| 1. |
- Lindberg, Siv M, et al.
(författare)
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A product semantic study of the influence of the sense of touch on the evaluation of wood-based materials
- 2013
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Ingår i: Materials & design. - : Elsevier BV. - 0264-1275 .- 1873-4197 .- 0261-3069. ; 52, s. 300-307
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Tidskriftsartikel (refereegranskat)abstract
- Based on product semantics, this study investigated how the tactile attributes of wood and wood-based composites are perceived and interpreted semantically. The wood-based samples included ash, birch, elm, oak, pine, OSB (oriented strand board), two wood pulp-reinforced polylactide composites, Comp A and B and one wood-fiber reinforced polypropene composite, Comp C. The subjects rated the samples by the descriptive words natural, exclusive, eco-. friendly, rough, inexpensive, reliable, warm, modern, snug and solid. The most significant differences between the samples were found for roughness and for the descriptors, reliable, natural and solid. A principal component analysis yielded three attributes based on the tactile perceptions: reliable, old-. fashioned and smooth. The solid wood pieces were perceived as natural and oak was perceived as being exclusive. The composite materials presented a greater variation in terms of perceived attributes than the wood specimens.
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| 2. |
- Åkerfeldt, Maria, 1982, et al.
(författare)
-
Textile piezoelectric sensors – melt spun bi-component poly(vinylidene fluoride) fibres with conductive cores and poly(3,4-ethylene dioxythiophene)-poly(styrene sulfonate) coating as the outer electrode
- 2014
-
Ingår i: Fashion and Textiles. - : Springer Science and Business Media LLC. - 2198-0802. ; 1:1
-
Tidskriftsartikel (refereegranskat)abstract
- The work presented here addresses the outer electroding of a fully textile piezoelectric strain sensor, consisting of bi-component fibre yarns of β-crystalline poly(vinylidene fluoride) (PVDF) sheath and conductive high density polyethylene (HDPE)/carbon black (CB) core as insertions in a woven textile, with conductive poly(3,4-ethylene dioxythiophene)-poly(styrene sulfonate) (PEDOT:PSS) coatings developed for textile applications. Two coatings, one with a polyurethane binder and one without, were compared for the application and evaluated as electrode material in piezoelectric testing, as well as tested for surface resistivity, tear strength, abrasion resistance and shear flexing. Both coatings served their function as the outer electrodes in the system and no difference in this regard was detected between them. Omission of the binder resulted in a surface resistivity one order of magnitude less, of 12.3 Ω/square, but the surface resistivity of these samples increased more upon abrasion than the samples coated with binder. The tear strength of the textile coated with binder decreased with one third compared to the uncoated substrate, whereas the tear strength of the coated textile without binder increased with the same amount. Surface resistivity measurements and scanning electron microscopy (SEM) images of the samples subjected to shear flexing showed that the coatings without the binder did not withstand this treatment, and that the samples with the binder managed this to a greater extent. In summary, both of the PEDOT:PSS coatings could be used as outer electrodes of the piezoelectric fibres, but inclusion of binder was found necessary for the durability of the coating.
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| 3. |
- Xu, Jinghao, et al.
(författare)
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Short-term creep behavior of an additive manufactured non-weldable Nickel-base superalloy evaluated by slow strain rate testing
- 2019
-
Ingår i: Acta Materialia. - : Elsevier BV. - 1359-6454 .- 1873-2453. ; 179, s. 142-157
-
Tidskriftsartikel (refereegranskat)abstract
- Additive manufacturing (AM) of high γ′ strengthened Nickel-base superalloys, such as IN738LC, is of high interest for applications in hot section components for gas turbines. The creep property acts as the critical indicator of component performance under load at elevated temperature. However, it has been widely suggested that the suitable service condition of AM processed IN738LC is not yet fully clear. In order to evaluate the short-term creep behavior, slow strain rate tensile (SSRT) tests were performed. IN738LC bars were built by laser powder-bed-fusion (L-PBF) and then subjected to hot isostatic pressing (HIP) followed by the standard two-step heat treatment. The samples were subjected to SSRT testing at 850 °C under strain rates of 1 × 10−5/s, 1 × 10−6/s, and 1 × 10−7/s. In this research, the underlying creep deformation mechanism of AM processed IN738LC is investigated using the serial sectioning technique, electron backscatter diffraction (EBSD), transmission electron microscopy (TEM). On the creep mechanism of AM polycrystalline IN738LC, grain boundary sliding is predominant. However, due to the interlock feature of grain boundaries in AM processed IN738LC, the grain structure retains its integrity after deformation. The dislocation motion acts as the major accommodation process of grain boundary sliding. Dislocations bypass the γ′ precipitates by Orowan looping and wavy slip. The rearrangement of screw dislocations is responsible for the formation of subgrains within the grain interior. This research elucidates the short-creep behavior of AM processed IN738LC. It also shed new light on the creep deformation mechanism of additive manufactured γ′ strengthened polycrystalline Nickel-base superalloys.
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| 4. |
- Grolig, Jan Gustav, 1986
(författare)
-
Coated Ferritic Stainless Steels as Interconnects in Solid Oxide Fuel Cells - Material Development and Electrical Properties
- 2015
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Solid oxide fuel cells (SOFCs) are attracting increasing interest as devices with potentialuses in decentralized and clean electricity and heat production. Several challengeswith respect to materials have to be overcome to achieve efficiencies and life-spansthat are sufficient for long-term applications.An important element of an SOFC stack is the interconnect component, which connectstwo adjacent fuel cell elements. Interconnects, which are commonly composedof ferritic stainless steels, have to be corrosion-resistant, mechanically stable and costoptimized.This work aimed to investigate economic solutions for interconnect materials and tounderstand the underlying mechanisms of degradation and electrical conduction ofthese materials. Mainly two substrates, a commercially available steel (AISI 441) anda ferritic stainless steel that was optimized for an SOFC application (Sandvik SanergyHT) were combined with different barrier coatings and exposed to a cathode-sideatmosphere. A method was developed that allows for the electrical characterizationof promising material systems and model alloys, thereby facilitating a fundamentalunderstanding of the dominant electrical conduction processes linked to the oxidescales that grow on interconnects. The AISI 441 steel coated with reactive elementsand cobalt showed good corrosion and chromium evaporation profiles, while AISI 441coated with cerium and cobalt also had promising electrical properties. The SanergyHT steel was examined with coatings of copper and iron and copper and manganese,respectively. The corrosion and chromium evaporation profiles of Sanergy HT wereimproved by coating with copper and iron. The copper and iron-coated Sanergy HTshowed lower area specific resistance values than cobalt-coated Sanergy HT. Chromia,which is the main constituent of oxide scales, was synthesized using differentmethods. The electrical properties of chromia were found to be sensitive to not onlyimpurities, but also heat treatment. Finally the electrical properties of cobalt- andcobalt cerium-coated Sanergy HT steels were investigated. It was revealed that theaddition of cerium improved the conductivity of the interconnect by both slowingdown chromia growth and preventing the outward diffusion of iron into the spinel.
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| 5. |
- Chen, Zhe, et al.
(författare)
-
Nano-scale characterization of white layer in broached Inconel 718
- 2017
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Ingår i: Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing. - Amsterdam : Elsevier BV. - 0921-5093 .- 1873-4936. ; 684, s. 373-384
-
Tidskriftsartikel (refereegranskat)abstract
- The formation mechanism of white layers during broaching and their mechanical properties are not well investigated and understood to date. In the present study, multiple advanced characterization techniques with nano-scale resolution, including transmission electron microscopy (TEM), transmission Kikuchi diffraction (TKD), atom probe tomography (APT) as well as nano-indentation, have been used to systematically examine the microstructural evolution and corresponding mechanical properties of a surface white layer formed when broaching the nickel-based superalloy Inconel 718.TEM observations showed that the broached white layer consists of nano-sized grains, mostly in the range of 20–50 nm. The crystallographic texture detected by TKD further revealed that the refined microstructure is primarily caused by strong shear deformation. Co-located Al-rich and Nb-rich fine clusters have been identified by APT, which are most likely to be γ′ and γ′′ clusters in a form of co-precipitates, where the clusters showed elongated and aligned appearance associated with the severe shearing history. The microstructural characteristics and crystallography of the broached white layer suggest that it was essentially formed by adiabatic shear localization in which the dominant metallurgical process is rotational dynamic recrystallization based on mechanically-driven subgrain rotations. The grain refinement within the white layer led to an increase of the surface nano-hardness by 14% and a reduction in elastic modulus by nearly 10% compared to that of the bulk material. This is primarily due to the greatly increased volume fraction of grain boundaries, when the grain size was reduced down to the nanoscale.
