| 1. |
- Chen, Zhe, et al.
(författare)
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Nano-scale characterization of white layer in broached Inconel 718
- 2017
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Ingår i: Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing. - Amsterdam : Elsevier BV. - 0921-5093 .- 1873-4936. ; 684, s. 373-384
-
Tidskriftsartikel (refereegranskat)abstract
- The formation mechanism of white layers during broaching and their mechanical properties are not well investigated and understood to date. In the present study, multiple advanced characterization techniques with nano-scale resolution, including transmission electron microscopy (TEM), transmission Kikuchi diffraction (TKD), atom probe tomography (APT) as well as nano-indentation, have been used to systematically examine the microstructural evolution and corresponding mechanical properties of a surface white layer formed when broaching the nickel-based superalloy Inconel 718.TEM observations showed that the broached white layer consists of nano-sized grains, mostly in the range of 20–50 nm. The crystallographic texture detected by TKD further revealed that the refined microstructure is primarily caused by strong shear deformation. Co-located Al-rich and Nb-rich fine clusters have been identified by APT, which are most likely to be γ′ and γ′′ clusters in a form of co-precipitates, where the clusters showed elongated and aligned appearance associated with the severe shearing history. The microstructural characteristics and crystallography of the broached white layer suggest that it was essentially formed by adiabatic shear localization in which the dominant metallurgical process is rotational dynamic recrystallization based on mechanically-driven subgrain rotations. The grain refinement within the white layer led to an increase of the surface nano-hardness by 14% and a reduction in elastic modulus by nearly 10% compared to that of the bulk material. This is primarily due to the greatly increased volume fraction of grain boundaries, when the grain size was reduced down to the nanoscale.
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| 2. |
- Grolig, Jan Gustav, 1986
(författare)
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Coated Ferritic Stainless Steels as Interconnects in Solid Oxide Fuel Cells - Material Development and Electrical Properties
- 2015
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Solid oxide fuel cells (SOFCs) are attracting increasing interest as devices with potentialuses in decentralized and clean electricity and heat production. Several challengeswith respect to materials have to be overcome to achieve efficiencies and life-spansthat are sufficient for long-term applications.An important element of an SOFC stack is the interconnect component, which connectstwo adjacent fuel cell elements. Interconnects, which are commonly composedof ferritic stainless steels, have to be corrosion-resistant, mechanically stable and costoptimized.This work aimed to investigate economic solutions for interconnect materials and tounderstand the underlying mechanisms of degradation and electrical conduction ofthese materials. Mainly two substrates, a commercially available steel (AISI 441) anda ferritic stainless steel that was optimized for an SOFC application (Sandvik SanergyHT) were combined with different barrier coatings and exposed to a cathode-sideatmosphere. A method was developed that allows for the electrical characterizationof promising material systems and model alloys, thereby facilitating a fundamentalunderstanding of the dominant electrical conduction processes linked to the oxidescales that grow on interconnects. The AISI 441 steel coated with reactive elementsand cobalt showed good corrosion and chromium evaporation profiles, while AISI 441coated with cerium and cobalt also had promising electrical properties. The SanergyHT steel was examined with coatings of copper and iron and copper and manganese,respectively. The corrosion and chromium evaporation profiles of Sanergy HT wereimproved by coating with copper and iron. The copper and iron-coated Sanergy HTshowed lower area specific resistance values than cobalt-coated Sanergy HT. Chromia,which is the main constituent of oxide scales, was synthesized using differentmethods. The electrical properties of chromia were found to be sensitive to not onlyimpurities, but also heat treatment. Finally the electrical properties of cobalt- andcobalt cerium-coated Sanergy HT steels were investigated. It was revealed that theaddition of cerium improved the conductivity of the interconnect by both slowingdown chromia growth and preventing the outward diffusion of iron into the spinel.
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| 3. |
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| 4. |
- Stolen, Reidar, et al.
(författare)
-
Solcelleteknologi og brannsikkerhet
- 2018
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Rapport (övrigt vetenskapligt/konstnärligt)abstract
- Bruken av solcelleteknologi er i stor vekst i Norge. I denne studien er branntekniske utfordringer ved bruk av solcelleteknologi undersøkt, med hensyn på brannstart, brannspredning og brannslokking. Studien danner et kunnskapsgrunnlag for å ivareta brannsikkerheten under montering, drift og under slokkeinnsats, samt for å utforme et enhetlig og tydelig regelverk. Resultatene fra studien viser:Brannstart: Solcelleinstallasjoner inneholder mange koblingspunkt, som kan være potensielle tennkilder, og en liten mengde brennbare materialer. Dermed er det som trengs til stede for å starte en brann. Det er viktig at alle kontaktpunkter i solcelleinstallasjonen er robuste og tåler den påkjenningen de blir utsatt for gjennom sin levetid uten at det oppstår dårlig kontakt som kan føre til brann.Brannspredning: For utenpåmonterte solcellemoduler er det ofte en åpen luftspalte mellom modul og bygning. Dersom det er en brann i denne luftspalten, vil varmen kunne bli akkumulert, noe som kan føre til raskere og større brannspredning enn om bygningsoverflaten ikke hadde vært tildekket. I fullskalaforsøk med solcellemoduler montert på tak spredte brannen seg under hele arealet som var dekket av moduler, men stoppet da den nærmet seg kanten av dette arealet. Dette illustrerer viktigheten av at områder med solceller utenpå en bygning blir seksjonert for å unngå brannspredning. Eventuelt kan det benyttes mindre brennbare materialer på taket under solcellemodulene for å motvirke den økte varmepåkjenningen som solcellemodulene gir. Luftspalten mellom modul og bygning kan potensielt også gi endringer i luftstrømningen langs bygget, som igjen kan påvirke brannspredningen.Brannslokking: Brannvesenet har behov for informasjon om det er solcelleinstallasjon i bygget og hvilke deler av det elektriske anlegget som kan være spenningssatt. Under slokkeinnsats må brannvesenet ta hensyn til berøringsfare, og fare for at det kan oppstå lysbuer og andre feil som kan føre til nye antennelsespunkt. Ferskvann kan brukes som slokkemiddel, dette må spyles fra minimum 1 meters avstand med spredt stråle og minimum 5 meters avstand med samlet stråle. Solcellemoduler kan komplisere brannslokking ved at de danner en fysisk barriere mellom brannvesenet og brannen, samt fordi det må tas hensyn til plassering av spenningssatte komponenter. Når disse punktene er tatt høyde for, bør ikke utenpåmonterte solcelleinstallasjoner være et problem.Videre arbeid: For utenpåmonterte solcelleinstallasjoner, er det lite forskning på vertikal montering (på fasader), og hvordan en eventuell endret branndynamikk kan påvirke brannspredning og slokking. Videre er det i dag økende bruk av bygningsintegrerte solcelleinstallasjoner, noe som gir mange mulige nye utfordringer for brannsikkerheten og for regelverk, ettersom solcellen da er en del av bygningskroppen, samtidig som den er en elektrisk komponent. Tysk statistikk tyder på at brannrisiko for slike installasjoner kan være større enn for utenpåmonterte solcelleinstallasjoner, og dette vil det derfor være viktig å undersøke nærmere.
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| 5. |
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| 6. |
- Skagestad, Ragnhild, 1978, et al.
(författare)
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GCCSI Webinar: Cutting Cost of CO2 Capture in Process Industry (CO2stCap) Project overview & first results for partial CO2 capture at integrated steelworks
- 2017
-
Annan publikation (övrigt vetenskapligt/konstnärligt)abstract
- GCCSI Webinar: Cutting Cost of CO2 Capture in Process Industry (CO2stCap) Project overview & first results for partial CO2 capture at integrated steelworks This publication has the format of a webinar: The CO2StCap project is a four year initiative carried out by industry and academic partners with the aim of reducing capture costs from CO2 intensive industries (more information here). The project, led by Tel-Tek, is based on the idea that cost reduction is possible by capturing only a share of the CO2 emissions from a given facility, instead of striving for maximized capture rates. This can be done in multiple ways, for instance by capturing only from the largest CO2 sources at individual multi-stack sites utilising cheap waste heat or adapting the capture volumes to seasonal changes in operations. The main focus of this research is to perform techno-economic analyses for multiple partial CO2 capture concepts in order to identify economic optimums between cost and volumes captured. In total for four different case studies are developed for cement, iron & steel, pulp & paper and ferroalloys industries. The first part of the webinar gave an overview of the project with insights into the cost estimation method used. The second part presented the iron & steel industry case study based on the Lulea site in Sweden, for which waste-heat mapping methodology has been used to assess the potential for partial capture via MEA-absorption. Capture costs for different CO2 sources were discussed, demonstrating the viability of partial capture in an integrated steelworks.
