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  • Bexell, Ulf, et al. (författare)
  • Characterisation of a Non-Organofunctional Silane Film Deposited on Al, Zn and Al-43.4Zn-1.6Si Alloy-Coated Steel, Part I. Surface Characterization by ToF-SIMS
  • 2001
  • Ingår i: Surface and Interface Analysis. - 0142-2421. ; 31:3, s. 212-222
  • Tidskriftsartikel (refereegranskat)abstract
    • The need to develop new environmentally friendly pretreatments in the surface engineering of metal substrates has become more and more important.This is mainly due to the toxic and carcinogenic properties of the chromium-based surface pretreatments frequently used in the industry. During the last decade, simple solution-dip silane-based pretreatments have emerged as promising candidates for the replacement of currently used pretreatments of metals. Recent investigations have shown that the performance of these newly developed pretreatments is strongly dependent on the chemical composition and structure of the silane film and consequently a lot of work, based on advanced surface analytical techniques, is needed in order to characterize these properties. In the present study, time-of-flight secondary ion mass spectrometry (ToF-SIMS) has been used to characterize the structure of thin films of the non-organofunctional silane 1,2-bis(triethoxysilyl)ethane (BTSE) deposited on three different metal substrates, i.e. Al, Zn and Al-43.4Zn-1.6Si (AlZn) alloy-coated steel. Of special interest was an evaluation of the influence of substrate material on the structure and composition of the silane films. The results show that the BTSE silane forms a thin, evenly distributed film over the substrate surfaces and that the molecular structure of the silane film is independent of the type of metal substrate. Analysis of the molecular ions in the positive mode shows that the surface structure of the BTSE silane is very complex and that the BTSE condensates via one to three SiOSi bridges. Also, the results show that the BTSE silane is not fully hydrolysed using a hydrolysing time of 1 h. Finally, if an alcohol is used as a solvent for the BTSE there is a clear chemical interaction between the alcohol and the silane, resulting in an exchange of alkoxy groups between the alcohol and the silane. Copyright © 2001 John Wiley & Sons, Ltd.
  • Bexell, Ulf, et al. (författare)
  • Tribological Characterisation of an Organic Coating by the use of ToF-SIMS
  • 2003
  • Ingår i: Applied Surface Science. - 0169-4332. ; 203-204, s. 596-599
  • Tidskriftsartikel (refereegranskat)abstract
    • ToF-SIMS has been used to analyse tribological induced chemical changes of organic coatings deposited on steel strip hot-dip coated with a 55.0% Al–43.4% Zn–1.6% Si alloy (Aluzink). The organic coating was a styrene–acrylic co-polymer containing different forming additives. The forming properties of the organic coatings were evaluated with modified scratch testing. The friction curves show that organic coated hot-dip coated steel displays significantly better tribological properties, i.e. lower coefficient of friction and lower wear, as compared to hot-dip coated steel. Furthermore, the organic coatings showing the highest material transfer tendency also show the highest wear. ToF-SIMS spectra show that a transfer film consisting of species from the organic coating is formed on the ball counter surface. Finally, a combination of SEM and ToF-SIMS analysis shows that mechanical failure of the coating dominates, i.e. no tribochemical changes of the coatings could be detected in the wear track.
