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Analyzing Boron in ...
Analyzing Boron in 9-12% Chromium Steels Using Atom Probe Tomography
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- Fedorova, Irina (författare)
- Danmarks Tekniske Universitet,Technical University of Denmark
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- Grumsen, F. B. (författare)
- Danmarks Tekniske Universitet,Technical University of Denmark
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- Hald, John (författare)
- Danmarks Tekniske Universitet,Technical University of Denmark
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- Andrén, Hans-Olof, 1947 (författare)
- Chalmers tekniska högskola,Chalmers University of Technology
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- Liu, Fang, 1975 (författare)
- Chalmers tekniska högskola,Chalmers University of Technology
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(creator_code:org_t)
- 2019
- 2019
- Engelska.
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Ingår i: Microscopy and Microanalysis. - 1435-8115 .- 1431-9276. ; 25:2, s. 462-469
- Relaterad länk:
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https://doi.org/10.1...
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https://research.cha...
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Abstract
Ämnesord
Stäng
- Microscopy Society of America 2019. Small additions of boron can remarkably improve the long-term creep resistance of 9-12% Cr steels. The improvement has been attributed to boron segregation to grain boundaries during quenching, and subsequent boron incorporation into certain families of precipitates during tempering. However, the detailed mechanisms are not yet fully understood. Atom probe tomography (APT) is an excellent technique for gaining insights into boron distribution, however, in order to acquire accurate analysis of boron in 9-12% Cr steels using APT, there are several key challenges. In order to better understand and address these challenges, we developed a novel method for site-specific APT specimen preparation, which enables convenient preparation of specimens containing specifically selected grain boundaries positioned approximately perpendicular to the axis of the APT tip. Additionally, when analyzing boron at boundaries and in carbides (as diluted solute) and borides, a widening of the profile of boron distribution compared to other elements was repeatedly observed. This phenomenon is particularly analyzed and discussed in light of the evaporation field of different elements. Finally, the possible effects of detector dead-time on quantitative analysis of boron in metal borides are discussed. A simple method using 10B correction was used to obtain good quantification.
Ämnesord
- NATURVETENSKAP -- Kemi -- Annan kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences -- Other Chemistry Topics (hsv//eng)
- TEKNIK OCH TEKNOLOGIER -- Materialteknik -- Annan materialteknik (hsv//swe)
- ENGINEERING AND TECHNOLOGY -- Materials Engineering -- Other Materials Engineering (hsv//eng)
- TEKNIK OCH TEKNOLOGIER -- Materialteknik -- Metallurgi och metalliska material (hsv//swe)
- ENGINEERING AND TECHNOLOGY -- Materials Engineering -- Metallurgy and Metallic Materials (hsv//eng)
Nyckelord
- quantification
- precipitates
- non-equilibrium segregation
- TKD
- equilibrium segregation
- carbides
- prior austenite grain boundaries
- borides
- custom-made specimen holder
Publikations- och innehållstyp
- art (ämneskategori)
- ref (ämneskategori)
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