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| 7. |
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| 8. |
- Hosseini Bab Anari, Elham, 1982, et al.
(författare)
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Fluorine-free salts for aqueous lithium-ion and sodium-ion battery electrolytes
- 2016
-
Ingår i: RSC Advances. - : Royal Society of Chemistry (RSC). - 2046-2069. ; 6:88, s. 6, 85194-85201
-
Tidskriftsartikel (refereegranskat)abstract
- A first generation of fluorine-free lithium and sodium salts based on the concept of pseudo-delocalized anions has been synthesized with both high purity and yield using water as the solvent in the reaction medium. The salts have been fully characterized by Raman and FT-IR spectroscopies, thermogravimetry, and X-ray crystallography to reveal both basic properties in terms of thermal stability and solubility as well as the local, mainly ion–ion interaction dictated, coordination details and by ionic conductivity and electrochemical stability window measurements as aqueous electrolytes. Together a picture is created of the salts' promise as components in electrolytes – primarily aiming at application in low voltage fluorinefree aqueous lithium-ion batteries (LIBs) and sodium-ion batteries (SIBs).
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| 9. |
- Heshmati, Mohsen, 1987, et al.
(författare)
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On the strength prediction of adhesively bonded FRP-steel joints using cohesive zone modelling
- 2018
-
Ingår i: Theoretical and applied fracture mechanics (Print). - : Elsevier BV. - 0167-8442 .- 1872-7638. ; 93, s. 64-78
-
Tidskriftsartikel (refereegranskat)abstract
- The variety of failure modes that are likely to occur in fibre-reinforced polymer (FRP)/steel joints used in the construction industry adds to the complexity associated with the design of these joints. This variation in possible failure modes is mainly attributed to the lack of a controlled application environment and to rather insufficient quality assurance protocols and procedures. The use of energy-based methods such as, cohesive zone modelling (CZM), can be a solution to circumvent such complexities. This paper investigates a number of issues related to CZM analyses of FRP/steel adhesive joints using various test configurations and a comprehensive numerical study. Parameters such as the effect of shape and type of cohesive law, crack path location, length of damage process zone, variations of adhesive and FRP properties, and different failure modes including cohesive, interfacial debonding and FRP failure on the strength of joints are investigated. The results show that the behaviour of the tested joints is accurately predicted provided that the variation of failure modes are taken into account. Moreover, it is shown that the damage process zone in adhesive layer is directly proportional to the shape of cohesive laws. This feature can be employed in the design phase to ensure sufficient overlap length and to account for important in-service parameters such as temperature and moisture.
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| 10. |
- Lei, Yu, et al.
(författare)
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Graphene and Beyond: Recent Advances in Two-Dimensional Materials Synthesis, Properties, and Devices
- 2022
-
Ingår i: ACS Nanoscience Au. - : American Chemical Society (ACS). - 2694-2496. ; 2:6, s. 450-485
-
Forskningsöversikt (refereegranskat)abstract
- Since the isolation of graphene in 2004, two-dimensional (2D) materials research has rapidly evolved into an entire subdiscipline in the physical sciences with a wide range of emergent applications. The unique 2D structure offers an open canvas to tailor and functionalize 2D materials through layer number, defects, morphology, moiré pattern, strain, and other control knobs. Through this review, we aim to highlight the most recent discoveries in the following topics: theory-guided synthesis for enhanced control of 2D morphologies, quality, yield, as well as insights toward novel 2D materials; defect engineering to control and understand the role of various defects, including in situ and ex situ methods; and properties and applications that are related to moiré engineering, strain engineering, and artificial intelligence. Finally, we also provide our perspective on the challenges and opportunities in this fascinating field.
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| 11. |
- Vilardell, A. M., et al.
(författare)
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B2-structured Fe3Al alloy manufactured by laser powder bed fusion : Processing, microstructure and mechanical performance
- 2023
-
Ingår i: Intermetallics (Barking). - : Elsevier. - 0966-9795 .- 1879-0216. ; 156
-
Tidskriftsartikel (refereegranskat)abstract
- Prealloyed Fe3Al was successfully manufactured by laser powder bed fusion. The best set of process parameters led to parts with a relative density of 99.5 %, a surface roughness, Sa, of 31.5 ± 5.6 μm and a hardness of 319 ± 14 HV0.1. Its microstructure as well as its mechanical properties at room and high temperatures were analyzed. The results of the chemical composition showed minor variations in aluminum content oscillating between 21 and 28 at.% along the melt pool. Additionally, elongated grains were observed to grow parallel to the building direction, as well as the development of a weak 001 texture along the building direction. The mechanical properties were influenced by the temperature. Compression tests showed a loss in strength with the increase in temperature, from a yield strength of 621 ± 40 MPa at room temperature to 89 ± 20 MPa at 650 °C. Reciprocating sliding wear tests showed that fragmentation of the intermetallic at room temperature occurs, whereas plastic deformation dominated at higher temperatures. For all temperatures, tribochemical wear was also present due to the oxidation of wear debris.
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| 12. |
- Wärmefjord, Kristina, 1976, et al.
(författare)
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Welding of non-nominal geometries : physical tests
- 2016
-
Ingår i: Procedia CIRP. - : Elsevier BV. - 2212-8271 .- 2212-8271. ; 43, s. 136-141
-
Tidskriftsartikel (refereegranskat)abstract
- The geometrical quality of a welded assembly is to some extent depending part positions before welding. Here, a design of experiment is set up in order to investigate this relation using physical tests in a controlled environment. Based on the experimental results it can be concluded that the influence of part position before welding is significant for geometrical deviation after welding. Furthermore, a working procedure for a completely virtual geometry assurance process for welded assemblies is outlined. In this process, part variations, assembly fixture variations and welding induced variations are important inputs when predicting the capability of the final assembly.
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| 13. |
-
INNOTRACK: Concluding technical report
- 2010
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Samlingsverk (redaktörskap) (refereegranskat)abstract
- The track structure, rails, switches and crossings account for more than 50% of maintenance and renewal costs for the rail industry. To improve the competitiveness of rail transportation, the cost-efficiency of these areas needs to be addressed.This the background to INNOTRACK, an integrated research project funded by the European Commission’s 6th research framework pro- gramme. Running from September 2006 to December 2009, INN- OTRACK has developed a multitude of innovative solutions in the areas of track substructure, rails & welds, and switches & crossings. The solutions have been assessed from technical, logistics and life cycle cost point of views.This Concluding Technical Report of INNOTRACK includes an overview of the project. It further details implementable results, and clusters them into ”highlight” areas. In addition, the book acts as a ”key” to the vast amount of information from INNOTRACK: All sections refer to project reports where more information can be found.
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| 14. |
- Mahade, Satyapal, 1987-, et al.
(författare)
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Incorporation of graphene nano platelets in suspension plasma sprayed alumina coatings for improved tribological properties
- 2021
-
Ingår i: Applied Surface Science. - : Elsevier BV. - 0169-4332 .- 1873-5584. ; 570
-
Tidskriftsartikel (refereegranskat)abstract
- Graphene possesses high fracture toughness and excellent lubrication properties, which can be exploited to enhance tribological performance of coating systems utilized to combat wear. In this work, suspension plasma spray (SPS) process was employed to deposit a composite, graphene nano-platelets (GNP) incorporated alumina coating. For comparison, monolithic alumina was also deposited utilizing identical spray conditions. The as-deposited coatings were characterized in detail for their microstructure, porosity content, hardness, fracture toughness and phase composition. Raman analysis of the as-deposited composite coating confirmed retention of GNP. The composite coating also showed good microstructural integrity, comparable porosity, higher fracture toughness and similar alumina phase composition as the monolithic alumina coating. The as-deposited coatings were subjected to dry sliding wear tests. The GNP incorporated composite coating showed lower CoF and lower specific wear rate than the pure alumina coating. Additionally, the counter surface also showed a lower wear rate in case of the composite coating. Post-wear analysis performed by SEM/EDS showed differences in the coating wear track and in the ball wear track of monolithic and composite coatings. Furthermore, Raman analysis in the wear track of composite coating confirmed the presence of GNP. The micro-indentation and wear test results indicate that the presence of GNP in the composite coating aided in improving fracture toughness, lowering CoF and specific wear rate compared to the monolithic coating. Results from this work demonstrated retention of GNP in an SPS processed coating, which can be further exploited to design superior wear-resistant coatings.
