What is in the fish? Collaborative trial in suspect and non-target screening of organic micropollutants using LC- and GC-HRMS

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What is in the fish? Collaborative trial in suspect and non-target screening of organic micropollutants using LC- and GC-HRMS

Dürig, Wiebke (författare): Swedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment

Lindblad, Sofia (författare): Swedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment

Golovko, Oksana (författare): Swedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment

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Gkotsis, Georgios (författare): Department of Chemistry, National and Kapodistrian University of Athens, Athens, Greece

Aalizadeh, Reza (författare): Department of Chemistry, National and Kapodistrian University of Athens, Athens, Greece

Nika, Maria-Christina (författare): Department of Chemistry, National and Kapodistrian University of Athens, Athens, Greece

Thomaidis, Nikolaos (författare): Department of Chemistry, National and Kapodistrian University of Athens, Athens, Greece

Alygizakis, Nikiforos A. (författare): Department of Chemistry, National and Kapodistrian University of Athens, Athens, Greece; Environmental Institute, Okružná 784/42, Koš, Slovakia

Plassmann, Merle, 1981- (författare): Stockholms universitet,Institutionen för miljövetenskap

Haglund, Peter (författare): Umeå universitet,Kemiska institutionen

Fu, Qiuguo (författare): Eawag: Swiss Federal Institute of Aquatic Science and Technology, Überlandstrasse 133, Dübendorf, Switzerland; Helmholtz Centre for Environmental Research - UFZ, Permoserstraße 15, Leipzig, Germany

Hollender, Juliane (författare): Eawag: Swiss Federal Institute of Aquatic Science and Technology, Überlandstrasse 133, Dübendorf, Switzerland; Institute of Biogeochemistry and Pollutant Dynamics, ETH Zürich, Universitätstrasse 16, Zürich, Switzerland

Chaker, Jade (författare): Université de Rennes, Inserm, EHESP, Irset - UMR_S, Rennes, France

David, Arthur (författare): Université de Rennes, Inserm, EHESP, Irset - UMR_S, Rennes, France

Kunkel, Uwe (författare): Bavarian Environment Agency, Bürgermeister-Ulrich-Straße 160, Augsburg, Germany

Macherius, André (författare): Bavarian Environment Agency, Bürgermeister-Ulrich-Straße 160, Augsburg, Germany

Belova, Lidia (författare): Toxicological Centre, University of Antwerp, Universiteitsplein 1, Wilrijk, Belgium

Poma, Giulia (författare): Toxicological Centre, University of Antwerp, Universiteitsplein 1, Wilrijk, Belgium

Preud'Homme, Hugues (författare): IPREM-UMR5254, E2S UPPA, CNRS, 2 avenue Angot, Pau cedex, France

Munschy, Catherine (författare): Ifremer, CCEM Contamination Chimique des Écosystèmes Marins, Nantes, France

Aminot, Yann (författare): Ifremer, CCEM Contamination Chimique des Écosystèmes Marins, Nantes, France

Jaeger, Carsten (författare): Bundesanstalt für Materialforschung und -prüfung (BAM), Analytical Chemistry, Richard-Willstätter-Straße 11, Berlin, Germany

Lisec, Jan (författare): Bundesanstalt für Materialforschung und -prüfung (BAM), Analytical Chemistry, Richard-Willstätter-Straße 11, Berlin, Germany

Hansen, Martin (författare): Department of Environmental Science, Aarhus University, Frederiksborgvej 399, Roskilde, Denmark

Vorkamp, Katrin (författare): Department of Environmental Science, Aarhus University, Frederiksborgvej 399, Roskilde, Denmark

Zhu, Linyan (författare): Department of Environmental Science, Aarhus University, Frederiksborgvej 399, Roskilde, Denmark

Cappelli, Francesca (författare): Water Research Institute, National Research Council of Italy, Via del Mulino 19, MB, Brugherio, Italy

Roscioli, Claudio (författare): Water Research Institute, National Research Council of Italy, Via del Mulino 19, MB, Brugherio, Italy

Valsecchi, Sara (författare): Water Research Institute, National Research Council of Italy, Via del Mulino 19, MB, Brugherio, Italy

Bagnati, Renzo (författare): Department of Environmental Health Sciences, Istituto di Ricerche Farmacologiche Mario Negri IRCCS, Via Mario Negri 2, Milan, Italy

González, Belén (författare): Department of Analytical Chemistry, Faculty of Science and Technology, University of the Basque Country (UPV/EHU), Barrio Sarriena s/n, Leioa, Spain; Research Centre for Experimental Marine Biology and Biotechnology (PIE), University of the Basque Country (UPV/EHU), Areatza Pasealekua 47, Plentzia, Spain

Prieto, Ailette (författare): Department of Analytical Chemistry, Faculty of Science and Technology, University of the Basque Country (UPV/EHU), Barrio Sarriena s/n, Leioa, Spain; Research Centre for Experimental Marine Biology and Biotechnology (PIE), University of the Basque Country (UPV/EHU), Areatza Pasealekua 47, Plentzia, Spain

Zuloaga, Olatz (författare): Department of Analytical Chemistry, Faculty of Science and Technology, University of the Basque Country (UPV/EHU), Barrio Sarriena s/n, Leioa, Spain; Research Centre for Experimental Marine Biology and Biotechnology (PIE), University of the Basque Country (UPV/EHU), Areatza Pasealekua 47, Plentzia, Spain

