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- Das, Prabir Kumar, 1982-
(författare)
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Ageing of Asphalt Mixtures : Micro-scale and mixture morphology investigation
- 2014
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- There are many variables that affect the viscoelastic properties of asphalt mixtures with time, among which age hardening may be considered one of the important ones. Age hardening of asphalt mixtures is an irreversible process, which contributes to a reduction of the durability of pavements and eventually increases the maintenance cost. Beside the environmental effects, ageing in asphalt mixture depends on the physicochemical properties of bitumen and mixture morphology which is a combined effect of aggregate packing, porosity, air void distribution and their interconnectivity. Thus, a clear understanding on the physicochemical properties of bitumen and mixture morphology may help to predict the performance of asphalt mixtures, which will contribute to longer-lasting and better performing pavements.When looking at the bitumen at micro-scale, one can see microstructures appearing under certain conditions which can be partially explained by the interaction of the individual phases. Since the thermo-rheological behavior of bitumen depends largely on its chemical structure and intermolecular microstructures, studying these can lead to understanding of the mechanism, speed and conditions under which this phase behavior occurs. Linking this to the changes in properties of bitumen can thus lead to better understanding of the causes of ageing, its dominant parameters and the resulting diminished mechanical response.To investigate ageing in asphalt pavements, along with physicochemical properties of bitumen one needs to also focus on the influence of mixture morphology. It is known that asphalt mixtures with similar percentages of air-voids can have different morphologies and thus can age differently. Prediction of ageing behavior without considering the influence of mixture morphology may thus lead to erroneous conclusions and non-optimal mix design. Hence, it is important to understand the interplay between the mixture morphology and ageing susceptibility and relate this to the long term mixture performance.The aim of this Thesis was to develop fundamental understanding on ageing in asphalt mixtures that can contribute to the asphalt community moving away from the currently used accelerated ageing laboratory tests and empirical models that can lead to erroneous conclusions.To reach this aim, experimental and numerical micro-scale analyses on bitumen and meso-scale investigations on mixture morphology have been performed which, collectively, allowed for the development of a method for the prediction of asphalt field ageing, incorporating both mixture morphology and micro-scale bitumen mechanisms. For this, first, the mechanisms of surface ageing and diffusion controlled oxidative ageing were identified. Secondly, the influence of mixture morphology on asphalt ageing susceptibility was investigated. Procedures to determine the controlling parameter were then developed and an empirical framework to quantify the long-term field ageing of asphalt mixtures was set-up. For this, a combination of experimental and numerical methods was employed.An extensive experimental study was carried out to understand the fundamental mechanisms behind the micro-structural phase appearance and the speed or mobility at which they change. Atomic Force Microscopy (AFM) was utilized at different temperatures to investigate the phase separation behavior for four different types of bitumen and co-relate it with the Differential Scanning Calorimetry (DSC) measurements. Based on the experimental findings, it was concluded that the observed phase separation is mainly due to the wax/paraffin fraction presence in bitumen (Paper I). A hypothesis was developed of the appearance of a thin film at the specimen surface due to ageing which is creating a barrier, restricting thus the microstructures to float towards the surface. Furthermore, investigation showed that depending on the bitumen and exposure types this surface thin film is water soluble and thus the moisture damage becomes more severe with the ageing of asphalt pavement (Paper II and IV).A new empirical relation to obtain the primary structure coating thickness was established utilizing mixture volumetric properties and gradation using a large set of data from different literature sources. It was found that the enhanced morphological framework can be used to optimize the long term performance of asphalt mixtures (Paper III). Thereafter, the effect of diffusion controlled oxidative ageing on different mixture morphologies based on oxidative ageing mechanism of bitumen and diffusion-reaction process was investigated using the Finite Element Method (FEM). From the FE analyses, the effect of air-void distribution and their interconnectivity combined with the aggregate packing was shown to have a significant effect on age hardening (Paper IV).It was shown that focusing only on the percentage of air-void as the main predictive ageing parameter may lead to an erroneous conclusion and non-optimal predictions of long-term behavior. To replace such approaches, a new way to predict the long-term ageing was proposed in this Thesis, utilizing the found influences of mixture morphology and fundamental mechanism. Though additional mechanisms and non-linear coupling between them may be still needed to reach the ‘ultimate’ ageing prediction model, the current model was found to be a significant improvement to the currently used methods and may lead the way towards further enhancing the fundamental knowledge towards asphalt mixture ageing (Paper V).