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| 15. |
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| 16. |
- Eivazihollagh, Alireza, et al.
(författare)
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On chelating surfactants : Molecular perspectives and application prospects
- 2019
-
Ingår i: Journal of Molecular Liquids. - : Elsevier BV. - 0167-7322 .- 1873-3166. ; 278, s. 688-705
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Tidskriftsartikel (refereegranskat)abstract
- Chelating agents, molecules that very strongly coordinates certain metal ions, are used industrially as well as in consumer products to minimize disturbances and increase performance of reactions and applications. The widely used sequestering agents, nitrilotriacetic acid (NTA), ethylenediaminetetraacetic acid (EDTA) and diethylenetriaminepentaacetic acid (DTPA) belong to this branch of readily water-soluble compounds. When these chemical structures also have hydrophobic parts, they are prone to adsorb at air-water interfaces and to self-assemble. Such bifunctional molecules can be called chelating surfactants and will have more extended utilization prospects than common chelating agents or ordinary ionic surfactants. The present review attempts to highlight the fundamental behavior of chelating surfactants in solution and at interfaces, and their very specific interactions with metal ions. Methods to recover chelating surfactants from metal chelates are also described. Moreover, utilization of chelating surfactants in applications for metal removal in environmental engineering and mineral processing, as well as for metal control in the fields of biology, chemistry and physics, is exemplified and discussed.
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| 17. |
- Goel, Sneha, 1993-, et al.
(författare)
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The Effect of Location and Post-treatment on the Microstructure of EBM-Built Alloy 718
- 2018
-
Ingår i: Proceedings of the 9th International Symposium on Superalloy 718 & Derivatives. - Cham : Springer. - 2367-1696 .- 2367-1181. - 9783319894799 - 9783319894805 ; , s. 115-129
-
Konferensbidrag (refereegranskat)abstract
- Additive manufacturing (AM) of Ni-based superalloys such as Alloy 718 may obviate the need for difficult machining and welding operations associated with geometrically intricate parts, thus potentially expanding design possibilities and facilitating cost-effective manufacture of complex components. However, processing AM builds completely free from defects, which may impair mechanical properties such as fatigue and ductility, is challenging. Anisotropic properties, microstructural heterogeneities and local formation of undesired phases are additional concerns that have motivated post-treatment of AM builds. This work investigates the microstructural changes associated with post-treatment of Alloy 718 specimens produced by Electron Beam Melting (EBM) for as-built microstructures at 3 build heights: near base plate, in the middle of build and near the top of the build. Two different post-treatment conditions, hot isostatic pressing (HIP) alone and a combined HIP with solutionising and two-step aging were examined and compared to the results for the as-built condition. The influence of various post-treatments on minor phase distributions (δ, γ″, carbides), overall porosity, longitudinal grain widths and Vickers microhardness was considered. The HIP treatment led to significant reduction in overall porosity and dissolution of δ phase, which led to appreciable grain growth for both post-treatment conditions. The variation in hardness noted as a function of build height for the as-built specimens was eliminated after post-treatment. Overall, the hardness was found to decrease after HIP and increase after the full HIP, solutionising and aging treatment, which was attributed to dissolution of γ″ during HIP and its re-precipitation in subsequent heat treatment steps.
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| 18. |
- Karimi Neghlani, Paria, 1986-, et al.
(författare)
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Influence of successive thermal cycling on microstructure evolution of EBM-manufactured alloy 718 in track-by-track and layer-by-layer design
- 2018
-
Ingår i: Materials & design. - : Elsevier BV. - 0264-1275 .- 1873-4197. ; 160, s. 427-441
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Tidskriftsartikel (refereegranskat)abstract
- Successive thermal cycling (STC) during multi-track and multi-layer manufacturing of Alloy 718 using electron beam melting (EBM) process leads to a microstructure with a high degree of complexity. In the present study, a detailed microstructural study of EBM-manufactured Alloy 718 was conducted by producing samples in shapes from one single track and single wall to 3D samples with maximum 10 longitudinal tracks and 50 vertical layers. The relationship between STC, solidification microstructure, interdendritic segregation, phase precipitation (MC, δ-phase), and hardness was investigated. Cooling rates (liquid-to-solid and solid-to-solid state) was estimated by measuring primary dendrite arm spacing (PDAS) and showed an increased cooling rate at the bottom compared to the top of the multi-layer samples. Thus, microstructure gradient was identified along the build direction. Moreover, extensive formation of solidification micro-constituents including MC-type carbides, induced by micro-segregation, was observed in all the samples. The electron backscatter diffraction (EBSD) technique showed a high textured structure in 〈001〉 direction with a few grains misoriented at the surface of all samples. Finer microstructure and possibility of more γ″ phase precipitation at the bottom of the samples resulted in slightly higher (~11%) hardness values compared to top of the samples.
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| 19. |
- Esmaeili, Ali, 1983, et al.
(författare)
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Modelling of temperature and strain rate dependent behaviour of pearlitic steel in block braked railway wheels
- 2021
-
Ingår i: Railway Engineering Science. - : Springer. - 2662-4745 .- 2662-4753. ; 29:4, s. 362-378
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Tidskriftsartikel (refereegranskat)abstract
- Block braked railway wheels are subjected to thermal and rolling contact loading. The thermal loading results in high temperatures and thermal stresses which cause slow time dependent processes such as creep, relaxation and static recovery of the wheel material. At the same time, the rolling contact loading implies a very fast mechanical load application. This paper is focused on material modeling of pearlitic steel for a wide range of loading rates at elevated temperatures. The starting point is a viscoplasticity model including nonlinear isotropic and kinematic hardening. The Delobelle overstress function is employed to capture strain rate dependent response of the material. The model also includes static recovery of the hardening to capture slower viscous (diffusion dominated) behaviour of the material. Experiments for the pearlitic wheel steel ER7 in terms of cyclic strain-controlled uniaxial tests with hold-time, uniaxial ratchetting tests including rapid cycles and biaxial cyclic tests with tension/compression and torsion are used to calibrate the material model. These experiments were performed under isothermal conditions at different temperatures. In the ratchetting tests, higher loading rates are obtained and these have been used to calibrate the high strain rate response of the viscoplasticity model. The paper is concluded with a numerical example of a block braked wheel where the importance of accounting for the viscoplasticity in modelling is highlighted.
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| 20. |
- Hedström, Peter, et al.
(författare)
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Load partitioning between single bulk grains in a two-phase duplex stainless steel during tensile loading
- 2010
-
Ingår i: Acta Materialia. - : Elsevier BV. - 1359-6454 .- 1873-2453. ; 58:2, s. 734-744
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Tidskriftsartikel (refereegranskat)abstract
- The lattice strain tensor evolution for single bulk grains of austenite and ferrite in a duplex stainless steel during tensile loading to 0.02 applied strain has been investigated using in situ high-energy X-ray measurements and finite-element modeling. Single-grain X-ray diffraction lattice strain data for the eight austenite and seven ferrite grains measured show a large variation of residual lattice strains, which evolves upon deformation to the point where some grains with comparable crystallographic orientations have lattice strains different by 1.5 x 10(-3), corresponding to a stress of similar to 300 MPa. The finite-element simulations of the 15 measured grains in three different spatial arrangements confirmed the complex deformation constraint and importance of local grain environment.
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| 21. |
- Dimitrios, Nikas, et al.