Gil-Solsona, Ruben (författare): Catalan Institute for Water Research (ICRA), Carrer Emili Grahit 101, Girona, Spain; Universitat de Girona, Girona, Spain; Institute of Environmental Assessment and Water Research – Severo Ochoa Excellence Center (IDAEA), Spanish Council of Scientific Research (CSIC), Barcelona 08034, Spain

Gago-Ferrero, Pablo (författare): Catalan Institute for Water Research (ICRA), Carrer Emili Grahit 101, Girona, Spain; Institute of Environmental Assessment and Water Research – Severo Ochoa Excellence Center (IDAEA), Spanish Council of Scientific Research (CSIC), Barcelona 08034, Spain

Rodriguez-Mozaz, Sara (författare): Catalan Institute for Water Research (ICRA), Carrer Emili Grahit 101, Girona, Spain; Universitat de Girona, Girona, Spain

Budzinski, Hélène (författare): University Bordeaux, CNRS, Bordeaux INP, EPOC, UMR 5805, Pessac, France

Devier, Marie-Helene (författare): University Bordeaux, CNRS, Bordeaux INP, EPOC, UMR 5805, Pessac, France

Dierkes, Georg (författare): Federal Institute of Hydrology, Am Mainzer Tor 1, Koblenz, Germany

Boulard, Lise (författare): Federal Institute of Hydrology, Am Mainzer Tor 1, Koblenz, Germany; Metabolomics Core Facility, Centre de Ressources et Recherches Technologiques (C2RT), Institut Pasteur, 25-28 Rue du Dr Roux, Paris, France

Jacobs, Griet (författare): Flemish Institute for Technological Research (VITO), Unit Separation and Conversion Technology, Boeretang 200, Mol, Belgium

Voorspoels, Stefan (författare): Flemish Institute for Technological Research (VITO), Unit Separation and Conversion Technology, Boeretang 200, Mol, Belgium

Rüdel, Heinz (författare): Fraunhofer Institute for Molecular Biology and Applied Ecology (Fraunhofer IME), Auf dem Aberg 1, Schmallenberg, Germany

Ahrens, Lutz (författare): Swedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment

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Elsevier, 2023
2023
Engelska.
Ingår i: Environment International. - : Elsevier. - 0160-4120 .- 1873-6750. ; 181

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Tidskriftsartikel (refereegranskat)

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A collaborative trial involving 16 participants from nine European countries was conducted within the NORMAN network in efforts to harmonise suspect and non-target screening of environmental contaminants in whole fish samples of bream (Abramis brama). Participants were provided with freeze-dried, homogenised fish samples from a contaminated and a reference site, extracts (spiked and non-spiked) and reference sample preparation protocols for liquid chromatography (LC) and gas chromatography (GC) coupled to high resolution mass spectrometry (HRMS). Participants extracted fish samples using their in-house sample preparation method and/or the protocol provided. Participants correctly identified 9–69 % of spiked compounds using LC-HRMS and 20–60 % of spiked compounds using GC-HRMS. From the contaminated site, suspect screening with participants’ own suspect lists led to putative identification of on average ∼145 and ∼20 unique features per participant using LC-HRMS and GC-HRMS, respectively, while non-target screening identified on average ∼42 and ∼56 unique features per participant using LC-HRMS and GC-HRMS, respectively. Within the same sub-group of sample preparation method, only a few features were identified by at least two participants in suspect screening (16 features using LC-HRMS, 0 features using GC-HRMS) and non-target screening (0 features using LC-HRMS, 2 features using GC-HRMS). The compounds identified had log octanol/water partition coefficient (KOW) values from −9.9 to 16 and mass-to-charge ratios (m/z) of 68 to 761 (LC-HRMS and GC-HRMS). A significant linear trend was found between log KOW and m/z for the GC-HRMS data. Overall, these findings indicate that differences in screening results are mainly due to the data analysis workflows used by different participants. Further work is needed to harmonise the results obtained when applying suspect and non-target screening approaches to environmental biota samples.

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Av författaren/redakt...: Dürig, Wiebke; Lindblad, Sofia; Golovko, Oksana; Gkotsis, Georgio ...; Aalizadeh, Reza; Nika, Maria-Chri ...; visa fler...; Thomaidis, Nikol ...; Alygizakis, Niki ...; Plassmann, Merle ...; Haglund, Peter; Fu, Qiuguo; Hollender, Julia ...; Chaker, Jade; David, Arthur; Kunkel, Uwe; Macherius, André; Belova, Lidia; Poma, Giulia; Preud'Homme, Hug ...; Munschy, Catheri ...; Aminot, Yann; Jaeger, Carsten; Lisec, Jan; Hansen, Martin; Vorkamp, Katrin; Zhu, Linyan; Cappelli, France ...; Roscioli, Claudi ...; Valsecchi, Sara; Bagnati, Renzo; González, Belén; Prieto, Ailette; Zuloaga, Olatz; Gil-Solsona, Rub ...; Gago-Ferrero, Pa ...; Rodriguez-Mozaz, ...; Budzinski, Hélèn ...; Devier, Marie-He ...; Dierkes, Georg; Boulard, Lise; Jacobs, Griet; Voorspoels, Stef ...; Rüdel, Heinz; Ahrens, Lutz; visa färre...

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What is in the fish? Collaborative trial in suspect and non-target screening of organic micropollutants using LC- and GC-HRMS

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