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Isolation and struc...
Isolation and structural elucidation by 2D NMR of planteose, a major oligosaccharide in the mucilage of chia (Salvia hispanica L.) seeds
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- Xing, Xiaohui (author)
- KTH,Glykovetenskap,University of Adelaide, Australia
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- Hsieh, Yves S.Y. (author)
- KTH,Glykovetenskap,Wallenberg Wood Science Center
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Yap, Kuok (author)
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Ang, Main E. (author)
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Lahnstein, Jelle (author)
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Tucker, Matthew R. (author)
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Burton, Rachel A. (author)
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- Bulone, Vincent (author)
- KTH,Glykovetenskap,Wallenberg Wood Science Center,University of Adelaide, Australia
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(creator_code:org_t)
- Elsevier, 2017
- 2017
- English.
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In: Carbohydrate Polymers. - : Elsevier. - 0144-8617 .- 1879-1344. ; 175, s. 231-240
- Related links:
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Subject headings
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- An oligosaccharide was isolated in high purity and excellent yield from the water-extractable mucilage of chia (Salvia hispanica L.) seeds using an optimized solid-phase extraction method. LC–MS analysis showed that the compound presents a molecular mass of 504 Da and trifluoroacetic acid hydrolysis revealed that it consists of galactose, glucose and fructose. Glycosidic linkage analysis showed that the oligosaccharide contains two non-reducing ends corresponding to terminal glucopyranose and terminal galactopyranose, respectively. The oligosaccharide was identified as planteose by the complete assignment of a series of 2D NMR spectra (COSY, TOCSY, ROESY, HSQC, and HMBC). The significance of the presence of planteose in chia seeds is discussed in the context of nutrition and food applications.
Subject headings
- NATURVETENSKAP -- Kemi -- Analytisk kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences -- Analytical Chemistry (hsv//eng)
- LANTBRUKSVETENSKAPER -- Lantbruksvetenskap, skogsbruk och fiske -- Livsmedelsvetenskap (hsv//swe)
- AGRICULTURAL SCIENCES -- Agriculture, Forestry and Fisheries -- Food Science (hsv//eng)
Keyword
- L
- Chia
- Seed mucilage
- Planteose
- Solid-phase extraction
- NMR
Publication and Content Type
- ref (subject category)
- art (subject category)
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