(författare)
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Effect of annealing on microstructure in railway wheel steel
- 2022
-
Ingår i: 42Nd Riso International Symposium On Materials Science. - : Institute of Physics Publishing (IOPP). ; 1249
-
Konferensbidrag (refereegranskat)abstract
- Railway wheels are commonly made from medium carbon steels (similar to 0.55 wt.% C), heat treated to a near pearlitic microstructure with 5-10% pro-eutectoid ferrite. During the operation of freight trains, where block brakes are used, high thermal loads occur together with the high contact stresses, which combined can affect the mechanical properties of the material. In this study, the effects of annealing on local microstructure and mechanical properties in pearlitic railway wheel steel were investigated using electron microscopy and micro-hardness. It is found that after annealing at 650 degrees C, the room temperature hardness reduces about 25%, accompanied by significant spheroidization of cementite in the pearlitic colonies, though the size and the orientation gradients of the pearlitic colonies have not changed much. The relationship between the microstructural changes and the mechanical properties are discussed.
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| 22. |
- Jeong, Seung Hee, 1978-
(författare)
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Soft Intelligence : Liquids Matter in Compliant Microsystems
- 2016
-
Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Soft matter, here, liquids and polymers, have adaptability to a surrounding geometry. They intrinsically have advantageous characteristics from a mechanical perspective, such as flowing and wetting on surrounding surfaces, giving compliant, conformal and deformable behavior. From the behavior of soft matter for heterogeneous surfaces, compliant structures can be engineered as embedded liquid microstructures or patterned liquid microsystems for emerging compliant microsystems.Recently, skin electronics and soft robotics have been initiated as potential applications that can provide soft interfaces and interactions for a human-machine interface. To meet the design parameters, developing soft material engineering aimed at tuning material properties and smart processing techniques proper to them are to be highly encouraged. As promising candidates, Ga-based liquid alloys and silicone-based elastomers have been widely applied to proof-of-concept compliant structures.In this thesis, the liquid alloy was employed as a soft and stretchable electrical and thermal conductor (resistor), interconnect and filler in an elastomer structure. Printing-based liquid alloy patterning techniques have been developed with a batch-type, parallel processing scheme. As a simple solution, tape transfer masking was combined with a liquid alloy spraying technique, which provides robust processability. Silicone elastomers could be tunable for multi-functional building blocks by liquid or liquid-like soft solid inclusions. The liquid alloy and a polymer additive were introduced to the silicone elastomer by a simple mixing process. Heterogeneous material microstructures in elastomer networks successfully changed mechanical, thermal and surface properties.To realize a compliant microsystem, these ideas have in practice been useful in designing and fabricating soft and stretchable systems. Many different designs of the microsystems have been fabricated with the developed techniques and materials, and successfully evaluated under dynamic conditions. The compliant microsystems work as basic components to build up a whole system with soft materials and a processing technology for our emerging society.
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| 23. |
- Pardon, Gaspard, 1983-
(författare)
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From Macro to Nano : Electrokinetic Transport and Surface Control
- 2014
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Today, the growing and aging population, and the rise of new global threats on human health puts an increasing demand on the healthcare system and calls for preventive actions. To make existing medical treatments more efficient and widely accessible and to prevent the emergence of new threats such as drug-resistant bacteria, improved diagnostic technologies are needed. Potential solutions to address these medical challenges could come from the development of novel lab-on-chip (LoC) for point-of-care (PoC) diagnostics.At the same time, the increasing demand for sustainable energy calls for the development of novel approaches for energy conversion and storage systems (ECS), to which micro- and nanotechnologies could also contribute.This thesis has for objective to contribute to these developments and presents the results of interdisciplinary research at the crossing of three disciplines of physics and engineering: electrokinetic transport in fluids, manufacturing of micro- and nanofluidic systems, and surface control and modification. By combining knowledge from each of these disciplines, novel solutions and functionalities were developed at the macro-, micro- and nanoscale, towards applications in PoC diagnostics and ECS systems.At the macroscale, electrokinetic transport was applied to the development of a novel PoC sampler for the efficient capture of exhaled breath aerosol onto a microfluidic platform.At the microscale, several methods for polymer micromanufacturing and surface modification were developed. Using direct photolithography in off-stoichiometry thiol-ene (OSTE) polymers, a novel manufacturing method for mold-free rapid prototyping of microfluidic devices was developed. An investigation of the photolithography of OSTE polymers revealed that a novel photopatterning mechanism arises from the off-stoichiometric polymer formulation. Using photografting on OSTE surfaces, a novel surface modification method was developed for the photopatterning of the surface energy. Finally, a novel method was developed for single-step microstructuring and micropatterning of surface energy, using a molecular self-alignment process resulting in spontaneous mimicking, in the replica, of the surface energy of the mold.At the nanoscale, several solutions for the study of electrokinetic transport toward selective biofiltration and energy conversion were developed. A novel, comprehensive model was developed for electrostatic gating of the electrokinetic transport in nanofluidics. A novel method for the manufacturing of electrostatically-gated nanofluidic membranes was developed, using atomic layer deposition (ALD) in deep anodic alumina oxide (AAO) nanopores. Finally, a preliminary investigation of the nanopatterning of OSTE polymers was performed for the manufacturing of polymer nanofluidic devices.
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| 24. |
- Heshmati, Mohsen, 1987, et al.
(författare)
-
Dependency of cohesive laws of a structural adhesive in Mode-I and Mode-II loading on moisture, freeze-thaw cycling, and their synergy
- 2017
-
Ingår i: Materials and Design. - : Elsevier BV. - 1873-4197 .- 0264-1275. ; 122, s. 433-447
-
Tidskriftsartikel (refereegranskat)abstract
- In recent years, adhesive bonding has found its way to construction applications such as bridges. Given the harsh conditions that such structures are usually exposed to, it is necessary to account for environmental factors, particularly moisture and temperature, in the design phase. Cohesive zone modelling has attracted much attention in the last decade as a promising method to design adhesive joints. Despite this interest, the effects of moisture and thermal cycles on cohesive laws have not been investigated to the knowledge of the authors. In this paper, we present a method to directly measure the environmental-dependent cohesive laws of a structural adhesive loaded in pure Mode-I and Mode-II. Special consideration is given to overcome issues such as the time-consuming nature of moisture ingression and specimen dimensions, which could be problematic due to the size-limitations of conditioning equipment. The accuracy of this method was verified through simulation of the experiments using the finite element analysis. The effects of exposure to 95% relative humidity, immersion in saltwater and distilled water, and freeze-thaw cycles in the presence or absence of moisture were investigated. The results indicate the damaging effects of combined saltwater and freeze-thaw cycles which were clearly reflected on the shape of the cohesive laws.
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| 25. |
- Lindberg, Siv M, et al.
(författare)
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A product semantic study of the influence of the sense of touch on the evaluation of wood-based materials
- 2013
-
Ingår i: Materials & design. - : Elsevier BV. - 0264-1275 .- 1873-4197 .- 0261-3069. ; 52, s. 300-307
-
Tidskriftsartikel (refereegranskat)abstract
- Based on product semantics, this study investigated how the tactile attributes of wood and wood-based composites are perceived and interpreted semantically. The wood-based samples included ash, birch, elm, oak, pine, OSB (oriented strand board), two wood pulp-reinforced polylactide composites, Comp A and B and one wood-fiber reinforced polypropene composite, Comp C. The subjects rated the samples by the descriptive words natural, exclusive, eco-. friendly, rough, inexpensive, reliable, warm, modern, snug and solid. The most significant differences between the samples were found for roughness and for the descriptors, reliable, natural and solid. A principal component analysis yielded three attributes based on the tactile perceptions: reliable, old-. fashioned and smooth. The solid wood pieces were perceived as natural and oak was perceived as being exclusive. The composite materials presented a greater variation in terms of perceived attributes than the wood specimens.
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| 26. |
- Åkerfeldt, Maria, 1982, et al.