  • Carlsson, Per, et al. (författare)
  • Tribological Behaviour of Thin Organic Permanent Coatings Deposited on Hot-dip Coated Steel Sheet - a Laboratory Study
  • 2000
  • Ingår i: Surface and Coatings Technology. - Elsevier. - 0257-8972. ; 132:2-3, s. 169-180
  • Tidskriftsartikel (refereegranskat)abstract
    • The forming and handling of hot-dip coated steel sheets is frequently associated with problems such as galling, scratching and discoloration. Recently, a new generation of thin organic coatings has been introduced on the market in order to improve the performance of hot-dip coated steel sheets and reduce these kinds of problems. In summary, these coatings have the potential to increase the formability of the steel sheet without additional lubrication, the anti-finger print properties and the corrosion protection of the product. Besides, they should also provide a pre-treatment for painting, i.e. they can be classified as permanent coatings. In the present study, the tribological behaviour of three different thin organic permanent coatings deposited on hot-dip coated (pure zinc and 55% Al–Zn) steel sheets is evaluated by three different laboratory tests; modified scratch testing, pin-on-disc testing and bending under tension testing. The results obtained show that all tests yield consistent and valuable information concerning the friction and wear properties of the materials and can, therefore, be used in order to study the tribology in sheet metal forming and the performance of different types of permanent coatings. Of the permanent coatings investigated, a pure organic coating shows the lowest coefficient of friction (µ close to 0.1) and the highest wear resistance, thus offering excellent anti-galling properties. In contrast, a mixed organic/inorganic coating displays a relatively high coefficient of friction (µ close to 0.3) and a significantly lower wear resistance. Surface analyses of the tested surfaces show that the thickness and coverage of the thin organic coating play an important role in controlling friction and wear. Furthermore, a thin organic coating optimized for improved formability and handling should display: a high adhesion to the underlying substrate material, a low coefficient of friction, a high load carrying capacity and a high intrinsic wear resistance.
  • Heinrichs, Jannica, et al. (författare)
  • Transfer of titanium in sliding contacts : New discoveries and insights revealed by in situ studies in the SEM
  • 2014
  • Ingår i: Wear. - 0043-1648. ; 315:1-2, s. 87-94
  • Tidskriftsartikel (refereegranskat)abstract
    • Titanium and its alloys generally display poor tribological properties in sliding contacts due to their high chemical activity and strong adhesion to the counter surface. The strong adhesion causes a high tendency to transfer and ultimately galling or build-up edge formation, resulting in severe surface damage. As a result, forming and machining of titanium and its alloys are generally associated with significant problems such as high friction, rapid tool wear and poor surface finish of the formed/machined surface. In the present study, in situ tests in a scanning electron microscope have been performed to increase the understanding of the mechanisms controlling the initial transfer of titanium (Grade 2) in sliding contact with tool surfaces. Tool materials included cover cold work tool steel, cemented carbide, CVD deposited Al2O3 and PVD deposited DLC. In these tests, a relatively sharp tip, representing the titanium work material, slides against a flat surface, representing the tool. The contact conditions result in plastic deformation of the work material against the tool surface, thereby simulating forming or machining. The limited and well-defined contact, along with the possibility to study the sliding in the SEM, makes it possible to correlate local surface variations to transfer of work material and frictional response. Post-test characterization of the contact surfaces was performed by high-resolution SEM, TEM, EDS and EELS. The initial friction was low and stable against all tested materials, but then gradually escalated against all surfaces except the DLC. The friction escalation was associated to increasing levels of transfer, while the DLC stayed virtually free from transfer. From these very initial sliding tests DLC is a promising tool coating in forming and machining of titanium. 
  • Carlsson, Per, et al. (författare)
  • Friction and wear mechanisms of thin organic permanent coatings deposited on hot-dip coated steel
  • 2001
  • Ingår i: Wear. - Elsevier. - 0043-1648. ; 247:1, s. 88-99
  • Tidskriftsartikel (refereegranskat)abstract
    • Adhesive wear, generally defined as ‘wear due to localised bonding between contacting solid surfaces leading to material transfer between the two surfaces or loss from either surface’ is a common phenomenon in many sliding contact tribosystems, e.g. sheet metal forming operations. In these operations, galling, i.e. seizure of the sheet surface caused by transfer of sheet material to the tool surface, is frequently a problem since it may results in scratching of the formed sheet surface and eventually cracking and fracture of the product due to high friction forces.In order to reduce the coefficient of friction and the galling tendency in sheet metal forming operations thin organic coatings has been introduced on the market with the intention of improving the performance of hot-dip coated steel sheet. In summary, these coatings have the potential to increase the formability without additional lubrication and serve as temporary corrosion protection during transportation. In the present study, the friction and wear mechanisms of five different thin organic permanent coatings deposited on hot-dip coated (Zn and 55% Al–Zn) steel sheet is evaluated by modified scratch testing.The results obtained show that this test method permits easy and reproducible evaluation of the tribological properties of thin organic coatings. Further, these coatings show a high potential when it comes to improve the formability of hot-dip coated steel. The results obtained are discussed in relation to the identified friction and wear mechanisms.
