On the other hand, commercial masterbatches based on Graphene Nano-Platelets (GNPs) were used to produce wood polymer composites (WPC) with added multifunctionality by melt extrusion process. The process is one of the conventional methods used inpolymerproductionand needsno modifications for processingfunctional composites. Both materials together can be used to produce hybrid functional composites.The incorporation of the GNP into HDPE has resulted in improvement in the mechanical propertiesof polymer as well as composite reinforced with wood fibers. Stiffness has increased to a large extent while effect on the strength was less pronounced(>100% and 18% for stiffness and strength at 15%GNP loading). The enhancement of thermal conductivityat higher graphene loadingswas also observed. Moreover, time-dependent response of the polymer has also been affected and the addition of GNP has resulted in reduced viscoplastic strains and improved creep behavior.The copper-coated cellulose fibers showed a significant increasein electrical conductivity(<1Ω/50mm of coated samples) and a potential in use as sensor materials. However, these results come with the cost of reduction in mechanical properties of fibers (10% and 70% for tensile stiffness and strength, respectively) due to theeffect ofchemicals involved in the process.
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| 4. |
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| 5. |
- Al-Maqdasi, Zainab, 1986-
(författare)
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Multifunctionality and Durability of Cellulosic Fiber Reinforced Polymer Composites
- 2022
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- The overall objective of this thesis is to develop and evaluate cellulose-based fiber composites with added multifunctionality for advanced applications. In the strive towards sustainable societies and industries, materials as well as production processes need to be assessed against the sustainability criteria and selected accordingly. Cellulosic fibers reinforced polymer composites are being increasingly used in applications where weight saving, and environmental friendliness is as important as structural performance. Nonetheless, these materials have their limitations regarding durability and stability of the properties, but their potential in use for advanced applications can be expanded if functionalized and considered beyond their structural performance. Such multi-functionality of composites can be achieved by the coating of fibers and/or modifying the matrix with functional reinforcement, or by both of these routes combined. Coating of fibers and modifying the matrix with nano-reinforcement are two selected approaches for imparting functionality to the cellulosic fiber composites in the current study. Conductive Regenerated Cellulose Fibers (RCFs) were produced by coating commercial RCFs with copper via electroless plating process. Electrical conductivity and mechanical performance were evaluated, and the coated fibers were transformed into an embedded strains sensor-like assembly that could be used as structural health monitoring system in composites structures. A noticeable degradation in the mechanical strength of fibers was realized and it was attributed to the influence of the chemicals of the final plating step of process on the chains of cellulose as well as the loss of crystalline order in the RCF. In order to obtain modified matrix (nanocomposites) for multifunctional wood polymer composites (WPC), the commercial masterbatches based on Graphene Nanoplatelets (GNPs) were utilized by melt extrusion process. Effect of the processing parameters in terms of change in screw configurations and the change in composition of the constituents on the structure and mechanical performance of the nanocomposites was studied. Results showed that there is insignificant effect of the change in the screw configuration in comparison with the effect of increasing the content of the GNPs. Stronger shear forces did not result in better dispersion of the nanoparticles. Addition of the compatibilizer, on the other hand, resulted in an adverse effect on the properties compared to the formulations where it is absent. The use of GNPs with larger aspect ratio resulted in much better improvement in the mechanical performance. Addition of the nanoparticles did not only improve mechanical performance but also resulted in increased thermal conductivity and diffusivity, especially when micro-scale reinforcement was added because of synergy between wood fibers and the GNPs. This synergy was reflected also in the significant 99% improved wear resistance and the >80% reduction in the creep strains of wood and graphene reinforced composites. During the design and selection of materials, quasi-static properties are often used as a selection criterion. However, in reality structures in use are often loaded during lengthy periods of time which are followed by multiple steps of unloading/reloading, depending on the service conditions. In such cases their time-dependent response becomes more crucial than instantaneous mechanical response. Typically, characterization of these properties requires a lot of time, but it may be significantly shortened if proper modeling and analysis are employed. The effect of addition of GNPs to the polymer and wood composites has been studied experimentally by short term creep tests. The materials showed highly nonlinear response even at very low loading stresses, but the addition of the nanoparticles resulted in a decrease in the nonlinearity and in the irreversible strains due to plasticity. Modelling approaches have been used to extract parameters from experimental data that could be used in predicting long term performance using Zapas model for viscoplasticity and Schapery’s model for nonlinear viscoelasticity. Overall, the results of the performed work contribute to enriching the research field with the potential the bio-based composites have to offer in the advanced application and how nano-scale reinforcement can interact synergistically with the micro-sized fibers to improve the overall performance of WPC and under different loading scenarios.