(författare)
-
Textile piezoelectric sensors – melt spun bi-component poly(vinylidene fluoride) fibres with conductive cores and poly(3,4-ethylene dioxythiophene)-poly(styrene sulfonate) coating as the outer electrode
- 2014
-
Ingår i: Fashion and Textiles. - : Springer Science and Business Media LLC. - 2198-0802. ; 1:1
-
Tidskriftsartikel (refereegranskat)abstract
- The work presented here addresses the outer electroding of a fully textile piezoelectric strain sensor, consisting of bi-component fibre yarns of β-crystalline poly(vinylidene fluoride) (PVDF) sheath and conductive high density polyethylene (HDPE)/carbon black (CB) core as insertions in a woven textile, with conductive poly(3,4-ethylene dioxythiophene)-poly(styrene sulfonate) (PEDOT:PSS) coatings developed for textile applications. Two coatings, one with a polyurethane binder and one without, were compared for the application and evaluated as electrode material in piezoelectric testing, as well as tested for surface resistivity, tear strength, abrasion resistance and shear flexing. Both coatings served their function as the outer electrodes in the system and no difference in this regard was detected between them. Omission of the binder resulted in a surface resistivity one order of magnitude less, of 12.3 Ω/square, but the surface resistivity of these samples increased more upon abrasion than the samples coated with binder. The tear strength of the textile coated with binder decreased with one third compared to the uncoated substrate, whereas the tear strength of the coated textile without binder increased with the same amount. Surface resistivity measurements and scanning electron microscopy (SEM) images of the samples subjected to shear flexing showed that the coatings without the binder did not withstand this treatment, and that the samples with the binder managed this to a greater extent. In summary, both of the PEDOT:PSS coatings could be used as outer electrodes of the piezoelectric fibres, but inclusion of binder was found necessary for the durability of the coating.
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| 27. |
- Zhang, Yubin, et al.
(författare)
-
Stress relief during annealing of railway wheel steel characterized by synchrotron X-ray micro-diffraction
- 2022
-
Ingår i: 42nd Risø International Symposium on Materials Science. - : Institute of Physics Publishing (IOPP). ; 1249
-
Konferensbidrag (refereegranskat)abstract
- Railway wheels in service experience rolling contact fatigue loading, but also need to resist frictional heating on braking, yielding temperatures up to 500 degrees C. The combination of mechanical and thermal loads leads to changes in the mechanical properties of the material. The focus of this study is to investigate the effect of annealing on local microstructure and residual stresses in railway wheel pearlitic steel (medium carbon steels, similar to 0.55 wt.% C) using synchroton X-ray Laue micro-diffraction. It is found that the local residual stress releases to a large extent after annealing at 500 degrees C. The stress formation and relief mechanisms and their relationship to the local microstructure are discussed.
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| 28. |
- Decrop, Deborah, et al.
(författare)
-
Single-step manufacturing of femtoliter microwell arrays in a novel surface energy mimicking polymer
- 2015
-
Ingår i: 18th International Conference on Solid-State Sensors, Actuators and Microsystems (IEEE TRANSDUCER 2015). - : IEEE.
-
Konferensbidrag (refereegranskat)abstract
- We report a novel polymer material formulation and stamp-molding technique that enable rapid single-step manufacturing of hydrophilic-in-hydrophobic microwell arrays. We developed a modified thiol-ene-epoxy polymer (mOSTE+) formulation that mimics the surface energy of its mold during polymerization. The polymer inherits the surface energy from the mold through molecular self-assembly, in which functional monomers self-assemble at the interface between the liquid prepolymer and the mold surface. Combining this novel mOSTE+ material with a stamp-molding process leads to simultaneous surface energy mimicking and micro-structuring. This method was used to manufacture microwells with hydrophilic bottom and hydrophobic sidewall, depressed in a surrounding hydrophobic surface. The microwell arrays were successfully tested for the self-assembly of 62’000 femtoliter-droplets. Such femtoliter droplet arrays are useful for, e.g., digital ELISA and single cell/molecule analysis applications.
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| 29. |
- Åkerfeldt, Pia, et al.
(författare)
-
Electron backscatter diffraction characterization of fatigue crack growth in laser metal wire deposited Ti-6Al-4V
- 2018
-
Ingår i: Materials Characterization. - : Elsevier BV. - 1044-5803 .- 1873-4189. ; 135, s. 245-256
-
Tidskriftsartikel (refereegranskat)abstract
- By additive manufacturing (AM) there is a feasibility of producing near net shape components in basically one step from 3D CAD model to final product. The interest for AM is high and during the past decade a lot of research has been carried out in order to understand the influence from process parameters on the microstructure and furthermore on the mechanical properties. In the present study laser metal wire deposition of Ti-6Al-4V has been studied in detail with regard to its fatigue crack propagation characteristics. Two specimen orientations, parallel and perpendicular to the deposition direction, have been evaluated at room temperature and at 250 °C. No difference in the fatigue crack growth rate could be confirmed for the two specimen orientations. However, in the fractographic study it was observed that the tortuosity varied between certain regions on the fracture surface. The local crack path characteristic could be related to the alpha colony size and/or the crystallographic orientation. Moreover, large areas exhibiting similar crystallographic orientation were observed along the prior beta grain boundaries, which were attributed to the wide alpha colonies frequently observed along the prior beta grain boundaries. © 2017 Elsevier Inc.
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| 30. |
- Moldenhauer, Patrick, 1983, et al.
(författare)
-
Chemical-looping combustion with heavy liquid fuels in a 10 kW pilot plant
- 2017
-
Ingår i: Fuel Processing Technology. - : Elsevier BV. - 0378-3820. ; 156, s. 124-137
-
Tidskriftsartikel (refereegranskat)abstract
- In this study, chemical-looping combustion was performed with highly viscous vacuum residue. A fuel reactor with a fuel-injection system for liquid fuels was designed and built for a chemical-looping reactor with the nominal fuel input of 10 kWth. The gas velocities in the riser section and at the gas-distribution nozzles of this unit are comparable to those of industrial circulating fluidized-bed boilers. Reference experiments were performed with an ilmenite oxygen carrier and two different fuel blends that contained 40 wt.% and respectively 80 wt.% of vacuum residue in fuel oil 1. Fuel conversion was in line with that of experiments from an earlier campaign, where fuel oil 1 was used as fuel. The fuel contained a significant fraction of sulfur, but no SO2 was detected in the flue gas of the air reactor. More experiments were performed using an oxygen carrier based on calcium manganite. The oxygen carrier was exposed to fluidization at hot conditions (more than 600°C) for about 95 h, out of which fuel was injected during a total of 9.6 h. Undiluted vacuum residue, fuel oil 1 as well as different blends of these two were used as fuel. Furthermore, the parameters fuel flow, fuel-reactor temperature and air flow in the air reactor were varied to observe trends in fuel conversion. The experiments were carried out with a fuel flow corresponding to 4.0-6.2 kWth and an oxygen carrier-to-fuel ratio of about 1300-2000 kg/MWth (fuel-reactor bed mass per thermal fuel-power). With undiluted vacuum residue as fuel and a fuel-reactor temperature of 1000°C, up to 93% of all carbon leaving the fuel reactor was in the form of CO2. Carbon leakage from fuel reactor to air reactor was usually below 1% for all fuel types tested, but no SO2 was detected in the off-gas from the air reactor. The reactivity of the calcium manganite-based material decreased over the course of the experiments, which is likely due to sulfur poisoning. No defluidization or agglomeration problems were experienced over the course of the experimental campaign.
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| 31. |
- André, Benny
(författare)
-
Nanocomposites for Use in Sliding Electrical Contacts
- 2011
-
Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- In this thesis nanocomposite materials for use in high performance electrical contacts are tested. Self mating silver as coatings on cupper substrates are the most used material combination in power connectors today. In this work two new concepts were tested. The first one was to change one of the mating surfaces to a hard thin coating and keep the other surface made of silver. Tested coatings were nanocomposites with hard carbides in a matrix of amorphous carbon. TiC/a-C and Ti-Ni-C/a-C were tested both electrically and tribologically. The total amount of carbon and the amount of carbon matrix was important, both for the electrical and the tribological properties. The Ti-Ni-C coating also showed that substituting Ti in TiC with the weak carbide former Ni changed the stability of the carbides. The substitution resulted in more a-C matrix and less C in the carbides. Thin coatings of nc-TiC/a-C and Ti-Ni-C/a-C showed high potential as material candidates for use in electrical contacts. The other tested concept was to modify the used silver instead of replacing it. This was done by embedding nanoparticles of solid lubricant IF-WS2 in the silver. The results from reciprocating sliding displayed low friction and high wear resistance. The modified silver surfaces lasted for 8000 strokes with a friction of about 0.3 while at the same time allowing for a low contact resistance. The results for surfaces of pure silver coating displayed a friction of 0.8-1.2 and that the silver was worn through already after 300 strokes. A new method to investigate inherent hardness and residual stress of thin coatings, on complex geometries or in small areas, was also developed. An ion beam was used to create stress free coating as free standing micro pillars. Hardness measured on the pillars and on as-deposited coating were then used to calculate the residual stress in the coatings.
