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- Dini, Hoda, 1984-
(författare)
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As-cast AZ91D magnesium alloy properties : Effects of microstructure and temperature
- 2017
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Today, there is an essential need for lightweight, energy-efficient, environmentally benign engineering systems, and this is the driving force behind the development of a wide range of structural and functional materials for energy generation, energy storage, propulsion, and transportation. These challenges have motivated the use of magnesium alloys for lightweight structural systems. Magnesium has a density of 1.74 g/cm3, which is almost 30% less than that of aluminium, one quarter of steel, and almost identicalto polymers. The ease of recycling magnesium alloys as compared to polymers makes them environmentally attractive, but their poor mechanical performance is the primary reason for the limited adoption of these alloys for structural applications.The Mg-Al-Zn alloy AZ91D exhibits an excellent combination of strength, die-castability, and corrosion resistance. However, its mechanical performance with regard to creep strength, for example, at evaluated temperatures is poor. Moreover, very little is known about the correlation between its mechanical properties and microstructural features. This thesis aims to provide new knowledge regarding the role played by microstructure in the mechanical performance of the magnesium alloy. The properties/performance of the material in relation to process parameters became of great interest during the investigation.An exhaustive characterisation of the grain size, secondary dendrite arm spacing (SDAS) distribution, and fraction of Mg17Al12 was performed using optical and electron backscatter diffraction (EBSD). These microstructural parameters were correlated to the offset yield point (Rp0.2), fracture strength, and elongation to failure of the material. It was proposed that the intermetallic phase, Mg17Al12, plays an important role in determining the mechanical and physical properties of the alloy in a temperature range of room temperature to 190°C by forming a rigid network of intermetallic. The presence of this network was confirmed by studying the thermal expansion behaviour of samples of the alloy containing different amounts of Mg17Al12.A physically based constitutive model with a wide validity range was successfully adapted to describe the flow stress behaviour of AZ91D with various microstructures. The temperature-dependent variables of the model correlated quite well with the underlying physics of the material. The model was validated through comparison with dislocation densities obtained using EBSD.The influence of high-pressure die-cast parameters on the distortion and residual stress of the cast components was studied, as were distortion and residual stress in components after shot peening and painting. Interestingly, it was found that intensification pressure has a major effect on distortion and residual stresses, and that the temperature of the fixed half of the die had a slight influence on the component's distortion and residual stress.
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| 2. |
- Dini, Hoda, 1984-
(författare)
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As-cast AZ91D Magnesium Alloy Properties- Effect of Microstructure and Temperature
- 2015
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Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Magnesium and magnesium alloys are used in a wide variety of structural applications including automotive, aerospace, hand tools and electronic industries thanks to their light weight, high specific strength, adequate corrosion resistance and good castability. Al and Zn are the primary alloying elements in commercial Mg alloys and commonly used in automotive industries. AZ91 is one of the most popular Mg alloys containing 9% Al and 1% Zn. Hence, lots of research have been done during last decades on AZ91D. However, the existing data concerning mechanical properties and microstructural features showed large scatter and is even contradictory. This work focused on the correlation between the microstructure and the mechanical properties of as-cast AZ91 alloy. An exhaustive characterization of the grain size, secondary dendrite arm spacing (SDAS) distribution, and fraction of Mg17Al12 using optical and electron backscattered diffraction (EBSD) was performed. These microstructural parameters were correlated to offset yield point (Rp0.2), fracture strength and elongation to fracture. It was understood that the intermetallic phase, Mg17Al12, plays an important role in determining the mechanical and physical properties of the alloy at temperature range from room temperature up to 190oC. It was realized that by increasing the Mg17Al12 content above 11% a network of intermetallic may form. During deformation this rigid network should break before any plastic deformation happen. Hence, increase in Mg17Al12 content resulted in an increase in offset yield point. The presence of this network was supported by study of thermal expansion behaviour of the alloy containing different amount of Mg17Al12. A physically-based model was adapted and validated in order to predict the flow stress behaviour of as-cast AZ91D at room temperature up to 190ºC for various microstructures. The model was based on dislocation glide and climb in a single-phase (matrix) material containing reinforcing particles. The temperature dependant variables of the model were quite well correlated to the underlying physics of the material.