  • Carlsson, Per, et al. (författare)
  • PVD coatings for sheet metal forming : a tribological evaluation
  • 2006
  • Ingår i: Surface & Coatings Technology. - 0257-8972. ; 200:14-15, s. 4654-4663
  • Tidskriftsartikel (refereegranskat)abstract
    • The use of liquid-based lubricants in sheet metal forming mutually has a negative impact on the environment and on the whole economy, and, consequently, there is an urgent need to find a solution to make the forming processes dry or nearly dry. The deposition of a low-friction PVD coating on the forming tool has during the last years proved to be an interesting choice when it comes to create an “unlubricated” forming process. In the present study, five different PVD coatings (one CrN and four metal-carbide-doped DLC coatings) have been evaluated in sliding contact against hot dip Zn and 55% Al–Zn-coated steel sheet using a ball-on-disc test. From the investigation, it was found that all DLC coatings have potential to prevent material pickup during dry forming of hot dip Zn-coated steel. However, the as-deposited surface morphology, showing surface irregularities such as droplets and dimples, of the coatings will strongly influence the tribological performance, and, consequently, a polishing treatment or a running-in process, resulting in a smooth surface, will significantly reduce the tendency to material pickup. In sliding contact against 55% Al–Zn-coated steel, all PVD coatings display material pickup and high friction values, the only exception being a CrC-doped DLC coating in the as-polished condition. The CrN coating showed poor performance in sliding contact against both steel sheet materials due to a high tendency to material pickup. The study focuses on the tribo-induced changes of the surface condition of the PVD coating and the steel sheet surface during the sliding event. The changes in surface chemistry and topography of the tribo surfaces were characterised using scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), Auger electron spectroscopy (AES) and light interference profilometry.
  • Carlsson, Per, et al. (författare)
  • Tribological Performance of Thin Organic Permanent Coatings Deposited on 55%Al-Zn Coated Steel – Influence of Coating Composition and Thickness on Friction and Wear
  • 2001
  • Ingår i: Wear. - 0043-16.48. ; 251:1-12, s. 1075-1084
  • Tidskriftsartikel (refereegranskat)abstract
    • Dry lubricants are today increasingly being used in various types of sheet metal forming operations. Among these, permanent coatings, based on organic resins are the only lubricants which have the potential to increase the formability without additional lubrication, serve as temporary corrosion protection during transportation and, finally, serve as a pre-treatment before subsequent painting.In the present study, the influence of coating composition and thickness on the friction and wear behaviour of different thin organic permanent coatings deposited on 55%Al–Zn coated steel sheet have been evaluated by various types of laboratory tests. Surface profilometry, scanning electron microscopy (SEM), Auger electron spectroscopy (AES) and time-of-flight secondary ion mass spectrometry (ToF–SIMS) were used in order to characterise and model the tribological behaviour of the coatings.The results obtained show that the tribological properties of thin organic permanent coatings are strongly influenced by the coating thickness. In order to reduce problems associated with high friction and galling, the coating must be deposited with a uniform thickness, i.e. uncoated regions must be avoided. Furthermore, the addition of various types of additives can be used in order to further improve the tribological performance of these types of coatings.
  • Eriksson, Jenny, 1985-, et al. (författare)
  • Evaluation of galling resistance for some selected combinations of tool steels / stainless steel sheet materials/ lubricants using pin-on-disc testing
  • 2010
  • Ingår i: NordTrib 2010 : 14th Nordic Symposium on Tribology, Storforsen, Sweden.
