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Sökning: WFRF:(Sobczak J. W.)

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1.
  • Sawicki, M., et al. (författare)
  • Homogeneous and heterogeneous magnetism in (Zn,Co)O : From a random antiferromagnet to a dipolar superferromagnet by changing the growth temperature
  • 2013
  • Ingår i: Physical Review B. Condensed Matter and Materials Physics. - 1098-0121 .- 1550-235X. ; 88:8
  • Tidskriftsartikel (refereegranskat)abstract
    • A series of (Zn,Co)O layers with Co contents x up to 40% grown by atomic layer deposition have been investigated. All structures deposited at 160 degrees C show magnetic properties specific to II-VI dilute magnetic semiconductors with localized spins S = 3/2 coupled by strong but short-range antiferromagnetic interactions resulting in low-temperature spin-glass freezing for x = 0.16 and 0.4. At higher growth temperature (200 degrees C) metallic Co nanocrystals precipitate in two locations giving rise to two different magnetic responses: (i) a superparamagnetic contribution coming from volume disperse nanocrystals; (ii) a ferromagneticlike behavior brought about by nanocrystals residing at the (Zn,Co)O/substrate interface. It is shown that the dipolar coupling within the interfacial two-dimensional dense dispersion of nanocrystals is responsible for the ferromagneticlike behavior.
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2.
  • Ilieva, L., et al. (författare)
  • Pure hydrogen production via PROX over gold catalysts supported on Pr-modified ceria
  • 2014
  • Ingår i: Fuel. - : Elsevier BV. - 0016-2361 .- 1873-7153. ; 134, s. 628-635
  • Tidskriftsartikel (refereegranskat)abstract
    • Two series of Pr-doped (5 and 10 at.% Pr) cerium oxides were synthesized by impregnation (IM) and microemulsion method (ME). The Au catalysts (3 wt.%) supported on these oxides were tested in PROX. The samples were characterized by XRD, XPS and TPR measurements. At the operating temperature of the fuel cells (80-120 degrees C) gold catalysts on Pr-doped ceria supports synthesized by IM method exhibited much higher PROX activity as compared to the case of ME method. The observed different catalytic behavior was attributed to the different support preparation affecting the gold particle sizes and the mixed support features. In the case of mixed supports synthesized by IM the size of gold particles established by XRD is smaller and the supply of oxygen evidenced by the obtained TPR results is higher as compared to the gold catalysts on the ME prepared mixed supports. The higher gold dispersion as well as the more defective structure assumed by higher microstrain parameter of ceria lattice (XRD data) due to Pr-doping by IM method, improved both the reducibility and the PROX activity up to 120 degrees C.
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