| 1. |
- Brueckner, Frank, et al.
(author)
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Enhanced manufacturing possibilities using multi-materials in laser metal deposition
- 2018
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In: Journal of laser applications. - : American Institute of Physics (AIP). - 1042-346X .- 1938-1387. ; 26:2, s. 10-12
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Journal article (peer-reviewed)abstract
- Additive manufacturing (AM) addresses various benefits as the buildup of complex shaped parts, the possibility of functional integration, reduced lead times or the use of difficult machinable materials compared to conventional manufacturing possibilities. Beside these advantages, the use of more than one material in a component would strongly increase the field of applications in typical AM branches as energy, aerospace, or medical technology. By means of multi-material buildups, cost-intensive alloys could be only used in high-loaded areas of the part, whereas the remaining part could be fabricated with cheaper compositions. The selection of combined materials strongly depends on the requested thermophysical but also mechanical properties. Within this contribution, examples (e.g., used in the turbine business) show how alloys can be arranged to fit together, e.g., in terms of a well-chosen coefficient of thermal expansion. As can be seen in nature, the multi-material usage can be characterized by sharp intersections from one material to the other (e.g., in case of a thin corrosion protection), but also by graded structures enabling a smoother material transition (e.g., in case of dissimilar materials which are joined together without defects). The latter is shown for an example from aerospace within this paper. Another possibility is the simultaneous placement of several materials, e.g., hard carbide particles placed in a more ductile matrix composition. These particles can be varied in size (e.g., TiC versus WC). Also the ratio between carbides and matrix alloy can be adjusted depending on its application. Especially, nozzle-based free form fabrication technologies, e.g., laser metal deposition, enable the utilization of more than one material. Within this contribution, possibilities to feed more than one filler material are demonstrated. In addition, results of multi-material processes are shown. Finally, this work focuses on different (potential) applications, mainly on power generation, but also for medical technology or wear resistant components.
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| 2. |
- Brueckner, Frank, et al.
(author)
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Fabrication of metallic multi-material components using Laser Metal Deposition
- 2017
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In: Solid Freeform Fabrication 2017. - : The University of Texas at Austin. ; , s. 2530-2538
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Conference paper (other academic/artistic)abstract
- Meanwhile, Laser Metal Deposition (LMD) is a well-known Additive Manufacturing technology used in various industrial branches as energy, tooling or aerospace. It can be used for the fabrication of new components but also repair applications. So far, volume build-ups were mostly carried out with one single material only. However, loading conditions may strongly vary and, hence, the use of more than one material in a component would yield major benefits. By means of multi-material build-ups, cost-intensive alloys could be used in highly-loaded areas of the part, whereas the remaining part could be fabricated with cheaper compositions. The selection of combined materials strongly depends on the requested thermo-physical and mechanical properties. Within this contribution, possibilities of material combinations by LMD and selected examples of beneficial multi-material use are presented.
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| 3. |
- Brueckner, Frank, et al.
(author)
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Phenomena in multi-material fabrication using laser metal deposition
- 2019
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In: Laser 3D Manufacturing VI. - : SPIE - The International Society for Optics and Photonics.
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Conference paper (peer-reviewed)abstract
- Additive Manufacturing (AM) processes as Laser Metal Deposition (LMD) addresses various benefits such as the build-up of complex shaped parts, the possibility of functional integration, reduced lead times or the use of difficult machinable materials compared to conventional manufacturing possibilities. Beside mentioned advantages, the use of more than one material in a component strongly increases the field of applications. Similar to structures in nature, multi-material arrangements can be realized by (I) sharp intersections from one material to the other (e. g. in the case of a thin corrosion protection), (II) graded structures enabling smoother material transitions (e. g. dissimilar materials joined together without defects), (III) composite structures with enclosed particles in a matrix material as well as by (IV) in-situ alloying of different material compositions. Due to varying material properties (e.g. thermo-physical, mechanical, optical), the combination of materials often requires a detailed investigation of occurring process phenomena and well-chosen modifications of the process regimes. Within this paper, (a) the right material feeding as well as powder interaction between various materials in Laser Metal Deposition, (b) the suitable selection of laser wavelengths for different materials, (c) process window adjustments by means of additional sensor equipment, (d) limitations of material combinations as well as (e) results and material characterization of multi-material parts are discussed. Phenomena are discussed by means of exemplary industrial applications, e.g. from the jet engine or medical business.
