Sökning: L773:0749 1581 OR L773:1097 458X
> (1989) >
Complete 1H and 13C...
Complete 1H and 13C NMR spectral assignment of venturicidin A by 2D NMR spectroscopy
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- Gogoll, Adolf, 1957- (författare)
- Uppsala universitet,Organisk kemi I
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- Tanner, David (författare)
- Uppsala universitet,Organisk kemi
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(creator_code:org_t)
- 2005-04-12
- 1989
- Engelska.
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Ingår i: Magnetic Resonance in Chemistry. - : Wiley. - 0749-1581 .- 1097-458X. ; 27:9, s. 863-871
- Relaterad länk:
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Ämnesord
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- After correlation of the majority of signals by COSY and one-bond heteronuclear correlation, the complete assignment of the 1H and 13C NMR spectra of the macrolide antibiotic venturicidin A required the application of long-range CH coupling information. This was accessible by the COLOC-S and selective INEPT experiments, and the sensitivity of these experiments is discussed. Steric information was obtained from a NOESY spectrum, and the solution structure compared with that in the crystal.
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