| 1. |
- Altenkirch, J., et al.
(författare)
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Comparison of methods to determine variations in unstrained unit cell parameter across welds
- 2011
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Ingår i: Journal of Strain Analysis for Engineering Design. - : SAGE Publications. - 0309-3247 .- 2041-3130. ; 46:7, s. 651-662
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Tidskriftsartikel (refereegranskat)abstract
- Many alloys undergo complex changes in local chemistry in the vicinity of weldments due to the thermal excursion during welding. The resulting changes in solute concentrations can lead to significant local variations in the unstrained unit cell parameter which, if not accounted for, can lead to serious error when determining residual stress by diffraction methods. Age-hardening aluminium alloys are particularly susceptible to such effects. The present paper compares three methods (plane stress assumption, sin(2)psi method, and comb correction method) for evaluating the stress-free unit cell parameter variation for friction stir welds in AA7449-W51 plates of two different thicknesses. All three methods gave comparable results for thin (5 mm) sheet, but for the thicker (12.2 mm) plate the results calculated on the basis of the plane stress assumption diverged from the other two, largely because in this case the other methods indicate there to be a significant triaxiality of stress. In the example cases, hardness and unstrained unit cell parameter variations were found to be strongly correlated across the welds. The advantages and disadvantages of the three methods are compared.
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| 2. |
- Altenkirch, J., et al.
(författare)
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Mechanical Tensioning of High-Strength Aluminum Alloy Friction Stir Welds
- 2008
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Ingår i: Symposium on Neutron and X-Ray Studies for Probing Materials Behavior held at the 137th TMS Annual Meeting and Exhibition. - : Springer Science and Business Media LLC. - 1073-5623. ; 39A, s. 3246-3259
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Konferensbidrag (refereegranskat)abstract
- The extent to which in-situ global mechanical tensioning (GMT) can be used to modify the residual stress state in friction stir (FS) welds is investigated in this article. Residual stress distributions have been determined by synchrotron X-ray and neutron diffraction for four sets of FS welds in high-strength AA7449-W51 and lithium containing AA2199-T8 aerospace aluminum alloys subjected to a systematic range of GMT levels. For the cases studied, the results indicate that the level of residual stresses present in the as-welded state is a function of the alloy. The rate of residual stress reduction brought about by GMT, however, is basically alloy independent; indeed, it is essentially linear with respect to the GMT load, so that the tensioning required to reduce the weld stresses to zero can be calculated directly from the stresses present in the untensioned case. For thin plates, proximity to the yield stress in the hot-softened zone means that a guideline rule is that 1 MPa of tensioning during welding reduces the tensile stress by approximately 1 MPa. The GMT was found to be less effective at greater depths in thick plates. Furthermore, a reduction in bending distortion and an increase in angular distortion was observed with increased GMT, while no effects on the weld microstructure and hardness were observed.
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| 3. |
- Altenkirch, J., et al.
(författare)
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The extent of relaxation of weld residual stresses on cutting out cross-weld test-pieces
- 2009
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Ingår i: Powder Diffraction. - : Cambridge University Press (CUP). - 0885-7156 .- 1945-7413. ; 24:2, s. 31-36
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Tidskriftsartikel (refereegranskat)abstract
- Weld residual stress (RS) measurements are often undertaken on test-pieces which have been Cut Out from large components, yet it remains unclear to what extent the RSs in test-pieces are representative of those present in the original component. Similarly weld mechanical performance tests are frequently undertaken on cross-weld test-pieces without a proper understanding of the level or influence of retained RS. We present a systematic study of the relaxation of longitudinal RS in thin-plate butt welds produced using different materials and welding methods (FSW, laser-MIG, and pulsed-MIG). In each case the RSs were measured repeatedly in the same location as the welds were progressively and symmetrically cut down. Although cutting inevitably leads to stress redistribution, significant relaxation of the longitudinal RS was only observed when the weld length or width was reduced to below a certain value. This critical value appears to correlate with the lateral width of the tensile zone local to the weld-line and may be considered to be the characteristic length as defined in St. Venant's principle. Further, it was found that the level of stress relaxation as a function of weld length for all the welds studied could be collapsed onto a single empirical curve using a simple approach based on the characteristic length scales of the weld. Given the range of materials and welding methods used, this relation appears to be of general use for thin-plate welds although further work is required to test the limits of its applicability. (C) 2009 International Centre for Diffraction Data. [DOI: 10.1154/1.3152580]
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| 4. |
- Attallah, Moataz M., et al.