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| 6. |
- Goel, Sneha, 1993-, et al.
(författare)
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Effect of post-treatments under hot isostatic pressure on microstructural characteristics of EBM-built Alloy 718
- 2019
-
Ingår i: Additive Manufacturing. - : Elsevier BV. - 2214-8604 .- 2214-7810. ; 28, s. 727-737
-
Tidskriftsartikel (refereegranskat)abstract
- Electron beam melting (EBM) has emerged as an important additive manufacturing technique. In this study, Alloy 718 produced by EBM was investigated in as-built and post-treated conditions for microstructural characteristics and hardness. The post-treatments investigated were hot isostatic pressing (HIP) and combined HIP + heat treatment (HIP + HT) carried out as a single cycle inside the HIP vessel. Both the post-treatments resulted in significant decrease in defects inevitably present in the as-built material. The columnar grain structure of the as-built material was found to be maintained after post-treatment, with some sporadic localized grain coarsening noted. Although HIP led to complete dissolution of δ and γ′′ phase, stable NbC and TiN (occasionally present) particles were observed in the post-treated specimens. Significant precipitation of γ′′ phase was observed after HIP + HT, which was attributed to the two-step aging heat treatment carried out during HIP + HT. The presence of γ′′ phase or otherwise was correlated to the hardness of the material. While the HIP treatment resulted in drop in hardness, HIP + HT led to ‘recovery’ of the hardness to values exceeding those exhibited by the as-built material.
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| 7. |
- Goel, Sneha, 1993-, et al.
(författare)
-
The Effect of Location and Post-treatment on the Microstructure of EBM-Built Alloy 718
- 2018
-
Ingår i: Proceedings of the 9th International Symposium on Superalloy 718 & Derivatives. - Cham : Springer. - 2367-1696 .- 2367-1181. - 9783319894799 - 9783319894805 ; , s. 115-129
-
Konferensbidrag (refereegranskat)abstract
- Additive manufacturing (AM) of Ni-based superalloys such as Alloy 718 may obviate the need for difficult machining and welding operations associated with geometrically intricate parts, thus potentially expanding design possibilities and facilitating cost-effective manufacture of complex components. However, processing AM builds completely free from defects, which may impair mechanical properties such as fatigue and ductility, is challenging. Anisotropic properties, microstructural heterogeneities and local formation of undesired phases are additional concerns that have motivated post-treatment of AM builds. This work investigates the microstructural changes associated with post-treatment of Alloy 718 specimens produced by Electron Beam Melting (EBM) for as-built microstructures at 3 build heights: near base plate, in the middle of build and near the top of the build. Two different post-treatment conditions, hot isostatic pressing (HIP) alone and a combined HIP with solutionising and two-step aging were examined and compared to the results for the as-built condition. The influence of various post-treatments on minor phase distributions (δ, γ″, carbides), overall porosity, longitudinal grain widths and Vickers microhardness was considered. The HIP treatment led to significant reduction in overall porosity and dissolution of δ phase, which led to appreciable grain growth for both post-treatment conditions. The variation in hardness noted as a function of build height for the as-built specimens was eliminated after post-treatment. Overall, the hardness was found to decrease after HIP and increase after the full HIP, solutionising and aging treatment, which was attributed to dissolution of γ″ during HIP and its re-precipitation in subsequent heat treatment steps.
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| 8. |
- Jaladurgam, Nitesh Raj, 1993
(författare)
-
Heterogeneous deformation of multi-phase engineering materials - an in-situ neutron diffraction study
- 2019
-
Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Gas turbines are complex power generation systems used in aerospace or land-based-power stations. Materials such as Ni-base superalloys are involved in the combustion zone of these machines, which continuously experiences harsh environments with loading at high temperatures. Moreover, the continuous demand for increasing operating temperature to achieve higher efficiencies and reduced emission levels opens the scene to new heat resistant materials like the state-of-the-art high entropy alloys (HEAs), which require a thorough understanding of the structure-process-property relationships. The microstructures of these advanced multi-phase, multi-component alloys are complex, and the deformation is generally heterogeneous both with respect to the different phases and to the crystallographic orientation within each phase. Hence, it is important to understand their behavior and performance during processing and service. In-situ neutron diffraction is a unique technique to probe the deformation behaviour during service/processing-like conditions, including plastic deformation at various temperatures, in order to provide insights into the structure-property relations. In the first part of this work the deformation mechanisms of a newly developed Ni-base superalloy was investigated using in-situ neutron diffraction and electron microscopy at room temperature. In addition, elasto-plastic self-consistent (EPSC) crystal plasticity simulations are used to obtain insights into the operating deformation mechanisms. In the second part, the as-cast eutectic high entropy alloy AlCoCrFeNi2.1 was studied using in-situ neutron diffraction at temperatures from 77 to 673 K. These investigations provide unique insights into the complex heterogeneous deformation behavior of these high-performance multi-phase engineering materials.
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| 9. |
- Åkerfeldt, Pia, et al.
(författare)
-
Electron backscatter diffraction characterization of fatigue crack growth in laser metal wire deposited Ti-6Al-4V
- 2018
-
Ingår i: Materials Characterization. - : Elsevier BV. - 1044-5803 .- 1873-4189. ; 135, s. 245-256
-
Tidskriftsartikel (refereegranskat)abstract
- By additive manufacturing (AM) there is a feasibility of producing near net shape components in basically one step from 3D CAD model to final product. The interest for AM is high and during the past decade a lot of research has been carried out in order to understand the influence from process parameters on the microstructure and furthermore on the mechanical properties. In the present study laser metal wire deposition of Ti-6Al-4V has been studied in detail with regard to its fatigue crack propagation characteristics. Two specimen orientations, parallel and perpendicular to the deposition direction, have been evaluated at room temperature and at 250 °C. No difference in the fatigue crack growth rate could be confirmed for the two specimen orientations. However, in the fractographic study it was observed that the tortuosity varied between certain regions on the fracture surface. The local crack path characteristic could be related to the alpha colony size and/or the crystallographic orientation. Moreover, large areas exhibiting similar crystallographic orientation were observed along the prior beta grain boundaries, which were attributed to the wide alpha colonies frequently observed along the prior beta grain boundaries. © 2017 Elsevier Inc.
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| 10. |
- Banerjee, Debashree, et al.
(författare)
-
Elevated thermoelectric figure of merit of n-type amorphous silicon by efficient electrical doping process
- 2018
-
Ingår i: Nano Energy. - : Elsevier BV. - 2211-2855 .- 2211-3282. ; 44, s. 89-94
-
Tidskriftsartikel (refereegranskat)abstract
- The currently dominant thermoelectric (TE) materials used in low to medium temperature range contain Tellurium that is rare and mild-toxic. Silicon is earth abundant and environment friendly, but it is characterized by a poor TE efficiency with a low figure of merit, ZT. In this work, we report that ZT of amorphous silicon (a-Si) thin films can be enhanced by 7 orders of magnitude, reaching ∼0.64 ± 0.13 at room temperature, by means of arsenic ion implantation followed by low-temperature dopant activation. The dopant introduction employed represents a highly controllable doping technique used in standard silicon technology. It is found that the significant enhancement of ZT achieved is primarily due to a significant improvement of electrical conductivity by doping without crystallization so as to maintain the thermal conductivity and Seebeck coefficient at the level determined by the amorphous state of the silicon films. Our results open up a new route towards enabling a-Si as a prominent TE material for cost-efficient and environment-friendly TE applications at room temperature.
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| 11. |
- Wójcik, Natalia A., et al.
