Sökning: onr:"swepub:oai:lup.lub.lu.se:148bad22-7f11-43b7-bb63-76e9e255e772" > Photoelectrochemica...
Fältnamn | Indikatorer | Metadata |
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000 | 02929naa a2200325 4500 | |
001 | oai:lup.lub.lu.se:148bad22-7f11-43b7-bb63-76e9e255e772 | |
003 | SwePub | |
008 | 160401s2005 | |||||||||||000 ||eng| | |
024 | 7 | a https://lup.lub.lu.se/record/1510282 URI |
024 | 7 | a https://doi.org/10.1016/j.aca.2005.04.0042 DOI |
040 | a (SwePub)lu | |
041 | a engb eng | |
042 | 9 SwePub | |
072 | 7 | a art2 swepub-publicationtype |
072 | 7 | a ref2 swepub-contenttype |
100 | 1 | a Dilgin, Y4 aut |
245 | 1 0 | a Photoelectrochemical investigation of methylene blue immobilised on zirconium phosphate modified carbon paste electrode in flow injection system |
264 | 1 | b Elsevier BV,c 2005 |
300 | a 7 s. | |
520 | a The adsorption of methylene blue (MB) onto zirconium phosphate (ZrP) was studied and the adsorption capacity value and isotherms were determined. The adsorption capacity of ZrP was increased after being exposed to gas phase n-butyl amine. The adsorbed MB on ZrP was used as a modifier material in carbon paste electrode (MCPE), which in turn was used in voltammetric investigations and flow injection (FI) amperometric determination of ascorbic acid (AA). A quasi-reversible electrode reaction of adsorbed MB was exhibited. A home made flow-through electrochemical cell with a suitable transparent window for irradiation of the electrode surface was constructed and used for amperometric FI studies. The photoamperometric-FI conditions were optimised as 1.5 mL min(-1) flow rate, a 25 cm transmission tubing length, a 100 mu L injection volume, and a constant applied potential of +100 mV versus SCE. The calibration curve for AA was linear over the concentration range from 1.0 x 10(-6) to 4.0 x 10(-5) M. The relative standard deviation of four replicate injections of 3.0 x 10(-5) M AA was 1.2 %. The results obtained for AA determination in pharmaceutical products are in good agreement with those obtained using the procedure involving the reaction between triiodide and AA. (c) 2005 Elsevier B.V. All rights reserved. | |
650 | 7 | a NATURVETENSKAPx Kemix Analytisk kemi0 (SwePub)104012 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Analytical Chemistry0 (SwePub)104012 hsv//eng |
700 | 1 | a Dursun, Z4 aut |
700 | 1 | a Nisli, G4 aut |
700 | 1 | a Gorton, Lou Lund University,Lunds universitet,Centrum för analys och syntes,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Centre for Analysis and Synthesis,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH4 aut0 (Swepub:lu)akem-lgo |
710 | 2 | a Centrum för analys och syntesb Kemiska institutionen4 org |
773 | 0 | t Analytica Chimica Actad : Elsevier BVg 542:2, s. 162-168q 542:2<162-168x 1873-4324x 0003-2670 |
856 | 4 | u http://dx.doi.org/10.1016/j.aca.2005.04.004y FULLTEXT |
856 | 4 8 | u https://lup.lub.lu.se/record/151028 |
856 | 4 8 | u https://doi.org/10.1016/j.aca.2005.04.004 |
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