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| 6. |
- Al-Maqdasi, Zainab, 1986-, et al.
(författare)
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Performance of recycled glass fibers from composite parts by different treatments
- 2022
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Ingår i: ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials. - Lausanne : EPFL Lausanne, Composite Construction Laboratory. - 9782970161400 ; , s. 77-84
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Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- In this work, glass fibers have been retrieved from decommissioned composite parts by three different methods. Namely, (i) pyrolysis, (ii) a novel solvolysis and (iii) a combination of solvolysis followed by pyrolysis. The techniques allowed successful recovering of sufficiently long fiber bundles (> 30 mm) that enabled separating single fibers for manual handling and testing. Single fiber tensile tests were performed to evaluate the efficiency of different recovery methods to preserve properties in comparison to the virgin fibers. The mechanical test results revealed that the stiffness of the recovered fibers has not been affected by the treatments. On the other hand, around 45% of the fiber’s strength was retained after the solvolysis process which is a comparable value to that found in literature.
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| 7. |
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| 8. |
- Al-Maqdasi, Zainab, 1986-, et al.
(författare)
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Time-dependent properties of graphene reinforced HDPE
- 2019
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Ingår i: Proceedings of 9<sup>th</sup> International Conference on Composite Testing and Model Identification.
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Konferensbidrag (övrigt vetenskapligt/konstnärligt)
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| 9. |
- Al-Maqdasi, Zainab, 1986-, et al.
(författare)
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Tribological Study on Wood and Graphene Reinforced High Density Polyethylene
- 2022
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Ingår i: ECCM 2022 - Proceedings of the 20th European Conference on Composite Materials. - Lausanne : EPFL Lausanne, Composite Construction Laboratory. - 9782970161400 ; , s. 585-592
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Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- Wear rate (WR) and coefficient of friction (COF) for high-density polyethylene (HDPE)and its composites of wood flour (WF) and/or graphene nanoplatelets (GNPs) are studied. Theinvestigation is performed by pin-on-disc test configuration on samples with different moisturecontents (dry, and samples saturated at RH of 33% and 79% in room temperature). The effect ofthe different scales of reinforcement (GNPs and WF) on these properties is discussed. Themorphological/microstructural changes in the materials induced by the motion in contact and/ormoisture content are investigated by differential scanning calorimetry (DSC). Results show thatreinforcing the polymer with WF or GNPs reduces the WR significantly, compared to neat HDPE.The hybrid reinforcements contribute to maximum improvement in wear resistance (>98%) andin the reduction of COF (>11%). The improvement in the tribological behavior of bio-basedmaterials has a significant impact on sustainable development through the improved design,durability, and environmental impact.