(författare)
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The influence of Be addition on the structure and thermal properties of alkali-silicate glasses
- 2019
-
Ingår i: Journal of Non-Crystalline Solids. - : Elsevier BV. - 0022-3093 .- 1873-4812. ; 521
-
Tidskriftsartikel (refereegranskat)abstract
- Be-Na-(Li)-Si oxide glasses containing up to 15 mol% of BeO were prepared. Their structure was characterized by X-ray powder diffraction and Raman as well as infrared spectroscopic techniques, while their chemical compositions were examined by Inductively Coupled Plasma Optical Emission Spectrometry. All materials were found to be amorphous and contain Al contaminations from minor dissolution of the alumina crucibles. The results of Raman and IR spectroscopies showed that BeO addition to Na-(Li)-Si glass systems resulted in the formation of [BeO4/2](2-) tetrahedra which are inserted into the silicate glass network, demonstrating the intermediate glass-forming role of BeO. In parallel, the effective destruction of Si-O-Si bridges was observed by vibrational spectroscopy. The glass transition temperature was studied by Differential Thermal Analysis and found to range from about 431 degrees C to 551 degrees C. A significant increase in T-g by 70 degrees C was found as SiO2 was substituted by up to 15 mol% BeO.
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| 12. |
- Krakhmalev, Pavel, 1973-, et al.
(författare)
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Microstructure, solidification texture, and thermal stability of 316 L stainless steel manufactured by laser powder bed fusion
- 2018
-
Ingår i: Metals. - : MDPI AG. - 2075-4701. ; 8:8, s. 1-18
-
Tidskriftsartikel (refereegranskat)abstract
- This article overviews the scientific results of the microstructural features observed in 316 L stainless steel manufactured by the laser powder bed fusion (LPBF) method obtained by the authors, and discusses the results with respect to the recently published literature. Microscopic features of the LPBF microstructure, i.e., epitaxial nucleation, cellular structure, microsegregation, porosity, competitive colony growth, and solidification texture, were experimentally studied by scanning and transmission electron microscopy, diffraction methods, and atom probe tomography. The influence of laser power and laser scanning speed on the microstructure was discussed in the perspective of governing the microstructure by controlling the process parameters. It was shown that the three-dimensional (3D) zig-zag solidification texture observed in the LPBF 316 L was related to the laser scanning strategy. The thermal stability of the microstructure was investigated under isothermal annealing conditions. It was shown that the cells formed at solidification started to disappear at about 800 °C, and that this process leads to a substantial decrease in hardness. Colony boundaries, nevertheless, were quite stable, and no significant grain growth was observed after heat treatment at 1050 °C. The observed experimental results are discussed with respect to the fundamental knowledge of the solidification processes, and compared with the existing literature data.
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| 13. |
- Saarimäki, Jonas, et al.
(författare)
-
3D Residual Stresses in Selective Laser Melted Hastelloy X
- 2017
-
Ingår i: Residual Stresses 2016: ICRS-10, Materials Research Proceedings 2 (2016). - : Materials Research Forum LLC. ; , s. 73-78
-
Konferensbidrag (refereegranskat)abstract
- 3D residual stresses in as manufactured EOS NickelAlloy HX, produced by laser powder bed additive manufacturing, are analysed on the surface closest to the build-plate. Due to the severe thermal gradient produced during the melting and solidification process, profound amounts of thermal strains are generated. Which can result in unwanted geometrical distortion and effect the mechanical properties of the manufactured component. Measurements were performed using a four-circle goniometer Seifert X-ray machine, equipped with a linear sensitive detector and a Cr-tube. Evaluation of the residual stresses was conducted using sin2ψ method of the Ni {220} diffraction peak, together with material removal technique to obtain in-depth profiles. An analysis of the material is reported. The analysis reveals unwanted residual stresses, and a complicated non-uniform grain structure containing large grains with multiple low angle grain boundaries together with nano-sized grains. Grains are to a large extent, not equiaxed, but rather elongated.
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| 14. |
- André, Benny
(författare)
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Nanocomposites for Use in Sliding Electrical Contacts
- 2011
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- In this thesis nanocomposite materials for use in high performance electrical contacts are tested. Self mating silver as coatings on cupper substrates are the most used material combination in power connectors today. In this work two new concepts were tested. The first one was to change one of the mating surfaces to a hard thin coating and keep the other surface made of silver. Tested coatings were nanocomposites with hard carbides in a matrix of amorphous carbon. TiC/a-C and Ti-Ni-C/a-C were tested both electrically and tribologically. The total amount of carbon and the amount of carbon matrix was important, both for the electrical and the tribological properties. The Ti-Ni-C coating also showed that substituting Ti in TiC with the weak carbide former Ni changed the stability of the carbides. The substitution resulted in more a-C matrix and less C in the carbides. Thin coatings of nc-TiC/a-C and Ti-Ni-C/a-C showed high potential as material candidates for use in electrical contacts. The other tested concept was to modify the used silver instead of replacing it. This was done by embedding nanoparticles of solid lubricant IF-WS2 in the silver. The results from reciprocating sliding displayed low friction and high wear resistance. The modified silver surfaces lasted for 8000 strokes with a friction of about 0.3 while at the same time allowing for a low contact resistance. The results for surfaces of pure silver coating displayed a friction of 0.8-1.2 and that the silver was worn through already after 300 strokes. A new method to investigate inherent hardness and residual stress of thin coatings, on complex geometries or in small areas, was also developed. An ion beam was used to create stress free coating as free standing micro pillars. Hardness measured on the pillars and on as-deposited coating were then used to calculate the residual stress in the coatings.
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| 15. |
- Chasoglou, Dimitris, 1982, et al.
(författare)
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Effect of reducing agents on the sintering of chromium alloyed PM steels
- 2013
-
Ingår i: Proceedings EURO PM2013 Congress & Exhibition, 15-18 September 2013, Gothenburg, Sweden. - : European Powder Metallurgy Association (EPMA). ; 2, s. 297-302
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Konferensbidrag (refereegranskat)abstract
- The control of the surface chemistry during sintering is the key factor for the successful and efficientproduction of PM parts, especially for powders containing elements with high affinity to oxygen such as chromium.The effect of different reducing agents was investigated by performing sintering trials on water atomized steel powder pre-alloyed with 3 wt.% Cr with and without the addition of graphite as well as using atmospheres with varying hydrogen content. The use of thermal analysis and photoacoustic spectroscopy in combination with results from fractographic investigation showed that oxide reduction is enhanced with the presence of hydrogen even if the main reduction mechanism is the carbothermal reactions. Oxides rich in Cr, Mn and Si were formed during sintering for all appliedconditions. The findings are summarized in a simple model describing the enclosure of oxides during the sinter-neckdevelopment and the changes in surface chemistry during the process.
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| 16. |
- Chasoglou, Dimitris, 1982, et al.
(författare)
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Optimisation of sintering atmospheres for controlled sintering of PM steels
- 2013
-
Ingår i: Proceedings EURO PM2013 Congress & Exhibition, 15-18 September 2013, Gothenburg, Sweden. - : European Powder Metallurgy Association (EPMA). ; 2, s. 339-346
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Konferensbidrag (refereegranskat)abstract
- The use of elements with high oxygen affinity such as Cr or Mn in PM steels has been met with skepticism although such grades are attractive options for structural applications. They require strict control of the used atmosphere during the sintering process. Various techniques such asphotoacoustic spectroscopy (PAS) and continuous CO/CO2/H2O measurements have been implemented for atmosphere monitoring during sintering trials of Cr-alloyed steel powder. The used atmospheres were nitrogen-hydrogen blends (0,3,10 and 100% H2) as well as vacuum. The progress of the oxidation/reduction processes was also followed with thermogravimetric studies. The pressed and sintered samples were examined using optical and electron microscopy in combination with EDX in order to evaluate the formed reaction products. The presence of hydrogen, even in smallamounts, is positive for the oxide reduction. Results show that careful adjustment of the used atmosphere leads to efficient production of steel components based on Cr -prealloyed powders.
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| 17. |
- Chen, Zhe, et al.