(författare)
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Microstructural and Residual Stress Development due to Inertia Friction Welding in Ti-6246
- 2012
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Ingår i: Metallurgical and Materials Transactions A - Physical Metallurgy and Materials Science. - : Springer Science and Business Media LLC. - 1073-5623. ; 43A:9, s. 3149-3161
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Tidskriftsartikel (refereegranskat)abstract
- A thorough investigation has been performed to assess the microstructural properties, mechanical properties (hardness and elastic modulus), and residual stress development in Ti-6Al-2Sn-4Zr-6Mo (Ti-6246) inertia friction welds in the as-welded and postweld heat-treated conditions. It was evident that the thermomechanical deformation in the weld region occurred above the beta transus, forming dynamically recrystallized beta grains and precipitating acicular alpha within the beta grains, which resulted in a localized hardness increase. In the heat-affected zone, a ghost microstructure of the base metal formed because of the absence of sufficient time for diffusion, resulting in Mo segregation in the prior primary alpha plates. Energy-dispersive synchrotron X-ray diffraction and neutron diffraction were used to assess the residual stress development in the three principal directions. The variation in the unstrained lattice parameters across the weld regions was established by imposing a stress balance on the axial stress component in the radial direction. It was found that the maximum stresses occurred in the hoop direction, with significantly lower stresses present in the radial and axial directions. The maximum tensile hoop stresses were located at similar to 4 mm from the weld centerline and not at the dynamically recrystallized beta-rich weld zone. This was associated with the alpha -> beta phase transformation and the subsequent acicular alpha precipitation within the region surrounding the weld centerline.
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| 5. |
- Barnes, S. J., et al.
(författare)
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Friction Stir Welding in HSLA-65 Steel: Part I. Influence of Weld Speed and Tool Material on Microstructural Development
- 2012
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Ingår i: Metallurgical and Materials Transactions A - Physical Metallurgy and Materials Science. - : Springer Science and Business Media LLC. - 1073-5623. ; 43A:7, s. 2342-2355
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Tidskriftsartikel (refereegranskat)abstract
- A systematic set of single-pass full penetration friction stir bead-on-plate and butt-welds in HSLA-65 steel were produced using a range of different traverse speeds (50 to 500 mm/min) and two tool materials (W-Re and PCBN). Microstructural analysis of the welds was carried out using optical microscopy, and hardness variations were also mapped across the weld-plate cross sections. The maximum and minimum hardnesses were found to be dependent upon both welding traverse speed and tool material. A maximum hardness of 323 Hv(10) was observed in the mixed martensite/bainite/ferrite microstructure of the weld nugget for a welding traverse speed of 200 mm/min using a PCBN tool. A minimum hardness of 179 Hv(10) was found in the outer heat-affected zone (OHAZ) for welding traverse speed of 50 mm/min using a PCBN tool. The distance from the weld centerline to the OHAZ increased with decreasing weld speed due to the greater heat input into the weld. Likewise for similar energy inputs, the size of the transformed zone and the OHAZ increased on moving from a W-Re tool to a PCBN tool probably due to the poorer thermal conductivity of the PCBN tool. The associated residual stresses are reported in Part II of this series of articles.
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| 6. |
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| 7. |
- Cereser, Alberto, et al.
(författare)
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Time-of-Flight Three Dimensional Neutron Diffraction in Transmission Mode for Mapping Crystal Grain Structures
- 2017
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Ingår i: Scientific Reports. - : Springer Science and Business Media LLC. - 2045-2322. ; 7:1
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Tidskriftsartikel (refereegranskat)abstract
- The physical properties of polycrystalline materials depend on their microstructure, which is the nano- to centimeter scale arrangement of phases and defects in their interior. Such microstructure depends on the shape, crystallographic phase and orientation, and interfacing of the grains constituting the material. This article presents a new non-destructive 3D technique to study centimeter-sized bulk samples with a spatial resolution of hundred micrometers: time-of-flight three-dimensional neutron diffraction (ToF 3DND). Compared to existing analogous X-ray diffraction techniques, ToF 3DND enables studies of samples that can be both larger in size and made of heavier elements. Moreover, ToF 3DND facilitates the use of complicated sample environments. The basic ToF 3DND setup, utilizing an imaging detector with high spatial and temporal resolution, can easily be implemented at a time-of-flight neutron beamline. The technique was developed and tested with data collected at the Materials and Life Science Experimental Facility of the Japan Proton Accelerator Complex (J-PARC) for an iron sample. We successfully reconstructed the shape of 108 grains and developed an indexing procedure. The reconstruction algorithms have been validated by reconstructing two stacked Co-Ni-Ga single crystals, and by comparison with a grain map obtained by post-mortem electron backscatter diffraction (EBSD).
