| 1. |
- Jiang, S., et al.
(author)
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Micromechanical behavior of multilayered Ti/Nb composites processed by accumulative roll bonding : An in-situ synchrotron X-ray diffraction investigation
- 2021
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In: Acta Materialia. - Oxford, United Kingdom : Elsevier. - 1359-6454 .- 1873-2453. ; 205
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Journal article (peer-reviewed)abstract
- Heterophase interfaces play a crucial role in deformation microstructures and thus govern mechanical properties of multilayered composites. Here, we fabricated Ti/Nb multilayers by accumulative roll bonding (ARB) where shear bands became predominant with increasing rolling cycles. To explore correlation between micromechanical behavior and mechanical properties of the composites with various lamellar morphologies, in-situ high-energy X-ray diffraction tensile tests were performed. The results quantitatively reveal that the rapid strengthening of the composites with increasing ARB cycles mainly originates from the Nb layers strengthened by dislocations, grain boundaries and heterophase interfaces, and the {211} grains mostly contribute to the global strain hardening. The softer Ti grains also extend global strain hardening to a wide range and postpone necking. Furthermore, complete stress state analysis show that in the presence of extensive shear bands, significant load partitioning between the neighboring metals leads to triaxial stresses in each constituent and dislocations tend to slip along the shear direction. This promotes dislocation multiplication and motion, which is conducive to overall strength enhancement while maintaining a satisfactory ductility. These findings elucidate the effect of strong constraints of the interfaces on mechanical properties, which provides a fundamental understanding of load partitioning and strengthening mechanisms of the multilayers processed by multiple ARB cycles.
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| 2. |
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| 3. |
- Nilsson, Karin H., et al.
(author)
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RSPO3 is important for trabecular bone and fracture risk in mice and humans
- 2021
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In: Nature Communications. - : Springer Science and Business Media LLC. - 2041-1723. ; 12:1
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Journal article (peer-reviewed)abstract
- Genetic association signals for fractures have been reported at the RSPO3 locus, but the causal gene and the underlying mechanism are unknown. Here, the authors show that RSPO3 exerts an important role for vertebral trabecular bone mass and bone strength in mice and fracture risk in humans. With increasing age of the population, countries across the globe are facing a substantial increase in osteoporotic fractures. Genetic association signals for fractures have been reported at the RSPO3 locus, but the causal gene and the underlying mechanism are unknown. Here we show that the fracture reducing allele at the RSPO3 locus associate with increased RSPO3 expression both at the mRNA and protein levels, increased trabecular bone mineral density and reduced risk mainly of distal forearm fractures in humans. We also demonstrate that RSPO3 is expressed in osteoprogenitor cells and osteoblasts and that osteoblast-derived RSPO3 is the principal source of RSPO3 in bone and an important regulator of vertebral trabecular bone mass and bone strength in adult mice. Mechanistic studies revealed that RSPO3 in a cell-autonomous manner increases osteoblast proliferation and differentiation. In conclusion, RSPO3 regulates vertebral trabecular bone mass and bone strength in mice and fracture risk in humans.
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| 4. |
- Palmert, Frans, 1986-
(author)
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Crack growth in single crystal gas turbine blade alloys under service-like conditions
- 2022
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Doctoral thesis (other academic/artistic)abstract
- This work concerns the fatigue crack growth behaviour of nickel base single crystal superalloys. The main industrial application of this class of materials is in gas turbine blades, where the ability to withstand severe mechanical loading in combination with high temperatures is required. In order to ensure the structural integrity of gas turbine blades, knowledge of the fatigue crack growth behaviour under service-like conditions is of utmost importance. The aim of the present work is both to improve the understanding of the crack growth behaviour of single crystal superalloys and to improve the testing and evaluation methodology for crack propagation under thermomechanical fatigue loading conditions. Single crystal superalloys have anisotropic mechanical properties and are prone to localization of inelastic deformation along the close packed planes of the crystal lattice. Under some conditions, crystallographic crack growth occurs along these planes, and this is a complicating factor throughout the whole chain of crack propagation life simulation; from material data generation to component calculation. Crack growth testing has been performed, both using conventional isothermal testing methods and using thermomechanical fatigue crack growth testing. Experimental observations regarding crystallographic crack growth have been made and its dependence on crystal orientation and testing temperature has been investigated. Quantitative crack growth data are presented for the case of Mode I crack growth under isothermal as well as thermomechanical fatigue conditions. Microstructural investigations have been undertaken to investigate the deformation mechanisms governing the crack growth behaviour. A compliance-based method for the evaluation of crack opening force under thermomechanical fatigue conditions was developed, to enable a detailed analysis of the test data. The crack opening force evaluation proved to be of key importance for the understanding of the crack driving force under different testing conditions. The influence of hold time on crack growth behaviour was analysed, both in terms of creep crack growth and in terms of creep effects on the crack opening force. The transition between non-crystallographic and crystallographic crack growth was studied in detail and a criterion was developed to enable accurate predictions of this transition under a wide range of loading conditions representative for gas turbine blades.
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| 5. |
- Pauzon, Camille Nicole Géraldine, 1994, et al.
(author)
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Effect of layer thickness on spatter properties during laser powder bed fusion of Ti–6Al–4V
- 2023
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In: Powder Metallurgy. - : Informa UK Limited. - 0032-5899 .- 1743-2901. ; 66:4, s. 333-342
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Journal article (peer-reviewed)abstract
- High layer thicknesses for laser powder bed fusion are promising for productivity increase. However, these are associated with increased process instability, spatter generation and powder degradation, crucial for alloys sensitive to oxygen. The effect of increasing layer thickness from 30 to 60 µm is studied focusing on Ti-6Al-4V spatter formation during LPBF and its characterisation, with scanning and transmission electron microscopy, combustion analysis and X-ray photoelectron spectroscopy. Results indicate that spatters are covered with a uniform Ti-Al-based oxide layer and Al-rich oxide particulates, the thickness of which is about twice that present on virgin powder. The oxygen content was about 60% higher in spatters compared to the virgin powder. The study highlights that increasing the layer thickness to 60 µm permits to reduce the total generation of spatters by ∼40%, while maintaining similar spatter characteristics and static tensile properties. Hence, this allows to increase build rate without compromising process robustness.
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| 6. |
- Stekovic, Svjetlana, et al.
(author)
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DevTMF - Towards code of practice for thermo-mechanical fatigue crack growth
- 2020
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In: International Journal of Fatigue. - : ELSEVIER SCI LTD. - 0142-1123 .- 1879-3452. ; 138
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Journal article (peer-reviewed)abstract
- The current paper presents work on identification and evaluation of a range of factors influencing accuracy and comparability of data generated by three laboratories carrying out stress-controlled thermo-mechanical fatigue crack growth tests. It addresses crack length measurements, heating methods and temperature measurement techniques. It also provides guidance for pre-cracking and use of different specimen geometries as well as Digital Image Correlation imaging for crack monitoring. The majority of the tests have been carried out on a coarse grain polycrystalline nickel-base superalloy using two phase angles, Out-of-Phase and In-Phase cycles with a triangular waveform and a temperature range of 400-750 degrees C.
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