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Improved procedure ...
Improved procedure for cyclization of vinyl azides into 3-substituted-2H-azirines
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Timen, A. S. (författare)
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Risberg, E. (författare)
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- Somfai, Peter (författare)
- KTH,Kemi
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(creator_code:org_t)
- Elsevier BV, 2003
- 2003
- Engelska.
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Ingår i: Tetrahedron Letters. - : Elsevier BV. - 0040-4039 .- 1359-8562. ; 44:28, s. 5339-5341
- Relaterad länk:
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Ämnesord
Stäng
- A significantly improved procedure for the preparation of 3-substituted 2H-azirines has been developed. By cyclization of the corresponding vinyl azides in low boiling solvents in closed vessels at elevated temperature, high purity, short reaction time and simple isolation of the product were achieved.
Nyckelord
- vinyl azide
- thermolysis
- azirine
- diels-alder reactions
- unsaturated azides
- general synthesis
- 2h-azirines
- 2h-azirine-3-carboxylate
- cycloadditions
- dienophiles
- pyrimidine
- azirines
- olefins
Publikations- och innehållstyp
- ref (ämneskategori)
- art (ämneskategori)
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