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| 3. |
- Dini, Hoda, 1984-, et al.
(författare)
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Effect of Process Parameters on Distortion and Residual Stress in High-Pressure Die Cast AZ91D Components After Clean Blasting and Painting
- 2021
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Ingår i: International Journal of metalcasting. - : Springer. - 1939-5981 .- 2163-3193. ; 15:1, s. 241-258
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Tidskriftsartikel (refereegranskat)abstract
- A high-pressure die-casting process was employed to produce AZ91D components. These cast components were exposed to three different post-treatments: (1) clean blasting, (2) clean blasting and painting, and (3) painting (without clean blasting). The influence of the process parameters first phase injection speed, temperature of fixed half of the die, cooling time, and intensification pressure on distortion and residual stress of the components after each post-treatment were investigated. The results showed that intensification pressure was the most significant factor among the four parameters.
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| 4. |
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| 5. |
- Dini, Hoda, 1984-, et al.
(författare)
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Effect of process parameters on distortion and residual stress of high-pressure die-cast AZ91D components
- 2018
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Ingår i: International Journal of metalcasting. - : Springer. - 1939-5981 .- 2163-3193. ; 12:3, s. 487-497
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Tidskriftsartikel (refereegranskat)abstract
- This paper presents a study of distortion and residual stress within a high-pressure die-cast AZ91D component, cast under different processing conditions. The influence of process parameters, i.e., die temperature, cooling time, intensification pressure and first-phase injection speeds, was examined. Distortions were measured using the in-house standard analog quality control fixture. Residual stress depth profiles were measured using a prism hole-drilling method. It was found that the most important process parameter affecting the distortion was intensification pressure and the second most important was temperature difference between the two die halves (fixed and moving side). Tensile residual stresses were found very near the surface. Increasing the intensification pressure resulted in an increased level of tensile residual stresses.
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| 6. |
- Dini, Hoda, 1984-, et al.
(författare)
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Effects of microstructure on deformation behaviour of AZ91D cast alloy
- 2014
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Ingår i: TMS 2014 Annual Meeting Supplemental Proceedings TMS, The Minerals, Metals & Materials Society, San Diego, February 16-20, 2014. - : John Wiley & Sons. - 9781118889725 ; , s. 565-572
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Konferensbidrag (refereegranskat)abstract
- The deformation behavior of AZ91D cast magnesium alloy was investigated using uniaxial tensile tests from room temperature up to 190°C and strain rates from 0.0001 up to 0.1 1/s. In present work gradient solidification in a Bridgeman furnace was employed to study the effect of initial microstructure on the tensile mechanical response of the AZ91D alloy. The furnace drawing rate was varied from minimum 0.3 to maximum 6 mm/s, which yielded a variation of SDAS from 4.2 up to 25 as well as a variation of the fraction of the γ -phase (Mg17Al12),. The effects of microstructural parameters such as SDAS and γ -phase morphology on the yield strength (YS), ultimate tensile strength (UTS) and hardening were investigated
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| 7. |
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| 8. |
- Dini, Hoda, 1984-, et al.
(författare)
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Optimization and validation of a dislocation density based constitutive model for as-cast Mg-9%Al-1%Zn
- 2018
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Ingår i: Materials Science & Engineering. - : Elsevier. - 0921-5093 .- 1873-4936. ; 710, s. 17-26
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Tidskriftsartikel (refereegranskat)abstract
- A dislocation density-based constitutive model, including effects of microstructure scale and temperature, was calibrated to predict flow stress of an as-cast AZ91D (Mg-9%Al-1%Zn) alloy. Tensile stress-strain data, for strain rates from 10-4 up to 10-1 s-1 and temperatures from room temperature up to 190 °C were used for model calibration. The used model accounts for the interaction of various microstructure features with dislocations and thereby on the plastic properties. It was shown that the Secondary Dendrite Arm Spacing (SDAS) size was appropriate as an initial characteristic microstructural scale input to the model. However, as strain increased the influence of subcells size and total dislocation density dominated the flow stress. The calibrated temperature-dependent parameters were validated through a correlation between microstructure and the physics of the deforming alloy. The model was validated by comparison with dislocation density obtained by using Electron Backscattered Diffraction (EBSD) technique.
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