| 1. |
- Seoane Martinez, Fernando, 1976, et al.
(författare)
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Simple voltage-controlled current source for wideband electrical bioimpedance spectroscopy: circuit dependences and limitations
- 2011
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Ingår i: Measurement Science and Technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 22:11
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Tidskriftsartikel (refereegranskat)abstract
- In this work, the single Op-Amp with load-in-the-loop topology as a current source is revisited. This circuit topology was already used as a voltage-controlled current source (VCCS) in the 1960s but was left unused when the requirements for higher frequency arose among the applications of electrical bioimpedance (EBI). The aim of the authors is not only limited to show that with the currently available electronic devices it is perfectly viable to use this simple VCCS topology as a working current source for wideband spectroscopy applications of EBI, but also to identify the limitations and the role of each of the circuit components in the most important parameter of a current for wideband applications: the output impedance. The study includes the eventual presence of a stray capacitance and also an original enhancement, driving with current the VCCS. Based on the theoretical analysis and experimental measurements, an accurate model of the output impedance is provided, explaining the role of the main constitutive elements of the circuit in the source's output impedance. Using the topologies presented in this work and the proposed model, any electronic designer can easily implement a simple and efficient current source for wideband EBI spectroscopy applications, e. g. in this study, values above 150 k Omega at 1 MHz have been obtained, which to the knowledge of the authors are the largest values experimentally measured and reported for a current source in EBI at this frequency.
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| 2. |
- Hagqvist, Petter, 1986, et al.
(författare)
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Emissivity compensated spectral pyrometry-algorithm and sensitivity analysis
- 2014
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Ingår i: Measurement Science and Technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 25:2
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Tidskriftsartikel (refereegranskat)abstract
- In order to solve the problem of non-contact temperature measurements on an object with varying emissivity, a new method is herein described and evaluated. The method uses spectral radiance measurements and converts them to temperature readings. It proves to be resilient towards changes in spectral emissivity and tolerates noisy spectral measurements. It is based on an assumption of smooth changes in emissivity and uses historical values of spectral emissivity and temperature for estimating current spectral emissivity. The algorithm, its constituent steps and accompanying parameters are described and discussed. A thorough sensitivity analysis of the method is carried out through simulations. No rigorous instrument calibration is needed for the presented method and it is therefore industrially tractable.
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| 3. |
- Hagqvist, Petter, 1986-, et al.
(författare)
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Emissivity compensated spectral pyrometry for varying emissivity metallic measurands
- 2014
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Ingår i: Measurement Science and Technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 25:2
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Tidskriftsartikel (refereegranskat)abstract
- A novel method for converting electromagnetic spectral radiance information into temperature measurements is presented. It allows for varying spectral emissivity of the metallic measurand during the course of the measurement. Such variations are due to, e. g., thermal oxidation or temperature dependent emissivity. Based on a requirement that emissivity changes with time and temperature are smooth, it is assumed that an emissivity estimate at one sample instance can be derived from the estimated emissivity found at the previous samples together with updated spectral information. This leads to successive recalculations of spectral emissivity together with corresponding temperature values. The proposed algorithm has been proven to give accurate temperature estimates from a measurement based on the data captured by a standard UV-Vis spectrophotometer even for an oxidizing Ti-6Al-4V specimen in a temperature range between 900 and 1400 K. The method however, is not limited to these wavelength or temperature ranges.
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| 4. |
- Jansson, Anna, 1985, et al.
(författare)
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Monitoring the osmotic response of single yeast cells through force measurement in the environmental scanning electron microscope
- 2014
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Ingår i: Measurement science and technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 25:2
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Tidskriftsartikel (refereegranskat)abstract
- We present a measurement system that combines an environmental scanning electron microscope (ESEM) and an atomic force microscope (AFM). This combination enables studies of static and dynamic mechanical properties of hydrated specimens, such as individual living cells. The integrated AFM sensor provides direct and continuous force measurement based on piezoresistive force transduction, allowing the recording of events in the millisecond range. The in situ ESEM-AFM setup was used to study Pichia pastoris wild-type yeast cells. For the first time, a quantified measure of the osmotic response of an individual yeast cell inside an ESEM is presented. With this technique, cell size changes due to humidity variations can be monitored with nanometre accuracy. In addition, mechanical properties were extracted from load-displacement curves. A Young's modulus of 13-15 MPa was obtained for the P. pastoris yeast cells. The developed method is highly interesting as a complementary tool for the screening of drugs directed towards cellular water transport activity and provides new possibilities of studying mechanosensitive regulation of aquaporins.