(författare)
-
Surface Integrity and Structural Stability of Broached Inconel 718 at High Temperatures
- 2016
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Ingår i: Metallurgical and Materials Transactions. A. - : Springer. - 1073-5623 .- 1543-1940. ; 47A:7, s. 3664-3676
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Tidskriftsartikel (refereegranskat)abstract
- The current study focused on the surface integrity issues associated with broaching of Inconel 718 and the structural stability of the broached specimen at high temperatures, mainly involving the microstructural changes and residual stress relaxation. The broaching operation was performed using similar cutting conditions as that used in turbo machinery industries for machining fir-tree root fixings on turbine disks. Thermal exposure was conducted at 723 K, 823 K, and 923 K (450 A degrees C, 550 A degrees C, and 650 A degrees C) for 30, 300, and 3000 hours, respectively. Surface cavities and debris dragging, sub-surface cracks, high intensity of plastic deformation, as well as the generation of tensile residual stresses were identified to be the main issues in surface integrity for the broached Inconel 718. When a subsequent heating was applied, surface recrystallization and alpha-Cr precipitation occurred beneath the broached surface depending on the applied temperature and exposure time. The plastic deformation induced by the broaching is responsible for these microstructural changes. The surface tension was completely relaxed in a short time at the temperature where surface recrystallization occurred. The tensile layer on the sub-surface, however, exhibited a much higher resistance to the stress relief annealing. Oxidation is inevitable at high temperatures. The study found that the surface recrystallization could promote the local Cr diffusion on the broached surface.
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| 18. |
- Cho, Sung-Woo, et al.
(författare)
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Injection-molded nanocomposites and materials based on wheat gluten
- 2011
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Ingår i: International Journal of Biological Macromolecules. - : Elsevier BV. - 0141-8130 .- 1879-0003. ; 48:1, s. 146-152
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Tidskriftsartikel (refereegranskat)abstract
- This is, to our knowledge, the first study of the injection molding of materials where wheat gluten (WG) is the main component. In addition to a plasticizer (glycerol), 5 wt.% natural montmorillonite clay was added. X-ray indicated intercalated clay and transmission electron microscopy indicated locally good clay platelet dispersion. Prior to feeding into the injection molder, the material was first compression molded into plates and pelletized. The filling of the circular mold via the central gate was characterized by a divergent flow yielding, in general, a stronger and stiffer material in the circumferential direction. It was observed that 20–30 wt.% glycerol yielded the best combination of processability and mechanical properties. The clay yielded improved processability, plate homogeneity and tensile stiffness. IR spectroscopy and protein solubility indicated that the injection molding process yielded a highly aggregated structure. The overall conclusion was that injection molding is a very promising method for producing WG objects.
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| 19. |
- Dimitrios, Nikas, et al.
(författare)
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Evaluation of local strength via microstructural quantification in a pearlitic rail steel deformed by simultaneous compression and torsion
- 2018
-
Ingår i: Materials Science & Engineering. - : Elsevier. - 0921-5093 .- 1873-4936. ; 737, s. 341-347
-
Tidskriftsartikel (refereegranskat)abstract
- Pearlitic steels are commonly used for railway rails because they combine good strength and wear properties. During service, the passage of trains results in large accumulation of shear strains in the surface layer of the rail, sometimes leading to crack initiation. Knowledge of the material properties versus the shear strain in this layer is therefore important for fatigue life predictions. In this study, fully pearlitic R260 rail steel was deformed using a bi-axial torsion-compression machine to reach different shear strains. Microstructural parameters including interlamellar spacing, thickness of ferrite and cementite lamellae and dislocation density in the ferrite lamellae, as well as hardness were quantitatively characterized at different shear strain levels. Based on the microstructural observations and the quantification of the microstructural parameters, the local flow stresses were estimated based on boundary strengthening and dislocation strengthening models. A good agreement was found between the estimated flow stresses and the flow stresses determined from microhardness measurements. d
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| 20. |
- Dimitrios, Nikas, et al.
(författare)
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Mechanical properties and fatigue behavior of railway wheel steels as influenced by mechanical and thermal loadings
- 2015
-
Ingår i: CM 2015 - 10th International Conference on Contact Mechanics of Wheel / Rail Systems. - : International Conference on Contact Mechanics of Wheel / Rail Systems. ; 366:SI, s. 407-415
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Konferensbidrag (refereegranskat)abstract
- In the current work the deterioration of mechanical properties of railway wheel steels (UIC ER7T and ER8T) is in focus. These are medium carbon steels (∼0.55 wt.% C) heat treated to a near pearlitic microstructure with some 5-10% pro-eutectoid ferrite. During operation of trains, high thermal loads are evolved because of recurring acceleration, braking, curving and occasional slippage. It is thus relevant to examine the high temperature performance of wheel material and evaluate the decrease in strength after thermal exposure as well as the degradation of fatigue properties. Samples were extracted from virgin wheels and pre-strained to around 6.5% strain as well as cyclically deformed, to also account for the change in properties that is induced by plastic deformation inherent in the wheel tread surface. Both un-deformed and pre-strained material was heat treated for different times in the temperature range of interest, from 250°C to 600-700°C. Hardening was observed in both conditions around 300°C followed by softening at higher temperatures. Spheroidization of the pearlite started to become visible at 450°C for the un-deformed material and at around 400°C for the pre-strained.
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| 21. |
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| 22. |
- He, Wenxiao, 1985
(författare)
-
Biomimetic Formation of Calcium Phosphate Based Nanomaterials
- 2014
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- The intercellular material in bone is a nanocomposite of aligned “hard” inorganics—calcium phosphate (CaP) platelets embedded in the long-range ordered “soft” organic collagen matrix. This elaborate structural arrangement redeems the weaknesses of the individual components (being soft protein or brittle mineral) and gives bone its excellent mechanical properties for the protection and support of our bodies. The structural order and hierarchy in the soft matrix is organized via self-assembly of collagen molecules and is reinforced by intermolecular crosslinking. The subsequent growth of “hard” crystallites inside the “soft” matrix compartments, likely through the deposition of a transient amorphous calcium phosphate (ACP) phase, results in the interpenetrated composite structure.The aim of this thesis was to prepare synthetic mimetics of “hard” material (CaP) with well-defined nanostructures, soft organic matrices with long-range order and interpenetrated composites composing of the two. The work was inspired by the material deposition process in natural bone. Lyotropic liquid crystal (LC) phases self-assembled by block copolymers were used to mimic the structural order of the collagen matrix. Both the inorganic morphogenesis of CaP in LCs and the controlled crystallization of ACP were investigated. To explore ordered organic matrices, crosslinking of the LCs and the self-assembly of an amphiphilic peptide with designed sequence were performed. In addition, controlled mineralization within crosslinked LCs was examined for the formation of nanocomposites.ACP nanospheres, CaP nanowires and nanosheets were prepared from LCs via templated growth. The ACP nanospheres were capable of transforming into bone-like apatite by controlled aging in water and the prepared nanoparticles were shown to affect osteoblast gene expression. Dicalcium phosphate crystals (brushite and monetite) with structural hierarchy and distinct features were also grown in LCs through epitaxial overgrowth or a self-organization regime. Polymerized LCs were successfully prepared from a modified block copolymer (diacrylate derivative of Pluronic® F127), which served as a resilient matrix for the deposition of ACP nanospheres. A subsequent in situ crystallization of ACP into bone-like apatite resulted in mechanically stable composites retaining nanostructures that resembled that of natural bone. An amphiphilic peptide was designed using mainly natural amino acids and it was shown to self-assemble into distinct structures at different concentrations. Based upon the results presented in this thesis, nanomaterials with assorted structures can be further designed for bio-related applications.
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| 23. |
- Hedström, Peter, et al.
(författare)
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Load partitioning between single bulk grains in a two-phase duplex stainless steel during tensile loading
- 2010
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Ingår i: Acta Materialia. - : Elsevier BV. - 1359-6454 .- 1873-2453. ; 58:2, s. 734-744
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Tidskriftsartikel (refereegranskat)abstract
- The lattice strain tensor evolution for single bulk grains of austenite and ferrite in a duplex stainless steel during tensile loading to 0.02 applied strain has been investigated using in situ high-energy X-ray measurements and finite-element modeling. Single-grain X-ray diffraction lattice strain data for the eight austenite and seven ferrite grains measured show a large variation of residual lattice strains, which evolves upon deformation to the point where some grains with comparable crystallographic orientations have lattice strains different by 1.5 x 10(-3), corresponding to a stress of similar to 300 MPa. The finite-element simulations of the 15 measured grains in three different spatial arrangements confirmed the complex deformation constraint and importance of local grain environment.
