Sökning: onr:"swepub:oai:lup.lub.lu.se:6cea0111-c485-4971-b5ae-bfbf5c78628e" > Introduction of aro...
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000 | 03877naa a2200337 4500 | |
001 | oai:lup.lub.lu.se:6cea0111-c485-4971-b5ae-bfbf5c78628e | |
003 | SwePub | |
008 | 160401s2005 | |||||||||||000 ||eng| | |
024 | 7 | a https://lup.lub.lu.se/record/1523632 URI |
024 | 7 | a https://doi.org/10.1002/ejoc.2005002132 DOI |
040 | a (SwePub)lu | |
041 | a engb eng | |
042 | 9 SwePub | |
072 | 7 | a art2 swepub-publicationtype |
072 | 7 | a ref2 swepub-contenttype |
100 | 1 | a Solano, Carlosu Lund University,Lunds universitet,Centrum för analys och syntes,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Centre for Analysis and Synthesis,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH4 aut0 (Swepub:lu)chem-cso |
245 | 1 0 | a Introduction of aromatic and heteroaromatic groups in the 2-and 8-positions of the Troger's base core by Suzuki, Stille and Negishi cross-coupling reactions - A comparative study |
264 | 1 | b Wiley,c 2005 |
520 | a A comparative study on the bis(functionalization) of the Troger's base core by aromatic and heteroaromatic groups using palladium-catalyzed cross-coupling reactions is presented. Three different reactions, the Suzuki, Stille, and Negishi couplings, were investigated using Troger's base analogues equally substituted in the 2,8-positions with (HO)(2)B, Bu3Sn and ZnCl groups, respectively, as the metallated comportent. Six aryl halides with different electronic and steric properties were employed as coupling partners. The presence of the bulky and electron-rich phosphane P(tBu)(3) as cocatalyst was found to play an important role. In addition, the palladium source, [Pd(PPh3)(4)] or [Pd-2(dba)(3)], was also found to be all important factor for the yield of the reactions, The Suzuki coupling was found to be the best method in general, giving excellent yields for most aryl halides, whereas the Stille and Negishi couplings gave moderate to good yields. Finally, the crystal structures of the 4-nitrophenyl- and the 2-pyridyl-appended analogues of Troger's base, 7d and 7f, are presented in the Supporting Information. | |
650 | 7 | a NATURVETENSKAPx Kemix Organisk kemi0 (SwePub)104052 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Organic Chemistry0 (SwePub)104052 hsv//eng |
700 | 1 | a Svensson, Daniel4 aut |
700 | 1 | a Olomi, Zarinau Lund University,Lunds universitet,Centrum för analys och syntes,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Centre for Analysis and Synthesis,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH4 aut0 (Swepub:lu)orgk-zol |
700 | 1 | a Jensen, Jacobu Lund University,Lunds universitet,Centrum för analys och syntes,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Centre for Analysis and Synthesis,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH4 aut0 (Swepub:lu)orgk1-jj |
700 | 1 | a Wendt, Olau Lund University,Lunds universitet,Centrum för analys och syntes,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Centre for Analysis and Synthesis,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH4 aut0 (Swepub:lu)ook1-owe |
700 | 1 | a Wärnmark, Kennethu Lund University,Lunds universitet,Centrum för analys och syntes,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Centre for Analysis and Synthesis,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH4 aut0 (Swepub:lu)orgk1-kw |
710 | 2 | a Centrum för analys och syntesb Kemiska institutionen4 org |
773 | 0 | t European Journal of Organic Chemistryd : Wileyg 2005:16, s. 3510-3517q 2005:16<3510-3517x 1434-193Xx 1099-0690 |
856 | 4 | u http://dx.doi.org/10.1002/ejoc.200500213y FULLTEXT |
856 | 4 8 | u https://lup.lub.lu.se/record/152363 |
856 | 4 8 | u https://doi.org/10.1002/ejoc.200500213 |
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