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| 5. |
- Knappe, Christoph, et al.
(författare)
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Enhanced color ratio calibration approach for two-dimensional surface thermometry using laser-induced phosphorescence
- 2013
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Ingår i: Measurement Science & Technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 24:8
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Tidskriftsartikel (refereegranskat)abstract
- An alternative concept for calibrating spectral image intensity ratios is described, which provides simple, but effective means of compensation for systematic errors, caused by nonlinearities in signal detection. The method relies on image segmentation by means of signal thresholds, where pixels are organized into different subgroups according to their corresponding signal count value. Instead of defining one global spectral ratio per calibration temperature, the phosphor-coated target surface is illuminated inhomogeneously and resulting image ratios are calibrated individually for each pixel intensity subgroup. This allows the exploitation of high intensity regions on the camera chip which offer great precision advantages, but suffer from systematic errors caused by signal nonlinearities. Temperature calibration data of BaMg2Al16O27:Eu in the temperature range between 270 and 470 K was used to assess and compare the potential of both calibration approaches. In comparison to the conventional, e.g. global calibration approach, accuracy improvements of up to 39% were gained even while keeping average signal intensities below 15% of the detector’s full dynamic range. Image ratio evaluations, based on segregated pixel subgroups, could help improve measurement accuracy also for other techniques, relying on the calibration of measured quantities. In two-dimensional phosphor thermometry, it helps bridge the current precision gap between two-color ratio methods and more elaborate lifetime-imaging approaches.
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| 6. |
- Buendia, Ruben, 1982, et al.
(författare)
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Experimental Validation of a Method for Removing the Capacitive Leakage Artifact from Electrical Bioimpedance Spectroscopy Measurements
- 2010
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Ingår i: Measurement Science and Technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 21:11, s. 115802-
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Tidskriftsartikel (refereegranskat)abstract
- Often when performing electrical bioimpedance (EBI) spectroscopy measurements, the obtained EBI data present a hook-like deviation, which is most noticeable at high frequencies in the impedance plane. The deviation is due to a capacitive leakage effect caused by the presence of stray capacitances. In addition to the data deviation being remarkably noticeable at high frequencies in the phase and the reactance spectra, the measured EBI is also altered in the resistance and the modulus. If this EBI data deviation is not properly removed, it interferes with subsequent data analysis processes, especially with Cole model-based analyses. In other words, to perform any accurate analysis of the EBI spectroscopy data, the hook deviation mustbe properly removed. Td compensation is a method used to compensate the hook deviation present in EBI data; it consists of multiplying the obtained spectrum, Zmeas(ω), by a complex exponential in the form of exp(–jωTd). Although the method is well known and accepted, Td compensation cannot entirely correct the hook-like deviation; moreover, it lacks solid scientific grounds. In this work, the Td compensation method is revisited, and it is shown that it should not be used to correct the effect of a capacitive leakage; furthermore, a more developed approach for correcting the hook deviation caused by the capacitive leakage is proposed. The method includes a novel correcting expression and a process for selecting the proper values of expressions that are complex and frequency dependent. The correctness of the novel method is validated with the experimental data obtained from measurements from three different EBI applications. The obtained results confirm the sufficiency and feasibility of the correcting method.
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| 7. |
- Abou Nada, Fahd Jouda, et al.
(författare)
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Development of an automatic routine for calibration of thermographic phosphors
- 2014
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Ingår i: Measurement Science & Technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 25:2
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Tidskriftsartikel (refereegranskat)abstract
- An automated routine for the continuous calibration of thermographic phosphors was developed as a replacement for the conventional calibration scheme that relied on fixed temperature points. The automated calibration routine was validated using Mg 3 F 2 GeO 4 :Mn as a calibration phosphor. Hardware and software aspects of the calibration process were addressed in this development. The hardware aspect included a new substrate design using a high performance alloy, the Hastelloy-C alloy, whereas the software aspect included an automated acquisition system which was capable of acquiring simultaneous thermocouple temperatures and phosphor decay waveform in real time. The design of the calibration process eliminates the need for a system in thermal equilibrium during a phosphor calibration measurement. Temperature ramping rates of up to 4 K min −1 were employed in the oven without a delay in the temperature response being measured between the phosphor and the thermocouples involved. In addition, the automated calibration setup allowed for detailed investigations on the effect of heat being delivered to the phosphor coating by the laser. These findings were confirmed by a simple heat transfer model, based on lumped system analysis. In comparison to the data acquisition performed at several fixed points with the conventional calibration scheme, the experiment duration was shortened by a factor of 4 with the overall accuracy improved by 1–2 K.