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| 24. |
- Hosseini, Seyed, 1981, et al.
(författare)
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Characterization of the Surface Integrity induced by Hard Turning of Bainitic and Martensitic AISI 52100 Steel
- 2012
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Ingår i: Procedia CIRP. - : Elsevier BV. - 2212-8271. ; 1:1, s. 494 - 499
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Konferensbidrag (refereegranskat)abstract
- Depending on the process parameters and the tool condition, hard turned surfaces can consist of a “white” and a “dark” etching layer having other mechanical properties compared to the bulk material. X-ray diffraction measurements revealed that tensileresidual stresses accompanied with higher volume fraction of retained austenite are present in the thermally induced white layer. While compressive residual stresses and decreased retained austenite content was found in the plastically created white layer. The surface temperature was estimated to be ~1200 C during white layer formation by hard turning.
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| 25. |
- Hryha, Eduard, 1980, et al.
(författare)
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Carbon Control in PM Sintering: Industrial Applications and Experience so Far
- 2012
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Ingår i: Proc. of EURO PM2012 Congress & Exhibition, 16-19 September 2012, Basel, Switzerland. - 9781899072231 ; 1, s. 265-270
-
Konferensbidrag (refereegranskat)abstract
- Challenges in controlling carbon potential during sintering of steel powder have been discussed in many experimental and theoretical studies. The main issues lie within the complex thermodynamics and kinetics of processing atmosphere chemistry in continuous sintering furnaces. Although many models have tried to address the problem, many of these have rarely come to reality and become an industrial practice.The purpose of this article is to summarize these discussions and investigate the interaction of the atmosphere constituents with the sintered compact within a sintering furnace. Considering an industrial practice perspective, the paper ensures the PM Industry with a fresh new look into the understanding of the furnace operations and provides recommendations to improve the control of the furnace conditions. As an example, existing furnace installation utilizing Linde SINTERFLEX technology allows monitor and/or control the furnace atmosphere. Article describes reduction of oxides and carbon potentials to enable optimization of the production parameters.
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| 26. |
- Hryha, Eduard, 1980, et al.
(författare)
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Influence of the Steel Powder Type and Processing Parameters on the Debinding of PM Compacts with Gelatin Binder
- 2014
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Ingår i: Journal of Thermal Analysis and Calorimetry. - : Springer Science and Business Media LLC. - 1388-6150 .- 1588-2926. ; 118:2, s. 695-704
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Tidskriftsartikel (refereegranskat)abstract
- Binders present an important part of the powder metallurgy technology as they are vital to provide efficient powder agglomeration and/or lubrication during shaping. At the same time, they have to be easily removed from the compacts during initial stages of sintering without any harmful effect for the base material, as well as for the environment. Therefore, behavior of gelatin as a binder for stainless- and tool-steel gas-atomised powder compacts was studied by thermal analysis and electron microscopy. Thermal analysis showed that peak mass-loss occurred in the range between 340 and 370 C, depending on the base powder and heating rate. Risk for base powder oxidation at temperatures below 425 C was detected. Based on the obtained results, it is recommended to perform debinding at *425 C after applying a heating rate of around 7.5 C min-1. Only in this way efficient enough binder removal can be obtained concurrently to avoiding base powder oxidation.
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| 27. |
- Hryha, Eduard, 1980, et al.
(författare)
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Process Control System for Delubrication of PM Steels
- 2012
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Ingår i: Acta Metallurgica Slovaca. - 1335-1532 .- 1338-1156. ; 18:2-3, s. 60-68
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Tidskriftsartikel (refereegranskat)abstract
- Lubricants are important additive in powder metallurgy (PM) steels as they are needed to improve powder compressibility and reduce tool wear. Removal of the lubricant results in production of number of gas species that can have harmful effect on the base material. Current paper describes process gas monitoring system for delubrication control that is built on industrially available gas sensors. Experimental results indicate that accurate delubrication process control can be performed by utilizing only CO2 and O2 sensors. It is recommended to perform delubrication below 500°C in dry inert atmospheres in the case of modern ethylene bis stearamide based lubricants.
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| 28. |
- Huang, Shuo, et al.
(författare)
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Thermal Expansion, Elastic and Magnetic Properties of FeCoNiCu-Based High-Entropy Alloys Using First-Principle Theory
- 2017
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Ingår i: JOM. - : Springer. - 1047-4838 .- 1543-1851. ; 69:11, s. 2107-2112
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Tidskriftsartikel (refereegranskat)abstract
- The effects of V, Cr, and Mn on the magnetic, elastic, and thermal properties of FeCoNiCu high-entropy alloy are studied by using the exact muffin-tin orbitals method in combination with the coherent potential approximation. The calculated lattice parameters and Curie temperatures in the face-centered-cubic structure are in line with the available experimental and theoretical data. A significant change in the magnetic behavior is revealed when adding equimolar V, Cr, and Mn to the host composition. The three independent single-crystal elastic constants are computed using a finite strain technique, and the polycrystalline elasticity parameters including shear modulus, Young's modulus, Pugh ratio, Poisson's ratio, and elastic anisotropy are derived and discussed. The effects of temperature on the structural parameters are determined by making use of the Debye-Gruneisen model. It is found that FeCoNiCuCr possesses a slightly larger thermal expansion coefficient than do the other alloys considered here.
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| 29. |
- Hörnqvist Colliander, Magnus, 1979, et al.
(författare)
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High-temperature crack growth in a Ni-base superalloy during sustained load
- 2014
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Ingår i: Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing. - : Elsevier BV. - 0921-5093. ; 609, s. 131-140
-
Tidskriftsartikel (refereegranskat)abstract
- he high-temperature sustained load crack growth behaviour of a Ni-base superalloy was investigated using a combination of mechanical testing in controlled atmosphere, fractographical and microanalytical investigations, and finite element modelling. The results show that the local crack front geometry is un- even on two scales – jaggedness on the scale of 100 μm was observed in all specimens, whereas mm- scale waviness could occasionally be observed. The jaggedness can be explained by a percolation-type crack growth along weaker grain boundaries, whereas the large-scale waviness is presumably due to larger regions of the material having specific grain texture with high crack growth resistance. The un-even crack front is shown to potentially have considerable effects on the loading conditions at the crack tip, whereas ligaments of un-cracked material in the crack wake are deemed to have less effect on the crack tip loading due to their low area fraction. The ligaments fail intergranularly in the wake as the crack grows in the present case, as opposed to by creep fracture as previously proposed. Finally, the plastically deformed regions about the crack and crack tip are shown not to exhibit any elevated oxygen levels, implying that the damage in these regions is purely mechanical.
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| 30. |
- Joseph, Ceena, 1982, et al.
(författare)
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Anisotropy of Room Temperature Ductility in Haynes 282 Forgings
- 2014
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Ingår i: Proceedings of the 8th International Symposium on Superalloy 718 and Derivatives. - Hoboken, NJ, USA : John Wiley & Sons, Inc.. - 9781119016809 ; , s. 601-609
-
Konferensbidrag (refereegranskat)abstract
- Haynes 282 is relatively new nickel base superalloy, offering excellent mechanical properties and attracting interest from the gas turbine and aerospace industry. One of the criteria for meeting specification requirement is the room temperature ductility.Forgings of Haynes 282 show large anisotropy in ductility, varying from approximately 25% in longitudinal transverse (LT) to 12% in the short transverse(ST) direction. In this paper LT and ST specimens from forgings were tested for its room temperature ductility.Fractographic and metallographic analysis show the presence of MC and Mc6C carbide banding. Failure in both ST and LT direction was ductile with intergranular fracture, but in the ST direction the failure was preferentially due to cracking of carbides. The orientation of carbides in preferred direction and their excessive segregation affecting ductility in ST is discussed in this work.
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| 31. |
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| 32. |
- Meyer, Knut Andreas, 1990, et al.
