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| 2. |
- Poley, L., et al.
(author)
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The ABC130 barrel module prototyping programme for the ATLAS strip tracker
- 2020
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In: Journal of Instrumentation. - : IOP PUBLISHING LTD. - 1748-0221 .- 1748-0221. ; 15:9
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Journal article (peer-reviewed)abstract
- For the Phase-II Upgrade of the ATLAS Detector [1], its Inner Detector, consisting of silicon pixel, silicon strip and transition radiation sub-detectors, will be replaced with an all new 100% silicon tracker, composed of a pixel tracker at inner radii and a strip tracker at outer radii. The future ATLAS strip tracker will include 11,000 silicon sensor modules in the central region (barrel) and 7,000 modules in the forward region (end-caps), which are foreseen to be constructed over a period of 3.5 years. The construction of each module consists of a series of assembly and quality control steps, which were engineered to be identical for all production sites. In order to develop the tooling and procedures for assembly and testing of these modules, two series of major prototyping programs were conducted: an early program using readout chips designed using a 250 nm fabrication process (ABCN-250) [2, 3] and a subsequent program using a follow-up chip set made using 130 nm processing (ABC130 and HCC130 chips). This second generation of readout chips was used for an extensive prototyping program that produced around 100 barrel-type modules and contributed significantly to the development of the final module layout. This paper gives an overview of the components used in ABC130 barrel modules, their assembly procedure and findings resulting from their tests.
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| 3. |
- Elg, Alf Peter, et al.
(author)
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Research project EMPIR 19ENG02 future energy
- 2020
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In: VDE High Voltage Technology 2020. - : VDE Verlag GmbH. - 9783800753550 ; , s. 252-257
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Conference paper (peer-reviewed)abstract
- Society's increasing demand for electrical energy, along with the increased integration of remote renewable generation has driven transmission levels to ever higher voltages in order to maintain (or improve) grid efficiency. Consequently, high voltage testing and monitoring beyond voltage levels covered by presently available metrology infrastructures are needed to secure availability and quality of supply. Calibration services for Ultra-High Voltage Direct Current (UHVDC) presently are only available up to 1000 kV. There is a need to extend the DC calibration capabilities for voltage instrument transformers up to 1200 kV and for factory component testing capabilities up to 2000 kV. Also, methods for linear extension of lightning impulse calibration, for dielectric testing of UHV grid equipment, urgently need revision. Recent research has raised questions regarding the validity of the current linearity extension methods for voltages beyond 2500 kV. Furthermore, new methods for calibration are needed for the 0.2 class HVAC voltage instrument transformers for system voltages up to 1200 kV. The current methods used for determination of the voltage dependence are very time consuming, raising the need for methods allowing faster assessment. Finally, with new HVDC transmission grids and associated components, novel methods are needed for detection, classification and localisation of partial discharge (PD) under DC stress. The industry needs methods for reliable monitoring of critical components such as cables, for both HVAC and HVDC, and gas insulated substations (GIS), and techniques for addressing new challenges introduced by HVDC technologies, such as the ability to distinguish PD signals from switching transients in converters and other sources of noise.
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| 4. |
- Pascanu, Vlad, et al.
(author)
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Double-Supported Silica-Metal-Organic Framework Palladium Nanocatalyst for the Aerobic Oxidation of Alcohols under Batch and Continuous Flow Regimes
- 2015
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In: ACS Catalysis. - : American Chemical Society (ACS). - 2155-5435 .- 2155-5435. ; 5:2, s. 472-479
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Journal article (peer-reviewed)abstract
- Stable and easily synthesized metal-organic framework MIL-88B-NH2 represents an attractive support for catalysts employed in oxidation reactions, which are typically performed under relatively harsh conditions. However, MIL-88B-NH2, the thermodynamic polymorph of the more popular MIL-101-NH2, has been rarely employed in catalytic applications because of a difficult impregnation process caused by the flexible nature of the framework. We report herein a new catalyst denoted Pd@MIL-88B-NH2 (8 wt % Pd), the first example of metallic nanoparticles successfully impregnated in the pores of MIL-88B-NH2. Furthermore, by enclosing the MOF crystals in a tailored protective coating of SiO2 nanoparticles, an even more enduring material was developed and applied to the aerobic oxidation of benzylic alcohols. This doubly supported catalyst Pd@MIL-88B-NH2@nano-SiO2 displayed high activity and excellent performance in terms of endurance and leaching control. Under batch conditions, a very convenient and efficient recycling protocol is illustrated, using a teabag approach. Under continuous flow, the catalyst was capable of withstanding 7 days of continuous operation at 110 degrees C without deactivation. During this time, no leaching of metallic species was observed, and the material maintained its structural integrity.
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| 5. |
- Pascanu, Vlad, et al.
(author)
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Highly Functionalized Biaryls via Suzuki-Miyaura Cross-Coupling Catalyzed by Pd@MOF under Batch and Continuous Flow Regimes
- 2015
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In: ChemSusChem. - : Wiley. - 1864-5631 .- 1864-564X. ; 8:1, s. 123-130
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Journal article (peer-reviewed)abstract
- A diverse set of more than 40 highly functionalized biaryls was synthesized successfully through the Suzuki-Miyaura cross-coupling reaction catalyzed by Pd nanoparticles supported in a functionalized mesoporous MOF (8 wt% Pd@MIL-101(Cr)-NH2). This could be achieved under some of the mildest conditions reported to date and a strong control over the leaching of metallic species could be maintained, despite the presence of diverse functional groups and/or several heteroatoms. Some of the targeted molecules are important intermediates in the synthesis of pharmaceuticals and we clearly exemplify the versatility of this catalytic system, which affords better yields than currently existing commercial procedures. Most importantly, Pd@MIL-101-NH2 was packed in a micro-flow reactor, which represents the first report of metallic nanoparticles supported on MOFs employed in flow chemistry for catalytic applications. A small library of 11 isolated compounds was created in a continuous experiment without replacing the catalyst, demonstrating the potential of the catalyst for large-scale applications.
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