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- Kubo, M., et al.
(författare)
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Nanosecond pump-probe device for time-resolved serial femtosecond crystallography developed at SACLA
- 2017
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Ingår i: Journal of Synchrotron Radiation. - : International Union of Crystallography (IUCr). - 1600-5775. ; 24, s. 1086-1091
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Tidskriftsartikel (refereegranskat)abstract
- X-ray free-electron lasers (XFELs) have opened new opportunities for timeresolved X-ray crystallography. Here a nanosecond optical-pump XFEL-probe device developed for time-resolved serial femtosecond crystallography (TRSFX) studies of photo-induced reactions in proteins at the SPring-8 Angstrom Compact free-electron LAser (SACLA) is reported. The optical-fiber-based system is a good choice for a quick setup in a limited beam time and allows pump illumination from two directions to achieve high excitation efficiency of protein microcrystals. Two types of injectors are used: one for extruding highly viscous samples such as lipidic cubic phase (LCP) and the other for pulsed liquid droplets. Under standard sample flow conditions from the viscous-sample injector, delay times from nanoseconds to tens of milliseconds are accessible, typical time scales required to study large protein conformational changes. A first demonstration of a TR-SFX experiment on bacteriorhodopsin in bicelle using a setup with a droplet-type injector is also presented.
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- Esmaeili, Ali, 1983, et al.
(författare)
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Thermomechanical cracking of railway wheel treads: a combined experimental and numerical approach
- 2015
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Ingår i: Proceedings of the 10th International Conference on Contact Mechanics and Wear of Rail/Wheel Systems (CM2015). ; , s. 8-
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Konferensbidrag (refereegranskat)abstract
- In the present study, thermal cracking of railway wheel treads is studied by full-scale brake rig tests and finite element simulations. The focus is on thermomechanical rolling contact fatigue (RCF) life predictions. The wheel tread material is subjected to simultaneous mechanical and thermal loads due to rolling contact and stop braking, respectively. Full-scale tests featuring three series of repeated stop braking cases have been performed at the Railway Technical Research Institute (RTRI) in Japan in a brake rig featuring a tread braked wheel that is in rolling contact with a railwheel. The brake rig test conditions have been simulated numerically using the finite element method. To this end, the effect of “hot bands” on the tread is accounted for as indicated by the experimental findings. Thermomechanical stresses induced by braking as well as Hertzian contact loading on the tread including tractive loads based on a partial slip assumption are considered. The mechanical response of the wheel material ER7 is obtained from a viscoplastic Chaboche material model calibrated against data from cyclic experiments with hold-time from room temperatures up to 650 °C. Finally, a strategy for prediction of fatigue life with respect to ratcheting failure is discussed.
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