(författare)
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Microstructure and mechanical properties of the running band in a pearlitic rail steel : Comparison between biaxially deformed steel and field samples
- 2018
-
Ingår i: Wear. - : Elsevier. - 0043-1648 .- 1873-2577. ; 396-397, s. 12-21
-
Tidskriftsartikel (refereegranskat)abstract
- The large deformations occurring in the surface layer of rail heads strongly influence the material behavior. Cracks typically develop from this critical region. However, conventional material testing of this layer is not possible due to the large gradients. A method for obtaining a similar material through predeformation is therefore investigated. Subsequent analyses of the obtained material can improve our understanding of the material behavior close to the running band. Hardness, shear lines and cementite lamella orientation distributions are compared in order to determine whether the obtained material is similar to that of the field samples extracted from rails that have been in service for several years. The predeformation method produces a consistent material, which is representative of the material in the rail field samples that have accumulated large shear strains.
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| 33. |
- Nikas, Dimitrios, 1984, et al.
(författare)
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High temperature bi-axial low cycle fatigue behaviour of railway wheel steel
- 2019
-
Ingår i: ICMFF12 - 12TH INTERNATIONAL CONFERENCE ON MULTIAXIAL FATIGUE AND FRACTURE. - : EDP Sciences. - 2261-236X. ; 300
-
Konferensbidrag (refereegranskat)abstract
- One of the most important aspects in railway operation is the interaction between rail and wheel. Railway wheels are commonly made from medium carbon steels (similar to 0.55 wt.% C), heat treated to a near pearlitic microstructure with some 5-10% pro-eutectoid ferrite. During the operation of freight trains, where block brakes are used, high thermal loads are evolved because of recurring braking and occasional slippage. Thus the combination of mechanical and thermal loads leads to changes in the mechanical properties of the material. The focus of the current investigation is to evaluate the mechanical behaviour of wheel material (UIC ER7T) subjected to non-proportional biaxial fatigue loading, as this simulates the actual working conditions in a better way than uniaxial loading. Axial-torsional low cycle fatigue tests were performed at room temperature and elevated temperatures using thin walled specimens to study the cyclic stress-strain properties of this material. The results showed large influence of temperature on the ratcheting behaviour of the material. Biaxial non-proportional loading gave much higher strain hardening as compared to uniaxial loading. Hardening due to dynamic strain ageing can be seen in the biaxial tests at temperatures around 300 degrees C.
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| 34. |
- Persson, Henrik, 1983, et al.
(författare)
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A simple way of improving graphite nanoplatelets (GNP) for their incorporation into a polymer matrix
- 2012
-
Ingår i: Express Polymer Letters. - : Department of Polymer Engineering, Scientific Society of Mechanical Engineering. - 1788-618X. ; 6:2, s. 142-147
-
Tidskriftsartikel (refereegranskat)abstract
- A simple method of solvent exfoliation/refining of direct-graphite nanoplatelets for their better incorporation into a polymer matrix is presented. We demonstrate the method for polystyrene. The method relies on sonication in N-methyl-2-pyrrolidone solvent, with surfactant assistance. A small amount of polystyrene is added to the solvent in order to increase the viscosity, this enhancing the exfoliation process and resulting in formation of a polymeric layer on graphene for its better incorporation in the polymer matrix. Polystyrene-coated thin graphene stacks form a stable dispersion, while thicker graphite nanoplatelets settle out. Thus bulk separation of thin and thick graphene stacks takes place.The polystyrene-coated thin graphene stacks are studied using Transmission Electron Microscopy in two ways: (i) we calculate the number of graphene layers forming thin graphene stacks, and (ii) we employ Selected Area Diffraction to confirm our image analysis results by checking the intensity ratio (1100) and (2100) deflections in the diffraction patterns. Five layers is found to be the cut-off number, that is there are no stacks >5 layers, and 3 layer stacks are dominantly present. The average largest in-plane dimension is found to be approximately 2.5 mu m (reduction by 50%).
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| 35. |
- Saarimäki, Jonas, et al.
(författare)
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Anisotropy effects during dwell-fatigue caused by δ-phase orientation in forged Inconel 718
- 2017
-
Ingår i: Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing. - : Elsevier BV. - 0921-5093 .- 1873-4936. ; 692, s. 174-181
-
Tidskriftsartikel (refereegranskat)abstract
- Inconel 718 is a commonly used superalloy for turbine discs in the gas turbine industry. Turbine discs are often subjected to dwell-fatigue as a result of long constant load cycles. The effect of anisotropy on dwell-fatigue cracking in forged turbine discs have not yet been thoroughly investigated. Crack propagation behaviour was characterised using compact tension (CT) samples cut in different orientations from a real turbine disc forging. Samples were also cut in two different thicknesses in order to investigate the influence of plane strain and plane stress condition on the crack propagation rates. The samples were subjected to dwell-fatigue tests at 550 °C with 90 s or 2160 s dwell-times at maximum load. Microstructure characterisation was done using scanning electron microscopy (SEM) techniques such as electron channelling contrast imaging (ECCI), electron backscatter diffraction (EBSD), and light optical microscopy (LOM). The forged alloy exhibits strong anisotropic behaviour caused by the non-random δ-phase orientation. When δ-phases were oriented perpendicular compared to parallel to the loading direction, the crack growth rates were approximately ten times faster. Crack growth occurred preferably in the interface between the γ-matrix and the δ-phase.
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| 36. |
- Yao, Yiming, 1957, et al.
(författare)
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Microstructure of plasma sprayed Al2O3-3wt%TiO2 coating using freeze granulated powder
- 2016
-
Ingår i: Journal of Materials Science and Chemical Engineering. - : Scientific Research Publishing, Inc.. - 2327-6045 .- 2327-6053. ; 4:7, s. 8-14
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Tidskriftsartikel (refereegranskat)abstract
- This study is aiming at controlling the microstructure of plasma sprayed Al2O3-TiO2 composite coatings using freeze granulated powders. As sprayed and sintered Al2O3+3wt%TiO2 powders were air plasma spayed with industry process parameters and compared with a commercial powder. The resulting coatings were investigated with respect to powder flowability, porosity and microstructure of the granules. The results showed that microstructure and melting fraction in the coatings could be tailored with the freeze granulation process and heat treatment conditions.
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| 37. |
- Åkerfeldt, Pia, et al.
(författare)
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The effect of crystallographic orientation on solid metal induced embrittlement of Ti-6Al-1Mo-1V in contact with copper
- 2013
-
Ingår i: IOP Conference Series: Materials Science and Engineering. - : IOP Publishing Ltd. - 1757-8981 .- 1757-899X. ; 48:1, s. 012011-
-
Konferensbidrag (refereegranskat)abstract
- Solid metal induced embrittlement (SMIE) occurs when a metal experiences tensilestress and is in contact with another metal with lower melting temperature. SMIE is believed tobe a combined action of surface self-diffusion of the embrittling species to the crack tip andadsorption of the embrittling species at the crack tip, which weakens the crack tip region. In thepresent study, both SMIE of the near alpha alloy Ti-8Al-1Mo-1V in contact with copper and itsinfluence by crystallographic orientation have been studied. U-bend specimens coated withcopper were heat treated at 480°C for 8 hours. One of the cracks was examined in detail usingelectron backscatter diffraction technique. A preferable crack path was found along high anglegrain boundaries with grains oriented close to [0001] in the crack direction; this indicates thatthere is a connection between the SMIE crack characteristics and the crystallographicorientation.
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| 38. |
- Dimitrios, Nikas, et al.
(författare)
-
Characterization of deformed pearlitic rail steel
- 2017
-
Ingår i: IOP Conference Series. - : Institute of Physics Publishing (IOPP). ; 219:1, s. Art no:UNSP 012035-
-
Konferensbidrag (refereegranskat)abstract
- Pearlitic steels are commonly used for railway rails because they combine good strength and wear properties. During service, the passage of trains results in a large accumulation of shear strains in the surface layer of the rail, leading to crack initiation. Knowledge of the material properties in this region is therefore important for fatigue life prediction. As the strain is limited to a thin surface layer, very large strain gradients can be found. This makes it very difficult to quantify changes in material behavior. In this study hardness measurements were performed close to the surface using the Knoop hardness test method. The orientation of the pearlitic lamellas was measured to give an overview of the deformed microstructure in the surface of the rail. Microstructural characterization of the material was done by optical microscopy and scanning electron microscopy to evaluate the changes in the microstructure due to the large deformation. A strong gradient can be observed in the top 50 μm of the rail, while deeper into the rail the microstructure of the base material is preserved.
