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  • Soldatov, Alexander, et al. (author)
  • Topochemical polymerization of C70 controlled by monomer crystal packing
  • 2001
  • In: Science. - : American Association for the Advanement of Science. - 0036-8075 .- 1095-9203. ; 293:5530, s. 680-683
  • Journal article (peer-reviewed)abstract
    • Polymeric forms of C60 are now well known, but numerous attempts to obtain C70 in a polymeric state have yielded only dimers. Polymeric C70 has now been synthesized by treatment of hexagonally packed C70 single crystals under moderate hydrostatic pressure (2 gigapascals) at elevated temperature (300°C), which confirms predictions from our modeling of polymeric structures of C70. Single-crystal x-ray diffraction shows that the molecules are bridged into polymeric zigzag chains that extend along the c axis of the parent structure. Solid-state nuclear magnetic resonance and Raman data provide evidence for covalent chemical bonding between the C70 cages.
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