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Efficient Conversion of Lignocellulosic Biomass to Levulinic Acid Using Acidic Ionic Liquids
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- Khan, Amir Sada (författare)
- Center of Research in Ionic Liquids, Department of Chemical Engineering, Universiti Teknologi PETRONAS
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- Man, Zakaria (författare)
- Center of Research in Ionic Liquids, Department of Chemical Engineering, Universiti Teknologi PETRONAS
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- Bustam, Mohamad Azmi (författare)
- Center of Research in Ionic Liquids, Department of Chemical Engineering, Universiti Teknologi PETRONAS
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- Nasrullah, Asma (författare)
- Fundamental and Applied Science Department, Universiti Teknologi PETRONAS
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- Ullah, Zahoor (författare)
- Department of Chemistry, Balochistan University of IT, Engineering and Management Sciences (BUITEMS)
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- Sarwono, Ariyanti (författare)
- Center of Research in Ionic Liquids, Department of Chemical Engineering, Universiti Teknologi PETRONAS
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- Shah, Faiz Ullah (författare)
- Luleå tekniska universitet,Kemiteknik
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- Muhammad, Nawshad (författare)
- Interdisciplinary Research Center in Biomedical Materials, COMSATS Institute of Information Technology, Lahore, Pakistan
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(creator_code:org_t)
- Elsevier, 2018
- 2018
- Engelska.
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Ingår i: Carbohydrate Polymers. - : Elsevier. - 0144-8617 .- 1879-1344. ; 181, s. 208-214
- Relaterad länk:
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Ämnesord
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- In the present research work, dicationic ionic liquids, containing 1,1-Bis(3-methylimidazolium-1-yl) butylene ([C4(Mim)2]) cation with counter anions [(2HSO4)(H2SO4)0], [(2HSO4)(H2SO4)2] and [(2HSO4)(H2SO4)4] were synthesised. ILs structures were confirmed using 1H NMR spectroscopy. Thermal stability, Hammett acidity, density and viscosity of ILs were determined. Various types of lignocellulosic biomass such as rubber wood, palm oil frond, bamboo and rice husk were converted into LA. Among the synthesized ionic liquids, [C4(Mim)2][(2HSO4)(H2SO4)4] showed higher % yield of LA up to 47.52 from bamboo biomass at 100 °C for 60 min, which is the better yield at low temperature and short time compared to previous reports. Surface morphology, surface functional groups and thermal stability of bamboo before and after conversion into LA were studied using SEM, FTIR and TGA analysis, respectively. This one-pot production of levulinic acid from agro-waste will open new opportunity for the conversion of sustainable biomass resources into valuable chemicals.
Ämnesord
- NATURVETENSKAP -- Kemi -- Fysikalisk kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences -- Physical Chemistry (hsv//eng)
Nyckelord
- Chemistry of Interfaces
- Gränsytors kemi
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