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  • Mockuté, Aurelija, et al. (author)
  • Age hardening in (Ti1-xAlx)B2+Delta thin films
  • 2017
  • In: Scripta Materialia. - : Elsevier BV. - 1359-6462 .- 1872-8456. ; 127, s. 122-126
  • Journal article (peer-reviewed)abstract
    • Thin films of (Ti0.71Al0.29)B2+1.08 have been deposited by magnetron sputtering. Post-deposition annealing at 1000 degrees C for 1 h results in increased hardness and elastic modulus, from 32 to 37 GPa and from 436 to 461 GPa, respectively. In both as-deposited and annealed states the films adhere well to the substrate, indicating no considerable internal stress. The initial high hardness is attributed to a columnar microstructure consisting of crystalline (Ti,Al)B-2 columns separated by an amorphous B matrix. The observed age hardening corresponds to phase separation within the (Ti,Al)B-2 columns including the formation of Ti-deficient crystallites within the grain interior upon annealing.
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