  • Konferensbidrag (refereegranskat)abstract
    • Stainless steels are well known to be prone to cold welding and material transfer in sliding contacts and therefore difficult to cold form unless certain precautions as discussed in this paper are taken. In the present study different combinations of tool steels/stainless steels/lubricants has been evaluated with respect to their galling resistance using pin-on-disc testing. The results show that a high galling resistance is favored by a high stainless steel sheet hardness and a blasted stainless steel sheet surface topography. The effect of type of lubricant was found to be more complex. For example, the chlorinated lubricants failed to prevent metal-to-metal contact on a brushed sheet surface but succeeded on a blasted sheet surface of the same stainless steel material. This is believed to be due to a protective tribofilm which is able to form on the blasted surface, but not on the brushed surface.
  • Eriksson, Jenny, 1985-, et al. (författare)
  • Tribological testing of commercial CrN, (Ti,Al)N and CrC/C PVD coatings : evaluation of galling and wear characteristics against different high strength steels
  • 2011
  • Ingår i: Surface & Coatings Technology. - Lausanne : Elsevier. - 0257-8972. ; 205:16, s. 4045-4051
  • Tidskriftsartikel (refereegranskat)abstract
    • The increasing use of high strength steels in a variety of mechanical engineering applications has illuminated problems associated with galling in sheet metal forming operations. Galling is a tribological phenomenon associated with transfer of material from the steel sheet to the tool surface during forming resulting in seizure of the tool/steel sheet contact and extensive scratching of the steel sheet surface. As a result, a number of concepts have been developed in order to reduce the tendency of galling in sheet metal forming, including the development of new dry lubricants, new forming tool steel grades and improved surface engineering treatments such as the deposition of low friction CVD- and PVD-coatings. In the present study the potential performance of three commercial PVD coatings, including CrN, (Ti,Al)N and a CrC/C DLC-based coating, in the forming of hot and cold rolled high strength steel as well as electro and hot-dip galvanized high strength steel has been evaluated using pin-on-disc testing under lubricated contact conditions. Post-test examination of the tribosurfaces using FEG-SEM and EDS analyses was performed in order to evaluate the mechanisms controlling the tendency to material transfer and wear. The results show that in contact with the hot and cold rolled steel the material pick-up tendency of the PVD coatings tend to increase in the order CrC/C–CrN–(Ti,Al)N while in contact with the two galvanized steel sheets, the CrC/C and the (Ti,Al)N coating show a significantly lower material pick-up tendency as compared with the CrN coating. Further, the substrate hardness has a strong influence on the wear of the PVD coatings and consequently on the friction characteristics and galling tendency of the coating/substrate composite. Low substrate hardness, resulting in a low load bearing capacity, increases the tendency to cracking and subsequently chipping of the brittle coating.
  • Fallqvist, Mikael, 1982-, et al. (författare)
  • Abrasive wear of multilayer kappa-Al2O3-Ti(C,N) CVD coatings on cemented carbide
  • 2007
  • Ingår i: Wear. - 0043-1648. ; 263:1-6, s. 74-80
  • Tidskriftsartikel (refereegranskat)abstract
    • In the present study the wear resistance of kappa-Al2O3–Ti(C,N) multilayer CVD coatings with different multilayer structures (8, 15, 32 layers of kappa-Al2O3 separated by thin Ti(C,N) layers) have been investigated using a micro-abrasion and a cutting test. The results show that the wear rate of the kappa-Al2O3 multilayer coatings tend to decrease with decreasing layer thickness in the micro-abrasion test and decrease with increasing layer thickness in the cutting tests. The reason for this is mainly due to the difference in wear behaviour depending on temperature. The results obtained are discussed in relation to the dominant wear mechanisms of the coatings which have been identified using scanning electron microscopy and energy dispersive X-ray spectroscopy. The potential of the micro-abrasion test in the characterisation of thin CVD coatings for cutting tool applications is discussed.
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