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Search: WFRF:(Hawthorne A) > (2005-2009)

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1.
  • Abdu, Y. A., et al. (author)
  • High-temperature cation ordering in olivine : an in situ Mossbauer study of synthetic (Mg0.55Fe0.45)(2) SiO4
  • 2008
  • In: Hyperfine Interactions. - : Springer Science and Business Media LLC. - 0304-3843 .- 1572-9540. ; 186:1-3, s. 99-103
  • Journal article (peer-reviewed)abstract
    • High- temperature in situ Mossbauer spectroscopy measurements ( 300 950. C) were done on synthetic olivine of composition ( Mg0.55Fe0.45) 2 SiO4 (= Fa45) in order to study the distribution of Fe2+ over the M1 and M2 octahedral sites. The spectra are fit with two doublets, which are assigned to Fe2+ at the M1 ( smaller splitting) and M2 sites. The Fe2+ site- occupancies at M1 and M2, obtained from the Mossbauer relative areas, suggest that Fe2+ has a slight preference for the M1 site at temperatures below similar to 500. C, with a tendency of disordering around this temperature. At higher temperatures, Fe2+ again prefers to occupy the M1 site, where it shows a considerable order at this site up to 750C. At still higher temperatures, the spectra indicated partial reduction of the Fa- component into metallic iron and the resolution of the doublets was severely deteriorated.
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