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| 10. |
- Al-Ramahi, Nawres Jabar, 1980-
(författare)
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Comprehensive numerical analysis of stress state in adhesive layer of joint including thermal residual stress and material non-linearity
- 2021
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- The main objective of this work is to improve understanding of the stress state in the adhesive layer of bonded joints and identify key parameters which govern performance of adhesive joints. This information is crucial for the prediction of the failure initiation and propagation with the further estimation of the durability and strength of adhesively bonded structures.A systematic numerical analysis of stress state in the adhesive layer of a single-lap and double- lap joint under various loading conditions (thermal and mechanical loading) and an alternative methodology to predict the direction for crack propagation within adhesive layer are presented in this thesis. To identification of the most important parameters of joints is done based on the assessment of the peel and shear stress distributions in the adhesive layer. The thermal residual stresses arising after assembling of joints at elevated temperature are accounted for in the analysis.Initially, accurate, realistic 3D finite element model with novel boundary conditions (displacement coupling) was developed and validated. The employed boundary conditions allow to eliminate the edge effect and simulate the behavior of an infinite plate of composite laminate with off-axis layers (monoclinic materials). It is also possible to decouple the edge effects induced by the finite specimen width from the interaction with ends of the joint overlap region. Due to these advanced setting it is possible to eliminate influence of some of the parameters as well as to reduce geometry of the model without losing precision. Thus, the model is optimized with respect to the number of elements as well as element size distribution and does not require excessive computational power to obtain accurate stress distributions even near to the possible sites with stress perturbations (e.g. corners, cracks, etc). Additionally to the geometrical parameters, various material models have been employed in simulations of adhesive joints. A linear and non-linear material models (adherend and adhesive) was used for the single-lap joint, while a linear material behavior was considered for double-lap joint. The geometrical non-linearity was also included in the analysis whenever required. To make results more general and applicable to a wide range of different joints the normalized (with respect to the thickness of adhesive layer) dimensions of joints were used. Depending on the analyzed type of joint (single- or double- lap), combination of similar and dissimilar (hybrid) materials for adherends are considered: a) metal-metal; b) composite-composite; c) composite-metal. In case of the composite adherend (carbon and/or glass fibers) different laminate lay-ups were selected: uni-directional ([08]T and [908]T) and quasi-isotropic ([0/45/90/-45]S and [90/45/0/-45]S). In general, discussion and conclusions concerning the importance of various joint parameters are based on the magnitude of the peel and shear stress concentration at the ends of the overlap. In order to identify general trends with respect to the influence of mechanical properties of adherends the master curves for shear and peel stresses are constructed and analyzed. To simulate effect of the residual thermal stresses on the behavior of joints different methods for assembly of joints were considered (using dedicated adhesive or employing co-curing method). The results of this investigation lead to the conclusions that the one of the most important factors affecting the simulation results is the sequences of application of thermo-mechanical loading for different assembly methods. It is shown that simple superposition of thermal and mechanical stresses (most common approach) in the adhesive layer works properly only for linear material but it gives inaccurate results if non-linear material is considered. The thesis demonstrates the appropriate way to combine thermal and mechanical loads to obtain correct stress distributions for any material (linear and non-linear). The analysis of the influence of residual thermal stresses has shown that the peel and shear stress concentration at the ends of overlap joint and the shear stress within the over-lap region are reduced due to thermal effect. In case of composite adherend the co-curing assembly method is more favorable (in terms of reducing stress concentrations) than using adhesive for joining the materials.Finally, the simulation of the crack propagation within the adhesive layer for the bi-material (steel and composite) DCB sample with thick adhesive layer was carried out. The alternative to traditional fracture mechanics approach is proposed for the prediction of the crack path in the adhesive layer: a maximum hoop stress criterion. The hoop stress on the perimeters of a relatively large circle around the crack tip is evaluated to predict the direction of the crack extension with respect to the existing crack. The fracture mechanics is used to validate this approach and it is proved that if the Mode I is dominant for the crack propagation the hoop stress criterion be successfully used to predict crack path in the adhesive layer. This methodology is much more effective (in terms of required time and resources) than energy release based criterion or even X-FEM.The main result of this thesis is a tool to obtain accurate stress distributions in the adhesive layer of joints. This tool provided better understanding of the behavior of adhesive joints and allowed to develop new approach for prediction of crack propagation in the adhesive layer. This is definitely a development in the design of stronger, more durable adhesive joints for lighter structural components.
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