| 1. |
- Cereser, Alberto, et al.
(författare)
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Time-of-Flight Three Dimensional Neutron Diffraction in Transmission Mode for Mapping Crystal Grain Structures
- 2017
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Ingår i: Scientific Reports. - : Springer Science and Business Media LLC. - 2045-2322. ; 7:1
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Tidskriftsartikel (refereegranskat)abstract
- The physical properties of polycrystalline materials depend on their microstructure, which is the nano- to centimeter scale arrangement of phases and defects in their interior. Such microstructure depends on the shape, crystallographic phase and orientation, and interfacing of the grains constituting the material. This article presents a new non-destructive 3D technique to study centimeter-sized bulk samples with a spatial resolution of hundred micrometers: time-of-flight three-dimensional neutron diffraction (ToF 3DND). Compared to existing analogous X-ray diffraction techniques, ToF 3DND enables studies of samples that can be both larger in size and made of heavier elements. Moreover, ToF 3DND facilitates the use of complicated sample environments. The basic ToF 3DND setup, utilizing an imaging detector with high spatial and temporal resolution, can easily be implemented at a time-of-flight neutron beamline. The technique was developed and tested with data collected at the Materials and Life Science Experimental Facility of the Japan Proton Accelerator Complex (J-PARC) for an iron sample. We successfully reconstructed the shape of 108 grains and developed an indexing procedure. The reconstruction algorithms have been validated by reconstructing two stacked Co-Ni-Ga single crystals, and by comparison with a grain map obtained by post-mortem electron backscatter diffraction (EBSD).
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| 2. |
- Holmberg, Jonas, 1976-, et al.
(författare)
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Residual stress state in an induction hardened steel bar determined by synchrotron- and neutron diffraction compared to results from lab-XRD
- 2016
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Ingår i: Materials Science & Engineering. - : Elsevier BV. - 0921-5093 .- 1873-4936. ; 667, s. 199-207
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Tidskriftsartikel (refereegranskat)abstract
- Induction hardening is a relatively rapid heat treatment method to increase mechanical properties of steel components. However, results from FE-simulation of the induction hardening process show that a tensile stress peak will build up in the transition zone in order to balance the high compressive stresses close to the surface. This tensile stress peak is located in the transition zone between the hardened zone and the core material. The main objective with this investigation has been to non-destructively validate the residual stress state throughout an induction hardened component. Thereby, allowing to experimentally confirming the existence and magnitude of the tensile stress peak arising from rapid heat treatment. For this purpose a cylindrical steel bar of grade C45 was induction hardened and characterised regarding the microstructure, hardness, hardening depth and residual stresses. This investigation shows that a combined measurement with synchrotron/neutron diffraction is well suited to non-destructively measure the strains through the steel bar of a diameter of 20 mm and thereby making it possible to calculate the residual stress profile. The result verified the high compressive stresses at the surface which rapidly changes to tensile stresses in the transition zone resulting in a large tensile stress peak. Measured stresses by conventional lab-XRD showed however that at depths below 1.5 mm the stresses were lower compared to the synchrotron and neutron data. This is believed to be an effect of stress relaxation from the layer removal. The FE-simulation predicts the depth of the tensile stress peak well but exaggerates the magnitude compared to the measured results by synchrotron/neutron measurements. This is an important knowledge when designing the component and the heat treatment process since this tensile stress peak will have great impact on the mechanical properties of the final component.
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| 3. |
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| 4. |
- Hörnqvist Colliander, Magnus, 1979, et al.
(författare)
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Early stages of spinodal decomposition in Fe-Cr resolved by in-situ small-angle neutron scattering
- 2015
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Ingår i: Applied Physics Letters. - : AIP Publishing. - 0003-6951 .- 1077-3118. ; 106:6
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Tidskriftsartikel (refereegranskat)abstract
- In-situ, time-resolved small-angle neutron scattering (SANS) investigations of the early stages of the spinodal decomposition process in Fe-35Cr were performed at 773 and 798K. The kinetics of the decomposition, both in terms of characteristic distance and peak intensity, followed a power-law behaviour from the start of the heat treatment (a' = 0.10-0.11 and a '' = 0.67-0.86). Furthermore, the method allows tracking of the high-Q slope, which is a sensitive measure of the early stages of decomposition. Ex-situ SANS and atom probe tomography were used to verify the results from the in-situ investigations. Finally, the in-situ measurement of the evolution of the characteristic distance at 773K was compared with the predictions from the Cahn-Hilliard-Cook model, which showed good agreement with the experimental data (a' = 0.12-0.20 depending on the assumed mobility).
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| 5. |
- Lopez-Crespo, P., et al.