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| 4. |
- Gruber, Samira, et al.
(author)
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Comparison of dimensional accuracy and tolerances of powder bed based and nozzle based additive manufacturing processes
- 2020
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In: Journal of laser applications. - : American Institute of Physics (AIP). - 1042-346X .- 1938-1387. ; 32:3
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Journal article (peer-reviewed)abstract
- Additive manufacturing processes have the potential to produce near-net shaped complex final parts in various industries such as aerospace, medicine, or automotive. Powder bed based and nozzle based processes like laser metal deposition (LMD), laser powder bed fusion (LPBF), and electron beam melting (EBM) are commercially available, but selecting the most suitable process for a specific application remains difficult and mainly depends on the individual know-how within a certain company. Factors such as the material used, part dimension, geometrical features, as well as tolerance requirements contribute to the overall manufacturing costs that need to be economically reasonable compared to conventional processes. Within this contribution, the quantitative analysis of basic geometrical features such as cylinders, thin walls, holes, and cooling channels of a special designed benchmark demonstrator manufactured by LMD; LPBF and EBM are presented to compare the geometrical accuracy within and between these processes to verify existing guidelines, connect the part quality to the process parameters, and demonstrate process-specific limitations. The fabricated specimens are investigated in a comprehensive manner with 3D laser scanning and CT scanning with regard to dimensional and geometrical accuracy of outer and inner features. The obtained results will be discussed and achievable as-built tolerances for assessed demonstrator parts will be classified according to general tolerance classes described [DIN ISO 2768-1,Allgemeintoleranzen-Teil 1: Toleranzen fur Langen- und Winkelmasse ohne einzelne Toleranzeintragung(1991). Accessed 26 February 2018; DIN ISO 2768-2,Allgemeintoleranzen-Teil 2: Toleranzen fur Form und Lage ohne einzelne Toleranzeintragung(1991). Accessed 26 February 2018].
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| 5. |
- Hendl, Julius, et al.
(author)
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In Situ CT Tensile Testing of an Additively Manufactured and Heat-Treated Metastable ß-Titanium Alloy (Ti-5Al-5Mo-5V-3Cr)
- 2021
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In: Applied Sciences. - : MDPI. - 2076-3417. ; 11:21
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Journal article (peer-reviewed)abstract
- Additive manufacturing has been considered a suitable process for developing high-performance parts of medical or aerospace industries. The electron beam powder bed fusion process, EB-PBF, is a powder bed fusion process carried out in a vacuum, in which the parts are melted using a highly focused electron beam. The material class of metastable β-titanium alloys, and especially Ti-5Al-5Mo-5V-3Cr, show great potential for use as small and highly complex load-bearing parts. Specimens were additively manufactured with optimised process parameters and different heat treatments used in order to create tailored mechanical properties. These heat-treated specimens were analysed with regard to their microstructure (SEM) and their mechanical strength (tensile testing). Furthermore, in situ tensile tests, using a Deben CT5000 and a YXLON ff35 industrial µ-CT, were performed and failure-critical defects were detected, analysed and monitored. Experimental results indicate that, if EB-PBF-manufactured Ti-5553 is heat-treated differently, a variety of mechanical properties are possible. Regarding their fracture mechanisms, failure-critical defects can be detected at different stages of the tensile test and defect growth behaviour can be analysed.
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| 6. |
- Hendl, Julius, et al.
