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- Joffre, Thomas, 1987-, et al.
(författare)
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A 3D in-situ investigation of the deformation in compressive loading in the thickness direction of cellulose fiber mats
- 2015
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Ingår i: Cellulose. - : Springer Science and Business Media LLC. - 0969-0239 .- 1572-882X. ; 22:5, s. 2993-3001
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Tidskriftsartikel (refereegranskat)abstract
- Fiber mat materials based on cellulose natural fibers combines a useful set of properties, including renewability, stiffness, strength and dielectric insulation, etc. The dominant in-plane fiber orientation ensures the in-plane performance, at the expense of reduced out-of-plane behavior, which has not been studied as extensively as the in-plane behavior. Quantitative use of X-ray micro-computed tomography and strain analyses under in-situ loading open up possibilities to identify key mechanisms responsible for deformation. In the present investigation, focus is placed on the out-of-plane deformation under compressive loading of thick, high density paper, known as pressboard. The samples were compressed in the chamber of a microtomographic scanner. 3D images were captured before and after the loading the sample. From sequential 3D images, the strain field inside the material was calculated using digital volume correlation. Two different test pieces were tested, namely unpolished and surface polished ones. The first principal strain component of the strain tensor showed a significant correlation with the density variation in the material, in particular on the top and bottom surfaces of unpolished samples. The manufacturing-induced grooves generate inhomogeneities in the microstructure of the surface, thus creating high strain concentration zones which give a sensible contribution to the overall compliance of the unpolished material. More generally, the results reveal that, on the micrometer scale, high density fiber pressboard behaves as a porous material rather than a low density fiber network.
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| 3. |
- Joffre, Thomas, 1987-, et al.
(författare)
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Characterization of interfacial stress transfer ability in acetylation-treated wood fibre composites using X-ray microtomography
- 2017
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Ingår i: Industrial crops and products (Print). - : Elsevier BV. - 0926-6690 .- 1872-633X. ; 95, s. 43-49
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Tidskriftsartikel (refereegranskat)abstract
- The properties of the fibre/matrix interface contribute to stiffness, strength and fracture behaviour of fibre-reinforced composites. In cellulosic composites, the limited affinity between the hydrophilic fibres and the hydrophobic thermoplastic matrix remains a challenge, and the reinforcing capability of the fibres is hence not fully utilized. A direct characterisation of the stress transfer ability through pull-out tests on single fibres is extremely cumbersome due to the small dimension of the wood fibres. Here a novel approach is proposed: the length distribution of the fibres sticking out of the matrix at the fracture surface is approximated using X-ray microtomography and is used as an estimate of the adhesion between the fibres and the matrix. When a crack grows in the material, the fibres will either break or be pulled-out of the matrix depending on their adhesion to the matrix: good adhesion between the fibres and the matrix should result in more fibre breakage and less pull-out of the fibres than poor adhesion. The effect of acetylation on the adhesion between the wood fibres and the PLA matrix was evaluated at different moisture contents using the proposed method. By using an acetylation treatment of the fibres it was possible to improve the strength of the composite samples soaked in the water by more than 30%.
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| 4. |
- Joffre, Thomas, 1987-
(författare)
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Structure and Mechanical Behaviour of Wood-Fibre Composites
- 2014
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Wood fibres have several advantages compared to man-made synthetic fibres: they have high specific stiffness, are renewable, relatively inexpensive, available in industrial quantities and biodegradable. However, to increase and diversify their utilisation, it is necessary to increase the understanding on what controls their mechanical properties.In this work, the hygroelastic behaviour of isolated wood fibres has been investigated using an analytical model and a finite element model based on three dimensional images obtained using synchrotron-based X-ray micro-computed tomography. It was thus possible to show how the cell wall responds to a mechanical load or a change in ambient relative humidity.The wood fibres were then mixed with a biopolymer aiming to produce a cost-efficient, 100% renewable composite material. The microstructure of the produced composites has been characterised using X-ray microtomography and digital image processing. It was for instance possible to measure the moisture-induced swelling of fibres embedded in a polymeric matrix. The experimental results have then been successfully compared with prediction obtained with a finite element model. The length of the fibres inside the composite has also been measured from three dimensional images, aiming to understand how each step of the processing chain is affecting the degradation of the aspect ratio of the reinforcing fibres.The presence of defects inside the composite has also been quantified using X-ray microtomography. The effects of the defects on the tensile strength have been predicted using an analytical model. The results have been compared with the measured tensile strength on each sample, showing that the size and orientation of the critical defect controls the tensile strength of the material.Finally, wood-fibre mats without any matrix material were compressed in the chamber of a microtomographic scanner. Sequential images were taken during the test. Using digital volume correlation, it was possible to calculate the local strain field inside the material. The effects of heterogeneities on the strain field have then been investigated. The applied compressive load resulted in transport of material from high to low density regions.
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| 6. |
- Tummala, Gopi Krishna, 1986-, et al.
(författare)
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Strain-induced stiffening of nanocellulose-reinforced poly(vinyl alcohol) hydrogels mimicking collagenous soft tissues
- 2017
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Ingår i: Soft Matter. - : Royal Society of Chemistry (RSC). - 1744-683X .- 1744-6848. ; 13:21, s. 3936-3945
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Tidskriftsartikel (refereegranskat)abstract
- Soft tissues possess remarkable mechanical strength for their high water content, which is hard to mimic in synthetic materials. Here, we demonstrate how strain-induced stiffening in hydrogels plays a major role in mimicking the mechanical properties of collagenous soft tissues. In particular, nanocellulose reinforced polyvinyl alcohol (PVA) hydrogels of exceptionally high water content (90-93 wt%) are shown to exhibit collagen-like mechanical behavior typical for soft tissues. High water content and co-existence of both soft and rigid domains in the gel network are the main factors responsible for strain-induced stiffening. This observed effect due to the alignment of rigid components of the hydrogel is simulated through modeling and visualized through strain-induced birefringence experiments. Design parameters such as nanocellulose aspect ratio and solvent composition are also shown to be important to control the mechanical properties. In addition, owing to their transparency (90-95% at 550 nm) and hyperelastic properties (250-350% strain), the described hydrogels are promising materials for biomedical applications, especially in ophthalmology.
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| 7. |
- Wu, Dan, 1990-, et al.
(författare)
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A combined experimental and numerical method to estimate the elastic modulus of single trabeculae
- 2022
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Ingår i: Journal of The Mechanical Behavior of Biomedical Materials. - : Elsevier. - 1751-6161 .- 1878-0180. ; 125
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Tidskriftsartikel (refereegranskat)abstract
- The elastic modulus at the single trabecular level is an important parameter for the understanding of the mechanical behavior of trabecular bone. Current methods are commonly limited by the irregular trabecular shape and the accuracy of displacement measurement. The aim of this study was to propose a method to estimate the trabecular modulus overcoming some of these limitations. For high-precision displacement measurements, insitu compression within a synchrotron radiation based X-ray tomograph was used. Trabecular displacements were subsequently estimated by a global digital volume correlation algorithm, followed by high-resolution finite element analyses to account for the irregular geometry. The trabecular elastic moduli were then estimated by comparing the loads from the finite element analyses with those of the experiments. With this strategy, the average elastic modulus was estimated to 3.83 +/- 0.54 GPa for three human trabeculae samples. Though limited by the sample size, the demonstrated method shows a potential to estimate the mechanical properties at the single trabecular level.
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