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| 2. |
- Das, Prabir Kumar, 1982-, et al.
(författare)
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Evaluation of the low temperature cracking performance of asphalt mixtures utilizing HMA fracture mechanics
- 2013
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Ingår i: Construction and Building Materials. - : Elsevier. - 0950-0618 .- 1879-0526. ; 47, s. 594-600
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Tidskriftsartikel (refereegranskat)abstract
- In the present study, the low temperature cracking performance of asphalt mixture has been investigated numerically and experimentally. To do so, the HMA thermal fracture model has extended by including fracture energy threshold and non-linear thermal contraction coefficient. This extended model is capable to predict thermally induced stress and fracture temperature, which is validated with experimental results obtained from three different types of asphalt mixtures. From the parametric study, it was observed that understanding the influence of thermal contraction coefficient, the cooling rate and the creep compliance parameters can make a significant contribution to the material's sustainability. From the analysis, it was found that this extended model can be utilized to evaluate the low temperature cracking performance of asphalt mixtures and capable to provide correct ranking. Interestingly, non-linear thermal contraction coefficient gave much better prediction than linear approach.
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| 3. |
- Das, Prabir Kumar, 1982-
(författare)
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Thermally Induced Fracture Performance of Asphalt Mixtures
- 2012
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Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- A major distress mode in asphalt pavements is low temperature cracking, which results from the contraction and expansion of the asphalt pavement under extreme temperature changes. The potential for low temperature cracking is an interplay between the environment, the road structure and importantly the properties of the asphalt mixture. The thermal cracking performance of asphalt concrete mixtures can be evaluated by conducting thermal stress restrained specimen tests (TSRST) which is known to be correlated well with the fracture temperatures observed in the field. Although TSRST provides a good estimation of the field performance, it may be unrealistic to implement the obtained results in a design framework. On the other hand, recent studies showed Superpave indirect tension tests can be used to evaluate fracture performance (fatigue, moisture damage, low temperature cracking, etc.) of the asphalt concrete mixtures. In addition, the obtained elastic and viscoelastic parameters from the Superpave IDT tests can be used as an input parameter to establish a design framework. The study presented in this thesis has a main objective to develop a framework using Superpave IDT test results as input parameters in order to evaluate the low temperature cracking performance of asphalt concrete mixtures. Moreover, the study aims to investigate micro-mechanically the low temperature cracking behavior of bitumen using atomic force microscopy (AFM) as a tool.The numerical model has been developed by integrating fracture energy threshold into an asphalt concrete thermal fracture model, considering non-linear thermal contraction coefficients. Based on the asphalt concrete mixture viscoelastic properties, this integrated model can predict thermally induced stresses and fracture temperatures. The elastic, viscoelastic and fracture energy input parameters of the model were measured by conducting indirect tension tests and the thermal contraction coefficients were measured experimentally. The proposed model has been validated by comparing the predicted fracture temperatures with the results obtained from TSRST tests. It was found that, while there is a quantitative discrepancy, the predicted ranking was correct. In the measurement of the thermal contraction coefficients it was observed that the thermal contraction coefficient in asphalt concrete is non-linear in the temperature range of interest for low temperature cracking. The implications of having non-linear thermal contraction coefficient were investigated numerically.In an effort to understand the effect of bitumen properties on low temperature fatigue cracking, AFM was used to characterize the morphology of bitumen. The AFM topographic and phase contrast image confirmed the existence of bee-shaped microstructure and different phases. The bitumen samples were subjected to both environmental and mechanical loading and after loading, micro-cracks appeared in the interfaces of the bitumen surface, confirming bitumen itself may also crack. It was also found that the presence of wax and wax crystallization plays a vital role in low temperature cracking performance of bitumen.
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