(author)
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NDE for Additive Manufacturing
- 2022. - 1
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In: Handbook of Nondestructive Evaluation 4.0. - Cham : Springer. - 9783030732066 - 9783030732059 ; , s. 665-696
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Book chapter (other academic/artistic)abstract
- By means of additive manufacturing (AM) complex-shaped parts can be manufactured using a broad range of different materials. The latter can be supplied in the form of powder, wire, paste material, or even as foil. Various technologies are covered by the term “Additive Manufacturing,” for example, direct energy deposition (DED), laser powder bed fusion (LPBF), fused filament fabrication (FFF), or binder jetting printing (BJP). In all varieties, parts are manufactured layer by layer which results in changed material properties compared to conventional manufacturing routes, for example, mechanical properties or fatigue life. To reach a conformal material deposition without defects such as lack of fusion, delamination or cracking, an optimal process window with well-chosen parameters (e.g., beam power, spot size, scanning speed) has to be identified.For nondestructive evaluation (NDE), different approaches can be used to classify AM manufactured parts regarding their defect structure and consequentially their performance:1.Process optimization and understanding of defect formation in order to prevent defects 2.In situ measurements by a variety of integrated sensors and (IR) cameras for direct process observations 3.Post-processing NDE methods such as ultrasonic testing, X-ray, or computer tomography (CT)If the three approaches are simultaneously executed, a prediction of the effect of defects can be made for certain cases.
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| 7. |
- Joshi, Siddarth Koduru, et al.
(author)
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Space QUEST mission proposal : experimentally testing decoherence due to gravity
- 2018
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In: New Journal of Physics. - : IOP Publishing. - 1367-2630. ; 20
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Journal article (peer-reviewed)abstract
- Models of quantum systems on curved space-times lack sufficient experimental verification. Some speculative theories suggest that quantum correlations, such as entanglement, may exhibit different behavior to purely classical correlations in curved space. By measuring this effect or lack thereof, we can test the hypotheses behind several such models. For instance, as predicted by Ralph et al [5] and Ralph and Pienaar [1], a bipartite entangled system could decohere if each particle traversed through a different gravitational field gradient. We propose to study this effect in a ground to space uplink scenario. We extend the above theoretical predictions of Ralph and coworkers and discuss the scientific consequences of detecting/failing to detect the predicted gravitational decoherence. We present a detailed mission design of the European Space Agency's Space QUEST (Space-Quantum Entanglement Space Test) mission, and study the feasibility of the mission scheme.
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| 8. |
- Lopez, Elena, et al.
(author)
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Evaluation of 3D-printed parts by means of high-performance computer tomography
- 2018
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In: Journal of laser applications. - : American Institute of Physics (AIP). - 1042-346X .- 1938-1387. ; 30:3
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Journal article (peer-reviewed)abstract
- Conventional tactile and optical testing methods are not capable to detect complex inner geometries or complex surface shapes. Detecting porosities in parts is also not possible with those nondestructive methods. Among other material parameters, geometrical accuracy is essential to determine part's quality. Additive manufacturing processes also have to be optimized regarding geometry deviations caused by distortion or unfavorable orientation in the build chamber. For additive manufactured parts that incorporate previously mentioned features, high-performance computer tomography is the more suitable nondestructive testing method. Components of different materials such as plastics, ceramics, composites, or metals can be completely characterized. This nondestructive testing method was used for porosity analysis regarding the shape and local distribution of pores in an additive manufactured part to find correlations concerning the most suitable process conditions. The measured part data were also compared to original CAD files to determine zones of deviation and apply specific process strategies to avoid distortion. This paper discusses the results of integrating high-performance computer tomography (power: 500 W, max. part size: Ø 300 mm, 300 × 430 mm2) in a productionlike environment of additively manufactured parts for a wide range of technologies (i.e., electron beam melting and selective laser melting). I. INTRODUCTION
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| 9. |
- Moritz, Juliane, et al.