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| 32. |
- Zhang, Emma, 1985, et al.
(författare)
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Predicting degradation of the anode-concrete interface for impressed current cathodic protection in concrete
- 2018
-
Ingår i: Construction and Building Materials. - : Elsevier BV. - 0950-0618. ; 185, s. 57-68
-
Tidskriftsartikel (refereegranskat)abstract
- Impressed current cathodic protection and prevention techniques are efficient methods to stop or prevent corrosion in steel reinforced concrete structures. The inevitable side effect of the current exchange is acidification at the anode-concrete interface. Accelerated test methods can be used to investigate the long-term performance of the system. However, a linear relation will not hold between the accelerated and normal conditions because of the influence of the current density. This paper presents results of an accelerated test. A power-relation conversion model is proposed and an acceleration factor is introduced. (C) 2018 Elsevier Ltd. All rights reserved.
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| 33. |
- Mathern, Alexandre, 1986, et al.
(författare)
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Experimental study of time-dependent properties of a low-pH concrete for deposition tunnels
- 2018
-
Ingår i: fib Symposium. - 2617-4820. ; , s. 1726-1735
-
Konferensbidrag (refereegranskat)abstract
- The Swedish Nuclear Fuel and Waste Management Company developed a method for the final disposal of canisters for spent nuclear fuel in tunnels at depths of about 500 meters. The concept for closure of the deposition tunnels is based on a bentonite seal supported by a spherical concrete dome structure. In order to fulfil the requirements specific to the repository concept, a special mix of low-pH self-compacting concrete was developed. A series of large-scale castings and laboratory tests were conducted to gain experience on this low-pH concrete mix, in conjunction with the full-scale demonstration test of an unreinforced concrete dome plug in the underground hard rock laboratory in Äspö, Sweden. The laboratory tests aimed at studying the creep properties under high sustained compressive stresses of the low-pH concrete mix, its shrinkage properties and the properties of the rock-concrete interface. This paper provides an overview of these tests and analyses the latest results of the recently completed creep tests, which include 6 years of measurements. These results allow to improve understanding of the structural behaviour of the concrete plug and to assess the effects of the very high pressure acting on the plug on its deformations, cracking and water tightness.
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| 34. |
- Holmberg, Jonas, et al.
(författare)
-
Experimental and PFEM-simulations of residual stresses from turning tests of a cylindrical Ti-6Al-4V shaft
- 2018
-
Ingår i: Procedia CIRP. - : Elsevier. - 2212-8271 .- 2212-8271. ; 71, s. 144-149
-
Tidskriftsartikel (refereegranskat)abstract
- Alloy Ti-6Al-4V is a frequently used material in aero space applications due the high strength and low weight. This material is however often considered as a difficult to machine alloy due to several material properties such as the inherent characteristics of high hot hardness and strength which is causing an increased deformation of the cutting tool during machining. The thermal properties also cause a low thermal diffusion from locally high temperatures in the cutting zone that allows for reaction to the tool material resulting in increased tool wear.Predicting the behavior of machining of this alloy is therefore essential when selecting machining tools or machining strategies. If the surface integrity is predicted, the influence of different machining parameters could be studied using Particle Finite Element (PFEM)-simulations. In this investigation the influence from cutting speed and feed during turning on the residual stresses has been measured using x-ray diffraction and compared to PFEM-simulations.The results showed that cutting speed and feed have great impact on the residual stress state. The measured cutting force showed a strong correlation especially to the cutting feed. The microstructure, observed in SEM, showed highly deformed grains at the surface from the impact of the turning operation and the full width half maximum from the XDR measurements distinguish a clear impact from different cutting speed and feed which differed most for the higher feed rate.The experimental measurements of the residual stresses and the PFEM simulations did however not correlate. The surface stresses as well as the sign of the residuals stresses differed which might be due to the material model used and the assumption of using a Coulomb friction model that might not represent the cutting conditions in the investigated case.
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| 35. |
- Henrysson, Erica, 1987, et al.
(författare)
-
Conceptual Design and Analysis of Membrane Structures
- 2016
-
Ingår i: Proceedings of 29th Nordic Seminar on Computational Mechanics – NSCM29.
-
Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- In this work one approach for formfinding and analysing tension membranestructures is described. Focus has been on the conceptual stage. For this the computersoftware SMART Form has been further developed, enabling the possibility to do real-timeformfinding and analysis of fabric structures. The software is based on a method where theorthotropic membrane is modeled with a triangular mesh, where the mass is lumped on thenodes. As a computational tool dynamic relaxation is used to find the static equilibriumconfiguration for the structure. The advantage with this is that there is no need for formulationand manipulation of matrices common in the finite element method.
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| 36. |
- Norman, Peter, et al.
(författare)
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A sophisticated platform for characterization, monitoring and control of machining
- 2006
-
Ingår i: Measurement science and technology. - BRISTOL, ENGLAND : IOP Publishing. - 0957-0233 .- 1361-6501. ; 17:4, s. 847-854
-
Tidskriftsartikel (refereegranskat)abstract
- The potential for improving the performance of machine tools is considerable. However, for this to be achieved without tool failure or product damage, the process must be sufficiently well understood to enable real-time monitoring and control to be applied. A unique sophisticated measurement platform has been developed and applied to two different machining centres, particularly for high-speed machining up to 24 000 rpm. Characterization and on-line monitoring of the dynamic behaviour of the machining processes has been carried out using both contact-based methods (accelerometer, force sensor) and non-contact methods (laser Doppler vibrometry and magnetic shaker) and numerical simulation (finite element based modal analysis). The platform was applied both pre-process and on-line for studying an aluminium testpiece based on a thin-walled aerospace component. Stability lobe diagrams for this specific machine/component combination were generated allowing selection of optimal process parameters giving stable cutting and metal removal rates some 8-10 times higher than those possible in unstable machining. Based on dynamic characterization and monitoring, a concept for an adaptive control with constraints based machine tool controller has been developed. The developed platform can be applied in manifold machining situations. It offers a reliable way of achieving significant process improvement
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| 37. |
- Täljsten, Björn, 1961-, et al.
(författare)
-
Assessment of prestressed concrete bridges - challenges
- 2020
-
Ingår i: IABSE Symposium, Wroclaw 2020. - Zürich : International Association For Bridge And Structural Engineering (IABSE). ; , s. 487-494
-
Konferensbidrag (refereegranskat)abstract
- Prestressed concrete bridges are important parts of our infrastructure. They are susceptible to different kinds of deterioration processes. Examples of damages and deficiencies are cracking, corrosion, voids, bond loss, reduction of cover layer, delamination, fatigue and loss of stiffness and strength. This necessitates methods to continuously assess their condition in order to avoid problems that might lead to shorter service life or reduction of structural integrity. Many of the existing prestressed bridges in Europe are now approaching their design life length. However, with proper and continuous inspection, monitoring and assessment, we may plan proactive maintenance and the structural safety can be assured or – if necessary - increased. This will save both money and decrease the environmental impact of the structure.
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| 38. |
- Guldris Leon, Lorena, 1983, et al.
(författare)
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Understanding Mineral Liberation during Crushing Using Grade-by-Size Analysis - A Case Study of the Penuota Sn-Ta Mineralization, Spain
- 2020
-
Ingår i: Minerals. - : MDPI AG. - 2075-163X. ; 10:2
-
Tidskriftsartikel (refereegranskat)abstract
- Coarse comminution test-work and modeling are powerful tools in the design and optimization of mineral processing plants and provide information on energy consumption. Additional information on mineral liberation characteristics can be used for assessing the potential of pre-concentration stages or screens in the plant design. In ores of high-value metals (e.g., Ta, W), standard techniques-such as the mineralogical quantification of grain mounts by quantitative evaluation of minerals by scanning electron microscopy (QEMSCAN) or chemical analysis by X-ray fluorescence (XRF) can be challenging, due to the low relative abundance of such valuable minerals. The cost of QEMSCAN is also a limiting factor, especially considering the large number of samples required for the optimization of coarse comminution. In this study, we present an extended analytical protocol to a well-established mechanical test of interparticle breakage to improve the assessment of coarse mineral liberation characteristics. The liberation of ore minerals is a function of the rock texture and the difference in size and mechanical properties of the valuable minerals relative to gangue minerals and they may fraction in certain grain sizes if they behave differently during comminution. By analyzing the bulk-chemistry of the different grain size fractions produced after compressional testing, and by generating element by size diagrams, it is possible to understand the liberation characteristics of an ore. We show, based on a case study performed on a tantalum ore deposit, that element distribution can be used to study the influence of mechanical parameters on mineral liberation. This information can direct further mineralogical investigation and test work.