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| 39. |
- Ekberg, Johanna, 1987, et al.
(författare)
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Analysis of single splats produced by axial suspension plasma spraying
- 2018
-
Ingår i: Surface Engineering. - : Informa UK Limited. - 1743-2944 .- 0267-0844. ; 34:5, s. 407-411
-
Tidskriftsartikel (refereegranskat)abstract
- Axial suspension plasma spraying (ASPS) is a relatively new, innovative technique with which microstructures have been produced that are similar to the ones produced by electron beam physical vapor deposition. They have a columnar structure and consist of nm- and µm-sized pores. However, so far the formation of the microstructure is not fully understood because fragmentation and vaporisation of the liquid significantly affects the deposition process. Analysis of single splats can provide important information on the phenomena controlling the coating formation process and the final coating properties. Therefore, the present study aims at providing first results of 8 wt-% yttria-stabilised zirconia single splats sprayed onto a steel substrate by use of ASPS. Scanning electron microscopy and atomic force microscopy have been used to characterise the splats with respect to appearance, shape, and size distribution.
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| 40. |
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| 41. |
- GUNNARSDÓTTIR, SOFFÍA ARNÞRÚÐUR, 1987, et al.
(författare)
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Towards Simulation of Geometrical Effects of Laser Tempering of Boron Steel before Self-Pierce Riveting
- 2016
-
Ingår i: Procedia CIRP. - : Elsevier BV. - 2212-8271. ; 44, s. 304-309
-
Konferensbidrag (refereegranskat)abstract
- The automotive industry is continuously developing and finding new ways to respond to the incremental demands of higher safety standards and lower environmental impact. As an answer to weight reduction of vehicles, the combination of boron steel and composite material is being developed along with their joining process, self-pierce riveting. Boron steel is an ultra-high strength material that needs to be locally softened before the joining process. However, the joining process deforms the part. This paper investigates factors affecting the geometrical deformation during the tempering process and lists important phenomena that need to be included when simulating the tempering process.
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| 42. |
- Henrysson, Erica, 1987, et al.
(författare)
-
Conceptual Design and Analysis of Membrane Structures
- 2016
-
Ingår i: Proceedings of 29th Nordic Seminar on Computational Mechanics – NSCM29.
-
Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- In this work one approach for formfinding and analysing tension membranestructures is described. Focus has been on the conceptual stage. For this the computersoftware SMART Form has been further developed, enabling the possibility to do real-timeformfinding and analysis of fabric structures. The software is based on a method where theorthotropic membrane is modeled with a triangular mesh, where the mass is lumped on thenodes. As a computational tool dynamic relaxation is used to find the static equilibriumconfiguration for the structure. The advantage with this is that there is no need for formulationand manipulation of matrices common in the finite element method.
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| 43. |
- Klement, Uta, 1962, et al.
(författare)
-
EBSD Analysis and Assessment of Porosity in Thermal Barrier Coatings Produced by Axial Suspension Plasma Spraying (ASPS)
- 2017
-
Ingår i: Materials Science Forum. - : Trans Tech Publications. - 1662-9752 .- 0255-5476. - 9783035711295 ; 879, s. 972-977, s. 972-977
-
Konferensbidrag (refereegranskat)abstract
- Axial suspension plasma spraying (ASPS) is a relatively new, innovative sprayingtechnique which has produced thermal barrier coatings (TBCs) with attractive properties such ashigh durability and low thermal conductivity. Using a suspension, it is possible to spray with finerpowder particles resulting in coatings that have a columnar microstructure and contain a wide rangeof pore sizes, both nm- and μm-sized pores. To optimize the thermal properties and to maintainthem during service of the components, it will be important to design TBCs with optimal porosity.Hence, an important part in the assessment of ASPS coatings is therefore the characterization of themicrostructure and how it is build up, and the determination of porosity. Both aspects are addressedby performing measurement on splats and ASPS-coating using electron backscatter diffraction(EBSD) technique and by measuring porosity by Mercury Intrusion Porosimetry (MIP).
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| 44. |
- Lund, Anja, et al.
(författare)
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Melt spinning of beta-phase poly(vinylidene fluoride) yarns with and without a conductive core
- 2011
-
Ingår i: Journal of Applied Polymer Science. - : Wiley Periodicals, Inc.. - 0021-8995 .- 1097-4628. ; 120:2, s. 1080-1089
-
Tidskriftsartikel (refereegranskat)abstract
- When poly(vinylidene fluoride) (PVDF) is to be used as a piezoelectric material, the processing must include the formation of polar β-phase crystallites, as well as the application of electrically conducting charge collectors, that is, electrodes. In this article, results from the melt spinning of PVDF yarns and a novel bicomponent PVDF-yarn with a conductive carbon black/polypropylene (CB/PP) core are presented. Melt spinning has been done under conditions typical for industrial large-scale fiber production. The effects on the resulting crystalline structure of varying the spinning velocity, draw rate, and draw temperature are discussed. The results show that, for maximum α-to-β phase transformation, cold drawing should take place at a temperature between 70 and 90°C, and both the draw ratio and the draw rate should be as high as possible. It was observed that the cold drawing necessary to form β-phase crystallinity simultaneously leads to a decrease in the core conductivity of the bicomponent yarns. In this work, the melt spinning of bicomponent fibers with high-β-phase PVDF in the sheath and a CB/PP core was successfully accomplished. The core material remained electrically conductive, paving the way for the use of a CB-polymer compound as inner electrode in the melt spinning of piezoelectric bicomponent fibers.
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| 45. |
- Lund, Anja
(författare)
-
Melt spun piezoelectric textile fibres : an experimental study
- 2013
-
Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Melt Spun Piezoelectric Textile Fibres - an Experimental Study ANJA LUND Department of Materials and Manufacturing Technology Chalmers University of Technology ABSTRACT The manufacturing and characterisation of piezoelectric textile fibres are described in this thesis. A piezoelectric material is one that generates an electric voltage when deformed, a property which exists in a number of materials. The polymer with the strongest known piezoelectric effect today is poly(vinylidene fluoride) (PVDF), however it must be processed under certain conditions to become piezoelectric. This study shows that piezoelectric bicomponent PVDF-based fibres can be produced by melt spinning, which is a common and relatively simple fibre spinning method. The melt spinning process must include cold drawing, as this introduces a polar crystalline structure in the polymer. The fibres must also be electroded, which is done by producing bicomponent fibres with a core-and-sheath structure. The core is electrically conductive and constitutes an inner electrode consisting of a carbon black/polymer compound, whereas the sheath is PVDF and constitutes the piezoelectric component. Being sensitive to both deformation and temperature changes, these fibres are anticipated to be useful in a number of sensor applications. The flexibility and small size of the fibres makes it possible to include them as miniature-sensors in structures or garment without affecting the shape or comfort.