(author)
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Electron beam powder bed fusion of γ‐titanium aluminide : Effect of processing parameters on part density, surface characteristics and aluminum content
- 2021
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In: Metals. - : MDPI. - 2075-4701. ; 11:7
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Journal article (peer-reviewed)abstract
- Gamma titanium aluminides are very interesting for their use in high‐performance applications such as aircraft engines due to their low density, high stiffness and favorable hightemperature properties. However, the pronounced brittleness of these intermetallic alloys is a major challenge for their processing through conventional fabrication methods. Additive manufacturing by means of electron beam powder bed fusion (EB‐PBF) significantly improves the processability of titanium aluminides due to the high preheating temperatures and facilitates complex components. The objective of this study was to determine a suitable processing window for EB‐PBF of the TNM‐B1 alloy (Ti‐43.5Al‐4Nb‐1Mo‐0.1B), using an increased aluminum content in the powder raw material to compensate for evaporation losses during the process. Design of experiments was used to evaluate the effect of beam current, scan speed, focus offset, line offset and layer thickness on porosity. Top surface roughness was assessed through laser scanning confocal microscopy. Scanning electron microscopy, electron backscatter diffraction (EBSD) and energydispersive X‐ray spectroscopy (EDX) were used for microstructural investigation and to analyze aluminum loss depending on the volumetric energy density used in EB‐PBF. An optimized process parameter set for achieving part densities of 99.9% and smooth top surfaces was derived. The results regarding microstructures and aluminum evaporation suggest a solidification via the β‐phase.
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| 10. |
- Moritz, Juliane, et al.
(author)
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Influence of Electron Beam Powder Bed Fusion Process Parameters at Constant Volumetric Energy Density on Surface Topography and Microstructural Homogeneity of a Titanium Aluminide Alloy
- 2023
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In: Advanced Engineering Materials. - : John Wiley & Sons. - 1438-1656 .- 1527-2648. ; 25:15
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Journal article (peer-reviewed)abstract
- In powder bed fusion additive manufacturing, the volumetric energy density E V is a commonly used parameter to quantify process energy input. However, recent results question the suitability of E V as a design parameter, as varying the contributing parameters may yield different part properties. Herein, beam current, scan velocity, and line offset in electron beam powder bed fusion (PBF-EB) of the titanium aluminide alloy TNM–B1 are systematically varied while maintaining an overall constant E V. The samples are evaluated regarding surface morphology, relative density, microstructure, hardness, and aluminum loss due to evaporation. Moreover, the specimens are subjected to two different heat treatments to obtain fully lamellar (FL) and nearly lamellar (NLγ) microstructures, respectively. With a combination of low beam currents, low-to-intermediate scan velocities, and low line offsets, parts with even surfaces, relative densities above 99.9%, and homogeneous microstructures are achieved. On the other hand, especially high beam currents promote the formation of surface bulges and pronounced aluminum evaporation, resulting in inhomogeneous banded microstructures after heat treatment. The results demonstrate the importance of considering the individual parameters instead of E V in process optimization for PBF-EB.
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| 11. |
- Moritz, Juliane, et al.
(author)
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Influence of Two-Step Heat Treatments on Microstructure and Mechanical Properties of a β-Solidifying Titanium Aluminide Alloy Fabricated via Electron Beam Powder Bed Fusion
- 2023
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In: Advanced Engineering Materials. - : John Wiley & Sons. - 1438-1656 .- 1527-2648. ; 25:2
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Journal article (peer-reviewed)abstract
- Additive manufacturing technologies, particularly electron beam powder bed fusion (PBF-EB/M), are becoming increasingly important for the processing of intermetallic titanium aluminides. This study presents the effects of hot isostatic pressing (HIP) and subsequent two-step heat treatments on the microstructure and mechanical properties of the TNM-B1 alloy (Ti–43.5Al–4Nb–1Mo–0.1B) fabricated via PBF-EB/M. Adequate solution heat treatment temperatures allow the adjustment of fully lamellar (FL) and nearly lamellar (NL-β) microstructures. The specimens are characterized by optical microscopy and scanning electron microscopy (SEM), X-ray computed tomography (CT), X-ray diffraction (XRD), and electron backscatter diffraction (EBSD). The mechanical properties at ambient temperatures are evaluated via tensile testing and subsequent fractography. While lack-of-fusion defects are the main causes of failure in the as-built condition, the mechanical properties in the heat-treated conditions are predominantly controlled by the microstructure. The highest ultimate tensile strength is achieved after HIP due to the elimination of lack-of-fusion defects. The results reveal challenges originating from the PBF-EB/M process, for example, local variations in chemical composition due to aluminum evaporation, which in turn affect the microstructures after heat treatment. For designing suitable heat treatment strategies, particular attention should therefore be paid to the microstructural characteristics associated with additive manufacturing.