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| 8. |
- Albani, Giorgia, et al.
(författare)
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Evolution in boron-based GEM detectors for diffraction measurements : From planar to 3D converters
- 2016
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Ingår i: Measurement science and technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 27:11
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Tidskriftsartikel (refereegranskat)abstract
- The so-called '3He-crisis' has motivated the neutron detector community to undertake an intense R&D programme in order to develop technologies alternative to standard 3He tubes and suitable for neutron detection systems in future spallation sources such as the European spallation source (ESS). Boron-based GEM (gas electron multiplier) detectors are a promising '3He-free' technology for thermal neutron detection in neutron scattering experiments. In this paper the evolution of boron-based GEM detectors from planar to 3D converters with an application in diffraction measurements is presented. The use of 3D converters coupled with GEMs allows for an optimization of the detector performances. Three different detectors were used for diffraction measurements on the INES instrument at the ISIS spallation source. The performances of the GEM-detectors are compared with those of conventional 3He tubes installed on the INES instrument. The conceptual detector with the 3D converter used in this paper reached a count rate per unit area of about 25% relative to the currently installed 3He tube. Its timing resolution is similar and the signal-to-background ratio (S/B) is 2 times lower.
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| 9. |
- Bladh, Henrik, et al.
(författare)
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Flame propagation visualization in a spark-ignition engine using laser-induced fluorescence of cool-flame species
- 2005
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Ingår i: Measurement Science & Technology. - : IOP Publishing. - 0957-0233 .- 1361-6501. ; 16:5, s. 1083-1091
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Tidskriftsartikel (refereegranskat)abstract
- The flame propagation in a spark-ignition engine has been studied using laser-induced fluorescence (LIF) of species formed during the first ignition stage of hydrocarbon combustion. The detected two-dimensional LIF images showed the distribution of unburned regions. For the excitation, two Nd:YAG lasers operating at 355 mn were used for two consecutive measurements within the same engine cycle with adjustable time separation between the pulses. Two ICCD cameras that were synchronized to each of the laser pulses recorded pairs of fluorescence images, i.e. the movement of the flame front could be tracked. It is well known that formaldehyde is excited using a wavelength of 355 nm and a spectral signature of this species was also identified in engine LIF spectra. Programme routines were developed and used for evaluation of the flame propagation velocity from the fluorescence images. This paper presents the potential and the characteristics of the experimental technique as well as the evaluation procedure. The measurements of cool-flame intermediates have also been compared with measurements of fuel-tracer as an indicator of unburned fuel-air mixture. A good agreement between position and shape of the signal areas was obtained at crank angles where both fluorescence signal from cool-flame species excited at 355 nm and added 3-pentanone excited at 266 nm could be detected.
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| 10. |
- Brackmann, Christian, et al.
(författare)
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Thermometry in internal combustion engines via dual-broadband rotational coherent anti-Stokes Raman spectroscopy
- 2004
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Ingår i: Measurement Science & Technology. - 0957-0233. ; 15:3, s. 13-25
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Forskningsöversikt (refereegranskat)abstract
- Rotational coherent anti-Stokes Raman spectroscopy (CARS) has since the beginning of the 1980s been developed as a non-intrusive tool for temperature measurements in combustion. Since the introduction of the dual-broadband concept in 1986, the quality of the technique has been much improved, and application to practical combustion situations facilitated. Since the first demonstration of its use in spark-ignition engines in 1993, several measurement campaigns in engines have been accomplished. These campaigns concerned temperature measurements in the unburned gas mixture before combustion as part of a larger project with the aim of improving the knowledge on the phenomenon of engine knock. In this paper, the results of this work are reviewed with a focus on the characteristics of the technique and the quality of the evaluated temperatures. Re-evaluations of data using an improved theoretical model are presented and compared with previous results. Moreover, the treatment of large data sets on single shots from spatial regions with conditions varying from unburned to burned gas is discussed. It is demonstrated that dual-broadband rotational CARS probing nitrogen and oxygen has a high potential for thermometry at the conditions in the unburned gas mixture. Merits and limitations of the technique are discussed and the issues treated are, among others, experimental problems, data evaluation, and single-shot temperature accuracy.
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