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| 39. |
- Meyer, Knut Andreas, 1990, et al.
(författare)
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Microstructure and mechanical properties of the running band in a pearlitic rail steel : Comparison between biaxially deformed steel and field samples
- 2018
-
Ingår i: Wear. - : Elsevier. - 0043-1648 .- 1873-2577. ; 396-397, s. 12-21
-
Tidskriftsartikel (refereegranskat)abstract
- The large deformations occurring in the surface layer of rail heads strongly influence the material behavior. Cracks typically develop from this critical region. However, conventional material testing of this layer is not possible due to the large gradients. A method for obtaining a similar material through predeformation is therefore investigated. Subsequent analyses of the obtained material can improve our understanding of the material behavior close to the running band. Hardness, shear lines and cementite lamella orientation distributions are compared in order to determine whether the obtained material is similar to that of the field samples extracted from rails that have been in service for several years. The predeformation method produces a consistent material, which is representative of the material in the rail field samples that have accumulated large shear strains.
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| 40. |
- Seoane, Fernando, et al.
(författare)
-
Conductive Polymer Films as Textrodes for Biopotential Sensing
- 2011
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Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- Introduction: After several years of progresses in textile technology and wearable measurement instrumentation, applications of wearable textile-electronics systems are arising providing a stable background for commercial applications. So far, the available commercial solutions are centered on fitness applications and mostly based in the acquisition of heart rate through Textile Electrodes (Textrodes) based on metallic threads or on conductive rubber compounds. Methods and Materials: In this work a novel material approach is presented to produce Textrodes for acquisition of Electrocardiographic (ECG) signals using a conductive polypropylene (PP1386 from Premix, Finland) polymer material. The polymer was film extruded into thin films, and used as such in the Textrode. Conductive Polymer Films (CPF) have been used to produce Textrodes, and its measurement performance has been compared with the ECG signals obtained with commercial Textrode fabrics and conventional Ag/AgCl electrodes. In order to set up the same measurement conditions, a chest strap tailored to host the testing electrodes has been used. Results: The close resemblance of the ECG acquired with the textile fabric electrodes, the Ag/AgCl electrodes and the PP1386 CPF electrodes suggest that the Polymer Electrodes PP1386 are a feasible alternative to the current textile fabrics that use silver thread as conductive material and also to conductive rubber material. Discussion & Conclusion: The availability of the Conductive Polymer Electrode PP1386 in a film form allows the manufacturing of electrodes by conventional textile processes, like lamination or sewing, therefore facilitating the transition from lab prototyping to industrial manufacturing. Replacing the traditional silver thread as conductive element in the fabrication of Textrodes will definitely reduce the material cost per Textrode. Biocompatibility issues and manufacturability issues must be addressed but the exhibited functional performance is showing encouraging results.
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| 41. |
- Jeong, Seung Hee, 1978-, et al.
(författare)
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Stretchable Thermoelectric Generators Metallized with Liquid Alloy
- 2017
-
Ingår i: ACS Applied Materials & Interfaces. - : American Chemical Society (ACS). - 1944-8252 .- 1944-8244. ; 9:18, s. 15791-15797
-
Tidskriftsartikel (refereegranskat)abstract
- Conventional thermoelectric generators (TEGs) are normally hard, rigid, and flat. However, most objects have curvy surfaces, which require soft and even stretchable TEGs for maximizing efficiency of thermal energy harvesting. Here, soft and stretchable TEGs using conventional rigid Bi2Te3 pellets metallized with a liquid alloy is reported. The fabrication is implemented by means of a tailored layer-by-layer fabrication process. The STEGs exhibit an output power density of 40.6 ?W/cm2 at room temperature. The STEGs are operational after being mechanically stretched-and-released more than 1000 times, thanks to the compliant contact between the liquid alloy interconnects and the rigid pellets. The demonstrated interconnect scheme will provide a new route to the development of soft and stretchable energy-harvesting avenues for a variety of emerging electronic applications.
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| 42. |
- Kanesund, Jan-erik
(författare)
-
Influence of deformation and environmental degradation of Inconel 792
- 2017
-
Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Industrial gas turbines are often used as a mechanical drive for pumps and compressors or in power generation as an electric power supply. The gas turbine has for many years been a popular engine due to its flexibility with respect to different types of fuel and due to a design, that enables a high power-to-weight ratio. A simplified description of a gas turbine is that the engine consists of a cold and hot section. The turbo compressor section belongs to cold section and the combustion chamber together with the turbine section belongs to the hot section. In the hot section of a gas turbine, the condition is extremely severe because of an aggressive environment characterized by high temperatures, increased temperature gradients, high pressure and centrifugal forces resulting in large stresses on individual components together with an oxidizing and corroding atmosphere. Materials used in the high temperature section (hot gas path) of a modern gas turbine are different types of superalloys, as single crystal, directionally solidified or polycrystalline alloys, depending on temperature and load conditions. In the first turbine stage, temperature is very high due to exposure to the combustion gas. To handle the problem with creep, single crystal superalloys are often used in this section. In the second row of turbine blades, the temperature of the gas is lower and polycrystalline superalloys are typically used. IN-792 is a cast polycrystalline superalloy with high strength, good resistance to hot corrosion and a cheaper option than single crystals. In the hot section of gas turbine, IN-792 is a suitable material for components such as turbine blades and vans where a complex load condition, high temperature and severe environment prevails. Due to startup and shutdown of the gas turbine engine during service, the components in the hot section are exposed to cyclic load and temperature. This will generate mechanical and thermal fatigue damage in gas turbine components. Steady state temperature gradient arises by the cooling system acting at cold spots during service to introduce tensile stress, which indirectly gives rise to creep damage in the component. This work includes tree studies of deformation and damage mechanisms of superalloy IN-792. The first study is made on test bars exposed to thermomechanical fatigue in laboratory environment, the second and the third study is made on turbine blades used during service. In the second study, the machines are placed off-shore and exposed to marine environment. In the third study the machine is landbased and exposed to an industrial environment. In the second study, the deformation and damage mechanisms are compared between the turbine blades used during service and the test bars exposed to thermomechanical fatigue testing in the first study.
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| 43. |
- Steyn, Erika, 1990
(författare)
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Railway wheel steel behaviour upon thermo-mechanical loadings
- 2022
-
Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Optimised railway maintenance techniques such as rail grinding and milling, or rail repair welding, are vital to more sustainable rail networks. As demands on the railway increases, the need to better understand the material behaviour during local heating events occurring during maintenance is amplified. Other heating events can occur during operation, for instance during severe block braking. This thesis provides insight into thermal damage resulting from these local heating events on railway wheels, which can lead to altered mechanical properties and changed residual stresses. The material behaviour of the ferritic-pearlitic railway wheel steel ER7T was studied during severe block braking (i.e., slow heating and cooling) at peak temperatures varying between 300 °C and 650 °C. The thermal dilatation was restricted to different degrees between free expansion and full restriction. This study thus explores the combined effect of thermal and mechanical cycling on the mechanical properties and material structure. The experimental results from the thermo-mechanical testing were also used to validate a new constitutive material model for use in FE models to predict severe block braking. The second part of the thesis explored the effect of rapid heating and cooling events on the microstructure and residual stress state of railway wheel steel. Localised heating using laser scanning with additive manufacturing equipment was compared to the heating done by scanning with laser welding equipment. This study thus investigated the similarities of different rapid heating (high temperature) processes and the effect of process parameter variations. The results can be used to provide insight into the material behaviour of railway steels during local heating events. Furthermore, it can support the development of more accurate simulations for both operation and maintenance processes.