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| 12. |
- Moritz, Juliane, et al.
(author)
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Locally Adapted Microstructures in an Additively Manufactured Titanium Aluminide Alloy Through Process Parameter Variation and Heat Treatment
- 2023
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In: Advanced Engineering Materials. - : John Wiley & Sons. - 1438-1656 .- 1527-2648. ; 25:2
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Journal article (peer-reviewed)abstract
- Electron beam powder bed fusion (PBF-EB/M) has been attracting great research interest as a promising technology for additive manufacturing of titanium aluminide alloys. However, challenges often arise from the process-induced evaporation of aluminum, which is linked to the PBF-EB/M process parameters. This study applies different volumetric energy densities during PBF-EB/M processing to deliberately adjust the aluminum contents in additively manufactured Ti–43.5Al–4Nb–1Mo–0.1B (TNM-B1) samples. The specimens are subsequently subjected to hot isostatic pressing (HIP) and a two-step heat treatment. The influence of process parameter variation and heat treatments on microstructure and defect distribution are investigated using optical and scanning electron microscopy, as well as X-ray computed tomography (CT). Depending on the aluminum content, shifts in the phase transition temperatures can be identified via differential scanning calorimetry (DSC). It is confirmed that the microstructure after heat treatment is strongly linked to the PBF-EB/M parameters and the associated aluminum evaporation. The feasibility of producing locally adapted microstructures within one component through process parameter variation and subsequent heat treatment can be demonstrated. Thus, fully lamellar and nearly lamellar microstructures in two adjacent component areas can be adjusted, respectively.
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| 13. |
- Müller, Michael, et al.
(author)
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Microstructure of NiAl-Ta-Cr in situ alloyed by induction-assisted laser-based directed energy deposition
- 2024
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In: Materials & design. - : Elsevier Ltd. - 0264-1275 .- 1873-4197. ; 238
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Journal article (peer-reviewed)abstract
- The development of new high temperature materials for coatings as well as structural components is an important topic to contribute to a higher efficiency and sustainability of e.g. gas turbine engines. One promising new class of high temperature materials are NiAl-based alloys. Within this study, the microstructure and microhardness of NiAl-Ta-Cr alloys with varying Cr and Ta content were investigated. Graded specimens were fabricated by laser-based directed energy deposition utilizing an in situ alloying approach by mixing elemental Ta and Cr as well as pre-alloyed NiAl powder. Thermodynamic calculations were performed to design the alloy compositions beforehand. Inductive preheating of the substrate was used to counter the challenge of cracking due to the high brittleness. The results show that the cracking decreases with increasing preheating temperature. However, even at 700 °C, the cracking cannot be fully eliminated. Scanning electron microscopy, X-ray diffraction and electron backscatter diffraction revealed the formation of the phases B2-NiAl, A2-Cr and C14-NiAlTa within NiAl-Ta and NiAl-Cr alloys. For NiAl-Ta-Cr compositions, deviations regarding the phase formation between calculation and experiment were observed. Maximum hardness values were achieved within the NiAl-Ta and NiAl-Ta-Cr systems for the eutectic compositions at 14 at.-% Ta with maximum values above 900 HV0.1.