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| 46. |
- Nikas, Dimitrios, 1984
(författare)
-
Influence of combined thermal and mechanical loadings on pearlitic steel microstructure in railway wheels and rails
- 2018
-
Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- One of the most important aspects in railway operation is the interaction between rail and wheel. The contact patch between these two components is around the size of a small coin, and since high loads act on this small area, stresses will give rise to wear and damage in both components. Frictional forces on the surface of wheels and rails caused by recurring train acceleration, braking, curving and occasional slippage can cause cyclic plastic deformation and heating, which in turn causes an aligned, anisotropic microstructure with altered mechanical behaviour. Control of material property degradation is an important topic for guiding maintenance, as well as ensuring safety of railways, since it will allow for a more accurate prediction of material wear and lifetime. The thesis focuses on the mechanical properties of railway wheel and rail steels after exposure to elevated temperatures and plastic deformation. Specifically examined are the carbon wheel steels, UIC ER7T and ER8T (~0.55 wt. %C) and rail steel R260 (~0.72 wt. %C). During their service life, the surface layers of rails and wheels are subjected to very high rolling contact loads. These lead to accumulation of large shear strains close to the running surface. Moreover the high thermal loads that wheels experience when block brakes are used can cause severe degradation of the material microstructure, more specifically spheroidisation of the pearlite, which combined with plastic deformation (that makes the material more prone to spheroidisation) can lead to severe deterioration of the material’s mechanical properties. Both un-deformed and pre-strained wheel materials were heat treated at various temperatures from 250°C to 600°C for various durations, and the change in room temperature hardness was analysed. Additionally, Electron Backscatter Diffraction Analysis (EBSD) was used to evaluate if orientation gradients in the pearlitic colonies affect the spheroidisation of the pearlitic microstructure, that is observed at higher temperatures. Uniaxial (tension-compression) and biaxial (including torsion) low cycle fatigue tests were performed to study the behaviour of R7T and R8T material at different temperatures. The influence of hold times as well as the ratchetting behaviour with mean stress effects were also studied. Virgin rail material was twisted using a biaxial machine to various shear strain levels to create a microstructure representative for the surface layer observed in field samples. The microstructure was characterised using scanning electron microscopy (SEM), transmission electron microscopy (TEM) and hardness measurements. The results showed that wheel material hardening due to strain ageing takes place at around 300°C while microstructural degradation caused softening at higher temperatures. Spheroidisation of the pearlite started to become visible at 450°C for the un-deformed material and at around 400°C for the pre-strained. The spheroidised areas appear to have lost their initial orientation gradients after spheroidisation and obtain a more uniform orientation. Cyclic tests at elevated temperature revealed cyclic hardening at around 300°C, as an effect of dynamic strain ageing. At higher temperatures, cyclic softening followed due to a combination of increasing thermal activation and spheroidisation. Biaxial testing showed a more severe effect of strain hardening and shorter fatigue life. For the rail material, the dislocation density was found to increase with increasing shear strain. The flow stresses calculated using microstructural parameters such as dislocation density and interlamellar spacing of the pearlite seem to agree well with those evaluated from hardness measurements.
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| 47. |
- Nilsson, Erik, 1976, et al.
(författare)
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Electrically conductive polymeric bi-component fibers containing a high load of low-structured carbon black
- 2015
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Ingår i: Journal of Applied Polymer Science. - : Wiley. - 1097-4628 .- 0021-8995. ; 132:29, s. art. no. 42255-
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Tidskriftsartikel (refereegranskat)abstract
- © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015, 132, 42255. © 2015 Wiley Periodicals, Inc. Melt spinning at semi-industrial conditions of carbon black (CB) containing textiles fibers with enhanced electrical conductivity suitable for heating applications is described. A conductive compound of CB and high density polyethylene (HDPE) was incorporated into the core of bi-component fibers which had a sheath of polyamide 6 (PA6). The rheological and fiber-forming properties of a low-structured and a high-structured CB/HDPE composite were compared in terms of their conductivity. The low-structured CB gave the best trade-off between processability and final conductivity. This was discussed in terms of the strength of the resulting percolated network of carbon particles and its effect on the spin line stability during melt spinning. The conductivity was found to be further enhanced with maintained mechanical properties by an in line thermal annealing of the fibers at temperatures in the vicinity of the melting point of HDPE. By an adequate choice of CB and annealing conditions a conductivity of 1.5 S/cm of the core material was obtained. The usefulness of the fibers for heating applications was demonstrated by means of a woven fabric containing the conductive fibers in the warp direction. By applying a voltage of 48 V the surface temperature of the fabric rose from 20 to 30°C.
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| 48. |
- Rasel, H., et al.
(författare)
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New bio-based plastics, from a non-edible plant oil side-stream, for film extrusion
- 2014
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Ingår i: 19th IAPRI World Conference on Packaging 2014. - : Victoria University. - 9781510821316 ; , s. 586-590
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Konferensbidrag (refereegranskat)abstract
- Renewable sourced PET, PA, PE, starch blends, etc, are fastly growing due to the processability and final performance, that is similar to their petroleum derived options. A bit in the shadow of the development of these plastics, development is ongoing on another group of plastics, made directly of the side-streams of agricultural products: oil plant residues and proteins. They can be used in edible applications but not all of them are suitable for food or forage. Industrial oilseed meal from crambe abyssinica contains relatively high levels of protein that is not suitable for human or animal consumption due to the presence of anti-nutritional compounds. This paper presents research on crambe meal as a base for new plastics, developed to extrude continuous, flexible plastic films based on crambe meal, blended with vital wheat gluten as an elastic component and urea as a protein denaturant. The effect of process parameters, such as screw speed, die temperature and pressure, and the effect of components were studied with regards to the final performance of the film extrudates. E.g. mechanical properties, oxygen permeability and moisture content were determined and surface and cross-section morphologies were examined with electron microscopy. The results showed that crambe-based blends can be extruded as continuous, flexible plastic films, which exhibit barrier properties towards oxygen. Recipes and methods for pelletizing of master batches for post-converting (e.g. extrusion or compression molding) were successfully developed. Addition of a renewable plasticizer improved the extrusion performance and resulted in less hygroscopic films, which further showed the overall highest tensile strength while the extensibility was nearly unaffected. The results provide a first basis to further develop the process and the blend towards potential industrial applications, for example as packaging materials to trays, pots and similar type of packages.
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| 49. |
- Ryttberg, Kristina, 1977, et al.
(författare)
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The effect of cold ring rolling on the evolution of microstructure and texture in 100Cr6 steel
- 2010
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Ingår i: Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing. - : Elsevier BV. - 0921-5093. ; 527:9, s. 2431-2436
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Tidskriftsartikel (refereegranskat)abstract
- This paper concerns the development of microstructure and texture during cold ring rolling of 100Cr6 steel rings with starting rectangular cross-sections. By interrupting the rolling process at pre-defined intervals expansion ratios ranging from 1.05 to 1.5 were achieved resulting in varying degrees of deformation of the rings. Results for rings with a simple rectangular cross-section were compared with results for a cold rolled ring with a more complex cross-section. By combining results from optical and scanning electron microscopy with hardness measurements the two different ring shapes were shown to display similar material flow during cold ring rolling. The deformation was most severe near the inner diameterof the rings decreasing towards the area of the outer diameter. By employing electron back scatter diffraction (EBSD) the ring rolling process was shown to change the {111}-fibre texture of the ring blanks to a {110} texture. This implies a mixture of both shear and compressive deformation during rolling.
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| 50. |
- Tam, Eric, 1980, et al.
(författare)
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XRD and XPS Characterisation of Transition Metal Silicide Thin Films
- 2012
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Ingår i: Surface Science. - : Elsevier BV. - 0039-6028. ; 606:3-4, s. 329-336
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Tidskriftsartikel (refereegranskat)abstract
- Binary transition metal silicides based on the systems Ti-Si, Fe-Si, Ni-Si and Cr-Si were fabricated on Si wafers by means of ion-beam co-sputter deposition and subsequent annealing. The crystalline structures of the phases formed were identified from the characteristic patterns acquired by means of X-ray diffraction (XRD) measurements. The phase formation sequences were described by means of the Pretorius’ effective heat of formation (EHF) model. For the Ti-Si, Fe-Si and Ni-Si systems, single phase thin films of TiSi2, β-FeSi2 and NiSi2 were generated as the model predicts, while a mixture of CrSi + CrSi2 phases was obtained for the Cr-Si system. The surface chemical condition of individual specimens were analysed by using X-ray photoelectron spectroscopy (XPS). The chemical shifts of transition metal 2p3/2 peaks from their metallic to silicide states were depicted by means of the Auger parameters and the Wagner plots. The positive chemical shift of 2.0 eV for Ni 2p3/2 peak of NiSi2 is mainly governed by the initial-state effects. For the other silicide specimens, the initial-state and final-state effects may oppose one another with similar impact. Consequently, smaller binding energy shifts of both negative and positive character are noted; a positive binding energy shift of 0.3 eV for the Fe 2p3/2 level was shown for β-FeSi2 and negative binding energy shifts of 0.1 and 0.3 eV were determined for CrSi + CrSi2 and TiSi2, respectively.
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