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| 44. |
- Elbadawi, Mohammed, 1987-, et al.
(författare)
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Pressure-assisted microsyringe 3D printing of oral films based on pullulan and hydroxypropyl methylcellulose
- 2021
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Ingår i: International Journal of Pharmaceutics. - : Elsevier. - 0378-5173 .- 1873-3476. ; 595
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Tidskriftsartikel (refereegranskat)abstract
- Oral films (OFs) continue to attract attention as drug delivery systems, particularly for pedatric and geriatric needs. However, immiscibility between different polymers limits the full potential of OFs from being explored. One example is pullulan (PUL), a novel biopolymer which often has to be blended with other polymers to reduce cost and alter its mechanical properties. In this study, the state-of-the-art in fabrication techniques, three-dimensional (3D) printing was used to produce hybrid film structures of PUL and hydroxypropyl methylcellulose (HPMC), which were loaded with caffeine as a model drug. 3D printing was used to control the spatial deposition of films. HPMC was found to increase the mean mechanical properties of PUL films, where the tensile strength, elastic modulus and elongation break increased from 8.9 to 14.5 MPa, 1.17 to 1.56 GPa and from 1.48% to 1.77%, respectively. In addition, the spatial orientation of the hybrid films was also explored to determine which orientation could maximize the mechanical properties of the hybrid films. The results revealed that 3D printing could modify the mechanical properties of PUL whilst circumventing the issues associated with immiscibility.
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| 45. |
- Belitsky, Victor, 1955, et al.
(författare)
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Towards Multi-Pixel Heterodyne Terahertz Receivers
- 2011
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Ingår i: Proceedings of the 22nd International Symposium on Space Terahertz Technology, Tucson, AZ, USA, April 26-28, 2011. ; , s. 1-3
-
Konferensbidrag (refereegranskat)abstract
- Terahertz multi-pixel heterodyne receivers introduce multiple challenges for their implementation, mostly due to the extremely small dimensions of all components and even smaller tolerances in terms of alignment, linear dimensions and waveguide component surface quality. In this manuscript, we present a concept of terahertz multi-pixel heterodyne receiver employing optical layout using polarization split between the LO and RF. The frontend is based on a waveguide balanced HEB mixer for the frequency band 1.6 – 2.0 THz. The balanced HEB mixer follows the layout of earlier demonstrated APEX T2 mixer. However for the mixer presented here, we implemented splitblock layout offering minimized lengths of all waveguides and thus reducing the associated RF loss. The micromachining methods employed for producing the mixer housing and the HEB mixer chip are very suitable for producing multiple structures and hence are in-line with requirements of multi-pixel receiver technology. The demonstrated relatively simple mounting of the mixer chip with self-aligning should greatly facilitate the integration of such multi-channel receiver.
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| 46. |
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| 47. |
- Shaikh, Abdul Shaafi, 1989, et al.
(författare)
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On the effect of building platform material on laser-powder bed fusion of a Ni-base superalloy HAYNES® 282®
- 2023
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Ingår i: European Journal of Materials. - : Informa UK Limited. - 2688-9277. ; 3:1
-
Tidskriftsartikel (refereegranskat)abstract
- Additive manufacturing (AM) by laser powder bed fusion (LPBF) involves melting of layers of powder onto a substrate, called a building platform. Due to cost or convenience considerations, building platform materials rarely match the LPBF material, especially for high temperature materials. To ensure tolerances in component geometries, AM components are often stress-relieved/heat-treated while still attached to the building platform. It is therefore important to understand the effect of dissimilar building platform materials on the properties of the built-up material. These effects may be particularly important for high performance materials such as Ni-base superalloys used for critical applications in the aerospace and energy industries. To investigate this effect, samples of a Ni-base superalloy HAYNES® 282® were built onto a carbon steel building platform in several configurations. The samples were removed from the building platform after heat treatment and subjected to detailed composition analysis and microstructural characterization to investigate the effect of the building platform material on the properties of the additively manufactured part. Room temperature and high temperature tensile testing were used to characterize the material. Results showed no risk of large-scale chemical composition change, or mechanical property degradation of built-up material from on-platform heat treatment.
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| 48. |
- Singh, Sukhdeep, 1988, et al.
(författare)
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Influence of Hot Isostatic Pressing on the Hot Ductility of Cast Alloy 718 : The Effect of Niobium and Minor Elements on the Liquation Mechanism
- 2020
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Ingår i: Metallurgical and Materials Transactions. A. - : Springer. - 1073-5623 .- 1543-1940. ; 51:12, s. 6248-6257
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Tidskriftsartikel (refereegranskat)abstract
- The influence of two hot isostatic pressing (HIP) treatments on liquation behavior was investigated and compared with regard to the extent of heat-affected zone liquation cracking in cast Alloy 718. The extent of liquation was seen to increase after HIP treatment at 1190 °C due to solute changes caused by the homogenization of Nb, which contributed to extensive grain boundary melting. The HIP treatment at 1120 °C exhibited lower liquation with contributions from particle liquation of the Laves phase and constitutional liquation of NbC carbides. This was also reflected in a lower ductility recovery temperature, with slower recovery for the former due to the extensive liquation. Interestingly, the nil ductility temperatures were both below the predicted equilibrium solidus of the alloy, which suggests that the ductility drop is related to liquation caused by solute segregation at the grain boundaries. © 2020, The Author(s).
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| 49. |
- Koptyug, Andrey, 1956-, et al.
(författare)
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Electron Beam Melting: from Shape Freedom to Materials Properties Control at Macro- and Microscale
- 2021
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Ingår i: Proceedings of the THERMEC 2020, Graz, Austria. - : Trans Tech Publications. ; , s. 755-759
-
Konferensbidrag (refereegranskat)abstract
- Electron beam melting (EBM) is one of the constantly developing powder bed fusion (PBF) additive manufacturing technologies (AM) offering advanced control over the manufacturing process. Freedom of component shapes is one of the AM competitive advantages already used at industrial and semi- industrial scale. Development of the additive manufacturing today is targeting both widening of the available materials classes, and introducing new enabling modalities. Present research is related to the new possibilities in tailoring different material properties within additively manufactured components effectively adding “fourth dimension to the 3D-printing”. Specific examples are given in relation to the electron beam melting, but majority of the conclusions are valid for the laser-based PBF techniques as well. Through manipulating beam energy deposition it is possible to tailor quite different material properties selectively within each manufactured component, including effective material density as well as thermal, mechanical, electrical and acoustic properties. It is also possible to acquire by choice both metal-metal composite and completely alloyed material, when blends of precursor powder are used together with the beam energy manipulation.
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| 50. |
- Sefer, Birhan, 1983-, et al.
(författare)
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Chemical Milling of Cast Ti-6Al-4V and Ti-6Al-2Sn-4Zr-2Mo Alloys in Hydrofluoric-Nitric Acid Solutions
- 2017
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Ingår i: Corrosion. - : Association for Materials Protection and Performance (AMPP). - 0010-9312 .- 1938-159X. ; 73:4, s. 394-407
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Tidskriftsartikel (refereegranskat)abstract
- The behavior of cast Ti-6Al-4V and Ti-6Al-2Sn-4Zr-2Mo during chemical milling in hydrofluoric-nitric (HF-HNO3) acid solutions with 1:3 and 1:11 molar ratios was investigated using electrochemical and atomic force microscopy (AFM) techniques. Faster corrosion rate in 1:3 solutions was measured for Ti-6Al-4V than for Ti-6Al-2Sn-4Zr-2Mo, whereas in 1:11 solution Ti-6Al-2Sn-4Zr-2Mo exhibited higher corrosion rate. Scanning Kelvin probe force microscopy measurements revealed difference in the Volta potential between the α-laths and the β-layers in the Widmansttäten microstructure indicating operation of microgalvanic cells between the microconstituents when in contact with HF-HNO3 solution. The AFM topography measurements demonstrated faster corrosion of the α-laths compared to the β-layers, in both alloys. In 1:3 solutions, higher α/β height difference was measured in Ti-6Al-4V, whereas in 1:11 solution, the difference was higher in Ti-6Al-2Sn-4Zr-2Mo. The results revealed that the chemical milling behavior of the two investigated alloys is controlled by the microscopic corrosion behavior of the individual microconstituents.
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