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| 14. |
- Seidel, André, et al.
(author)
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Added value by hybrid additive manufacturing and advanced manufacturing approaches
- 2018
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In: Journal of laser applications. - : American Institute of Physics (AIP). - 1042-346X .- 1938-1387. ; 26:2, s. 6-8
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Journal article (peer-reviewed)abstract
- In order to lead to a competitive advantage, there is the need to carefully consider the pros and cons of state-of-the-art manufacturing techniques. This is frequently carried out in a competitive manner, but can also be done in a complementary way. This complementary approach is often used for the processing of difficult-to-machine materials with particular regard to high-tech parts or components. Hybrid machining processes or, more general, advanced machining processes can be brought to the point that the results would not be possible with the individual constituent processes in isolation [Hybrid Machining Processes Perspectives on Machining and Finishing (Springer International Publishing AG, 2016)]. Hence, the controlled interaction of process mechanisms and/or energy sources is frequently applied for a significant increase of the process performance [Advanced Machining Processes of Metallic Materials: Theory, Modelling, and Applications, 2nd ed. (2016)] and will be addressed within the present paper. A via electron beam melting manufactured gamma titanium aluminide nozzle is extended and adapted. This is done via hybrid laser metal deposition. The presented approach considers critical impacts like processing temperatures, temperature gradients, and solidification conditions with particular regard to crucial material properties like the phenomena of lamellar interface cracking [Laser-Based Manufacturing of Components using Materials with High Cracking Susceptibility (Laser Institute of America–LIA), pp. 586–592; Ti-2015: The 13th World Conference on Titanium, Symposium 5]. Furthermore, selected destructive and non-destructive testing is performed in order to prove the material properties. Finally, the results will be evaluated. This will also be done in the perspective of other applications.
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| 15. |
- Seidel, André, et al.
(author)
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Intrinsic Heat Treatment Within Additive Manufacturing of Gamma Titanium Aluminide Space Hardware
- 2019
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In: JOM. - : Springer. - 1047-4838 .- 1543-1851. ; 71:4, s. 1513-1519
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Journal article (peer-reviewed)abstract
- A major part of laser additive manufacturing focuses on the fabrication of metallic parts for applications in the space and aerospace sectors. Especially, the processing of the very brittle titanium aluminides can be particularly challenging because of their distinct tendency to lamellar interface cracking. In the present paper, a gamma titanium aluminide (γ-TiAl) nozzle, manufactured via electron beam melting, is extended and adapted via hybrid laser metal deposition. The presented example considers a new field of application for this class of materials and approaches the process-specific manipulation of the composition and/or microstructure via the adjustment of processing temperatures, temperature gradients and solidification conditions. Furthermore, intrinsic heat treatment is investigated for electron beam melting and laser metal deposition with powder, and the resulting influence is releated to conventional processing.
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| 16. |
- Selbmann, Alex, et al.
(author)
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Mechanical and geometrical characterization of additively manufactured INCONEL® 718 porous structures for transpiration cooling in space applications
- 2022
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In: Laser 3D Manufacturing IX. - : SPIE - International Society for Optical Engineering.
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Conference paper (peer-reviewed)abstract
- The need for ever increasing process temperatures during combustion in space engines and gas turbines to increase efficiency requires the use of thermally resistant materials and novel cooling solutions. For the improved cooling of thermally highly stressed components, the technology of transpiration cooling, in which a cooling medium flows through a porous structure, has been known for a long time. Additive manufacturing and, in particular, laser powder bed fusion (LPBF) offers great potential for the near-net-shape production of porous structures compared to complex conventional manufacturing. In this contribution, porous structures were manufactured and the process parameters were optimized to increase the quality of the pores. The study discloses an adapted exposure parameter set for the improved fabrication of cylindrical pores in an INCONEL® 718 material and the associated mechanical properties of porous and dense components.
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