| 1. |
- Chen, Jinhan, et al.
(författare)
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The effect of hot isostatic pressing on thermal conductivity of additively manufactured pure tungsten
- 2020
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Ingår i: International journal of refractory metals & hard materials. - : Elsevier BV. - 0263-4368. ; 87
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Tidskriftsartikel (refereegranskat)abstract
- The crack-healing behaviors and microstructure evolution of pure tungsten produced by laser powder bed fusion (LPBF) were studied and compared before and after post hot isostatic pressing (post-HIP) treatment. An average thermal conductivity of 133 W.m(-1).K-1 at room temperature (RT) was obtained after HIP, which was 16% higher than that of as-built sample (115 W.m(-1).K-1). Although the HIP process had little effect on density, it resulted in a large grain size of > 300 mu m accompanied by a decrease in dislocation density and crack healing, which led to a substantial improvement of thermal conductivity of pure tungsten. The positive correlation between relative density and thermal conductivity of as-built tungsten was reported.
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| 2. |
- Li, Kailun, et al.
(författare)
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Crack suppression in additively manufactured tungsten by introducing secondary-phase nanoparticles into the matrix
- 2019
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Ingår i: International journal of refractory metals & hard materials. - : Elsevier BV. - 0263-4368. ; 79, s. 158-163
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Tidskriftsartikel (refereegranskat)abstract
- In this study, an effective strategy was developed to suppress cracking by introducing secondary-phase ZrC nanoparticles into a tungsten (W) matrix. Pure W and W-0.5wt%ZrC bulks were additively manufactured via the laser powder bed fusion (LPBF) technique, and their cracking behaviour was compared. It was observed that the crack density of W-ZrC was reduced by 88.7% compared with that of pure W. The grains in W-ZrC were obviously refined compared with the grains in pure W, which significantly increased the cracking resistance. In addition, ZrC diminished the oxygen impurities, further increasing the cracking resistance. This study provides a promising strategy for the additive manufacturing of high-quality W by introducing secondary-phase nanoparticles into the metal matrix.
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| 3. |
- Olsén, Jon, 1983-, et al.
(författare)
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Tailoring hierarchical structures in selective laser melted materials
- 2017
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Ingår i: IOP Conference Series. - : Institute of Physics (IOP).
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Konferensbidrag (refereegranskat)abstract
- With selective laser melting the potential to manufacture a wide variety of geometries from different materials has presented itself. Interest in this technology keeps growing every year, and with that growth a deeper understanding of the process and resulting materials is urgently needed. In this paper we present a short overview of the structural elements that appear during selective laser melting, and explain how to tailor them to achieve specific structures and material properties. Melt-pools, texture and grains, subgrain cells, and inclusions are the elements discussed herein, and tailoring of these elements can have effects on density, and corrosion resistance, as well as mechanical properties in general.
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| 4. |
- Song, Lu, et al.
(författare)
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Core/shell structured Zn/ZnO nanoparticles synthesized by gaseous laser ablation with enhanced photocatalysis efficiency
- 2018
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Ingår i: Applied Surface Science. - : Elsevier BV. - 0169-4332 .- 1873-5584. ; 442, s. 101-105
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Tidskriftsartikel (refereegranskat)abstract
- Zinc oxide (ZnO) is a competitive candidate in semiconductor photocatalysts, only if the efficiency could be fully optimized especially by tailored nanostructures. Here we report a kind of core/shell structured Zn/ZnO nanoparticles with enhanced photocatalysis efficiency, which were synthesized by a highly-productive gaseous laser ablation method. The nanodroplets generated by laser ablation would be reduced to zinc in the protective atmosphere, and further be oxidized at surface to form a specific core/shell structured Zn/ZnO nanoparticles within seconds. Thanks to the formation of this Zn-ZnO Schottky junction, the photocatalysis degradation efficiency of such core/shell Zn/ZnO nanostructure is significantly improved owing to the enhanced visible light absorption and inhibited carrier recombination by introducing the metallic zinc.
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| 5. |
- Wang, Yafei, et al.