(författare)
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Measuring overload effects during fatigue crack growth in bainitic steel by synchrotron X-ray diffraction
- 2015
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Ingår i: International Journal of Fatigue. - : Elsevier BV. - 1879-3452 .- 0142-1123. ; 71, s. 11-16
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Tidskriftsartikel (refereegranskat)abstract
- In this work we present the results of in situ synchrotron X-ray diffraction measurements of fatigue crack-tip strain fields following a 100% overload (OL) under plane strain conditions. The study is made on a bainitic steel with a high toughness and fine microstructure. This allowed a very high (60 mu m) spatial resolution to be achieved so that fine-scale changes occurring around the crack-tip were captured along the crack plane at the mid-thickness of the specimen. We have followed the crack as it grew through the plastic/residually stressed zone associated with the OL crack location. We observed two effects; one when the enhanced plastic zone is ahead of the crack and one after it has been passed. Regarding the former it was found that the compressive stress at the crack-tip initially falls sharply, presumably due to the increased plastic stretch caused by the OL. This is associated with a concomitant fall in peak tensile stress at K-max, the elastic excursion between K-min and K-max remaining essentially unchanged from before OL. Subsequently discontinuous closure as seen previously for plane stress caused by crack face contact at the OL location limits the elastic strain range experienced by the crack tip and thereby retards crack growth. (C) 2014 Elsevier Ltd. All rights reserved.
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| 6. |
- Lundbäck, Andreas, et al.
(författare)
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Modeling and Experimental Measurement with Synchrotron Radiation of Residual Stresses in Laser Metal Deposited Ti-6Al-4V
- 2016
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Ingår i: Proceedings of the 13th World Conference on Titanium. - Hoboken, NJ, USA : John Wiley & Sons, Inc.. - 9781119293668 - 9781119296126 ; , s. 1279-1282
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Konferensbidrag (refereegranskat)abstract
- There are many challenges in producing aerospace components by additive manufacturing (AM). One of them is to keep the residual stresses and deformations to a minimum. Another one is to achieve the desired material properties in the final component. A computer model can be of great assistance when trying to reduce the negative effects of the manufacturing process. In this work a finite element model is used to predict the thermo-mechanical response during the AM-process. This work features a physically based plasticity model coupled with a microstructure evolution model for the titanium alloy Ti -6Al-4V. Residual stresses in AM components were measured non-destructively using high-energy synchrotron X-ray diffraction on beam line ID15A at the ESRF, Grenoble. The results are compared with FE model predictions of residual stresses. During the process, temperatures and deformations was continuously measured. The measured and computed thermal history agrees well. The result with respect to the deformations agrees well qualitatively. Meaning that the change in deformation in each sequence is well predicted but there is a systematic error that is summing so that the quantitative agreement is lost.
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| 7. |
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| 8. |
- Lundbäck, Andreas, et al.
(författare)
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Modelling and Simulation of Metal Deposition on a Ti-6al-4v Plate
- 2015
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Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- There are many challenges in producing aerospace components by metal deposition (MD). One of them is to keep the residual stresses and deformations to a minimum. Anotherone is to achieve the desired material properties in the final component. A computer model can be of great assistance when trying to reduce the negative effects of the manufacturing process. In this work a finite element model is used to predict the thermo-mechanical response during the MD-process. This work features a pysically based plasticity model coupled with a microstructure evolution model for the titanium alloy Ti-6Al-4V. A thermally driven microstructure model is used to derive the evolution of the non-equilibrium compositions of α-phases and β-phase. Addition of material is done by activation of elements. The method is taking large deformations into consideration and adjusts the shape and position of the activated elements. This is particularilly important when adding material onto thin and flexible structures. The FE-model can be used to evaluate the effect of different welding sequenses. Validation of the model is performed by comparing measured deformations, strains, residual stresses and temperatures with the computed result. The deformations, strains and temepratures are measured during the process. The deformations are measured with a LVDT-gauge at one location. The strains are measured with a strain gauge at the same location as the deformations. The temperature is measured at five locations, close to the weld and with an increasing distance of one millimeter between each thermo couple. The residual stresses in MD component were measured non-destructively using high-energy synchrotron X-ray diffraction on beam line ID15A at the ESRF, Grenoble.
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| 9. |
- Maimaitiyili, Tuerdi, et al.
(författare)
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In situ hydrogen loading on zirconium powder
- 2015
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Ingår i: Journal of Synchrotron Radiation. - : International Union of Crystallography. - 1600-5775 .- 0909-0495. ; 22, s. 995-1000
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Tidskriftsartikel (refereegranskat)abstract
- For the first time, various hydride phases in a zirconium-hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were monitored in real time during hydrogenation and dehydrogenation, then whole pattern crystal structure analysis such as Rietveld and Pawley refinements were performed. All commonly reported low-pressure phases presented in the Zr-H phase diagram are obtained from a single experimental arrangement.
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| 10. |
- Olsson, C. -O. A., et al.
(författare)
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Strain Profiling of a Ferritic-Martensitic Stainless Steel Sheet - Comparing Synchrotron with Conventional X-Ray Diffraction
- 2015
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Ingår i: Strain. - : Wiley. - 0039-2103. ; 51:1, s. 71-77
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Tidskriftsartikel (refereegranskat)abstract
- To improve the fatigue resistance of stainless steel sheet, it is a common practice to induce compressive residual stress in the surface through shot-peening or tumbling. Stress depth profiles obtained by tumbling of thin stainless steel tensile rods were analysed using laboratory and synchrotron X-Ray Diffraction (XRD). Both the non-destructive synchrotron and the laboratory XRD etch-depth profile gave similar results: a residual stress profile decaying over a depth not exceeding 50 mu m into the material.
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