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| 8. |
- Chahardehi, A., et al.
(författare)
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The effect of residual stresses arising from laser shock peening on fatigue crack growth
- 2010
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Ingår i: Engineering Fracture Mechanics. - : Elsevier BV. - 0013-7944. ; 77:11, s. 2033-2039
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Konferensbidrag (refereegranskat)abstract
- Residual stresses have in the past been introduced to manipulate growth rates and shapes of cracks under cyclic loads. Previously, the effectiveness of shot peening in retarding the rate of fatigue crack growth was experimentally studied. It was shown that the compressive residual stresses arising from the shot peening process can affect the rate of crack growth. Laser shock peening can produce a deeper compressive stress field near the surface than shot peening. This advantage makes this technique desirable for the manipulation of crack growth rates. This paper describes an experimental program that was carried out to establish this effect in which steel specimens were partially laser peened and subsequently subjected to cyclic loading to grow fatigue cracks. The residual stress fields generated by the laser shock peening process were measured using the neutron diffraction technique. A state of compressive stress was found near the surface and tensile stresses were measured in the mid-thickness of the specimens. Growth rates of the cracks were observed to be more affected by the tensile core than by the compressive surface stresses. (c) 2010 Elsevier Ltd. All rights reserved.
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| 9. |
- Colegrove, P., et al.
(författare)
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Welding process impact on residual stress and distortion
- 2009
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Ingår i: Science and Technology of Welding and Joining. - 1362-1718. ; 14:8, s. 717-725
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Tidskriftsartikel (refereegranskat)abstract
- Residual stress and distortion continue to be important issues in shipbuilding and are still subject to large amounts of research. This paper demonstrates how the type of welding process influences the amount of distortion. Many shipyards currently use submerged arc welding (SAW) as their welding process of choice. In this manuscript, the authors compare welds made by SAW with DC gas metal arc welding, pulsed gas metal arc welding, Fronius cold metal transfer (CMT), autogenous laser and laser hybrid welding on butt welds in 4 mm thick DH36 ship plate. Laser and laser hybrid welding were found to produce the lowest distortion. Nevertheless, a considerable improvement can be achieved with the pulsed gas metal arc welding and CMT processes. The paper seeks to understand the relationship between heat input, fusion area, measured distortion and the residual stress predicted from a simple numerical model, and the residual stresses validated with experimental data.
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| 10. |
- du Plessis, Hester Esna, et al.
(författare)
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In situ reduction study of cobalt model Fischer-Tropsch synthesis catalysts
- 2013
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Ingår i: Physical Chemistry Chemical Physics. - : Royal Society of Chemistry (RSC). - 1463-9084 .- 1463-9076. ; 15:28, s. 11640-11645
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Tidskriftsartikel (refereegranskat)abstract
- Fischer-Tropsch (FT) synthesis is an important process to manufacture hydrocarbons and oxygenated hydrocarbons from mixtures of carbon monoxide and hydrogen (syngas). The catalysis process occurs on, for example, cobalt metal surfaces at elevated temperatures and pressures. A fundamental understanding of the reduction pathway of supported cobalt oxides, and the intermediate species present during the activation, can assist in developing improved industrial supported cobalt catalysts. Hard synchrotron X-rays have the unique ability to probe atomic processes both in terms of phases present as well as the crystallographic and local structure (using the pair distribution function approach) under realistic conditions. In this manuscript we present results from measurements during in situ hydrogen activation of a model Co/alumina catalyst using in situ synchrotron X-ray powder diffraction and pair-distribution function (PDF) analysis on beam line ID31 at the ESRF in Grenoble, France. The PDF analysis showed a substantially improved understanding of the reduction of cobalt oxides, as for the first time all cobalt could be accounted for by using total scattering analysis.
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