(författare)
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A Data-Driven Scheme for Quantitative Analysis of Texture
- 2020
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Ingår i: Metallurgical and Materials Transactions. A. - : Springer Science and Business Media LLC. - 1073-5623 .- 1543-1940. ; 51:2, s. 940-950
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Tidskriftsartikel (refereegranskat)abstract
- Texture is the orientation distribution of crystallites in polycrystalline materials. Given the discrete orientations, Schaeben suggested to adopt statistics for quantitative analysis of texture from discrete orientations, and he also conceived a clustering algorithm to facilitate the applications of statistical methods (H. Schaeben, J Appl Crystal 26:112-121, 1993). This data-driven scheme becomes more urgent and more necessary for the oncoming fourth paradigm: data-intensive scientific discovery, which follows after experimental science, theoretical science, and computational science paradigm. This research adopts a density-based clustering algorithm, DBSCAN, to process the orientation data from an austenitic stainless steel 316 L sample fabricated by selective laser melting. It is validated that the algorithm can robustly identify the orientation cluster (or texture component or preferred orientation). The statistical methods can successfully quantify the features of the identified orientation cluster with quantified uncertainty (statistical significance), which is often lacked in the general method of orientation distribution function. It is believed that this data-driven scheme can be applied to the many aspects of texture analysis.
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| 6. |
- Wang, Yafei, et al.
(författare)
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Band-Like Distribution of Grains in Selective Laser Melting Track Under Keyhole Mode
- 2019
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Ingår i: Metallurgical and materials transactions. B, process metallurgy and materials processing science. - : Springer Science and Business Media LLC. - 1073-5615 .- 1543-1916. ; 50:2, s. 1035-1041
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Tidskriftsartikel (refereegranskat)abstract
- Grain structure in the melt pool under keyhole mode is complex due to complicated solidified conditions, especially in consideration of the intense fluid flow. This paper aims to clarify grain structure and grain growth mechanism in melt pool under keyhole mode in selective laser melting. The microstructure from transverse cross section and longitudinal cross section near the centerline of 316L single tracks was characterized. In the longitudinal cross section, band-like grain structure formed. It is found that fluid flow can refine the grains, and large columnar grains grow towards crystallographic < 110 > direction.
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| 7. |
- Wang, Yafei, et al.
(författare)
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Construction of Cellular Substructure in Laser Powder Bed Fusion
- 2019
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Ingår i: Metals. - : MDPI AG. - 2075-4701.
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Tidskriftsartikel (refereegranskat)abstract
- Cellular substructure has been widely observed in the sample fabricated by laser powder bed fusion, while its growth direction and the crystallographic orientation have seldom been studied. This research tries to build a general model to construct the substructure from its two-dimensional morphology. All the three Bunge Euler angles to specify a unique growth direction are determined, and the crystallographic orientation corresponding to the growth direction is also obtained. Based on the crystallographic orientation, the substructure in the single track of austenitic stainless steel 316L is distinguished between the cell-like dendrite and the cell. It is found that, with the increase of scanning velocity, the substructure transits from cell-like dendrite to cell. When the power is 200 W, the critical growth rate of the transition in the single track can be around 0.31 ms(-1).
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| 8. |
- Wang, Yafei, et al.
(författare)
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Grain structure and texture of the SLM single track
- 2020
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Ingår i: Journal of Materials Processing Technology. - : Elsevier BV. - 0924-0136 .- 1873-4774. ; 281
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Tidskriftsartikel (refereegranskat)abstract
- The grain structure and texture of metal parts fabricated by selective laser melting (SLM) are of interest for their effect on the properties. The study of the SLM single track can reduce the variables to be concerned and, hence, facilitate the understanding of the development of grain and texture in the SLM process. In this work, the austenitic stainless 316L single tracks are fabricated at different scanning speeds, and they are characterized by electron backscattered diffraction (EBSD) from transverse, serial transverse, and longitudinal cross-sections. It is validated that curved grain is common in the SLM single track. The effects of the varied thermal gradient and the shape of the melt pool on competitive growth of grain are analyzed. All the three equivalent < 001 > orientations of the columnar grain are considered, which leads us to put forward a crystallographic feature of a favorable grain during the competitive growth in SLM. Such a crystallographic feature is validated by the texture of the SLM single track, especially the < 001 > // scanning direction (SD) texture.
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