Synthesis, characterization and optical power limiting behaviour of phenylazo- and 4-nitrophenylazo-tetrahydroxytetrathiacalix[4]arene

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Desroches, CUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)

Synthesis, characterization and optical power limiting behaviour of phenylazo- and 4-nitrophenylazo-tetrahydroxytetrathiacalix[4]arene

Article/chapterEnglish2001

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2001
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LIBRIS-ID:oai:DiVA.org:liu-49047
https://urn.kb.se/resolve?urn=urn:nbn:se:liu:diva-49047URI

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Language:English
Summary in:English

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p-Tetrakis(4-nitrophenylazo) tetrahydroxytetrathiacalix[4] arene and p-tetrakis(phenylazo) tetrahydroxytetrathiacalix[4] arene were prepared and fully characterized using H-1 and C-13 NMR, mass spectroscopy, thermogravimetric analysis and differential scanning calorimetry. The solid-state structure of p-tetrakis(4-nitrophenylazo) tetrahydroxytetrathiacalix[4] arene was investigated by single crystal X-ray diffraction. It crystallized in the triclinic system (space group: P (1) over bar). z-Scan experiments were performed on the p-tetrakis(4-nitrophenylazo) tetrahydroxytetrathiacalix[ 4] arene showing non linear absorption due to two photon absorption with a TPA cross-section of about 50 x 10(-50) cm(4) s per photon. Optical power limiting measurements on the p-tetrakis( phenylazo) tetrahydroxytetrathiacalix[ 4] arene at 532 nm (48% linear transmission) was found to limit the energy to similar to9 muJ.

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NATURAL SCIENCES
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Parola, SUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)
Vocanson, FUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)
Ehlinger, NUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)
Miele, PUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)
Lamartine, RUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)
Bouix, JUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)
Eriksson, A (author)
Lindgren, M (author)
Lopes, CUniv Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (author)
Univ Lyon 1, CNRS, UMR 5615, Lab Multimat & Interfaces, F-69622 Villeurbanne, France Swedish Def Res Agcy FOI, Div Sensor Technol, SE-58111 Linkoping, Sweden Univ Lyon 1, CNRS, UMR 5078, Lab Synth & Reconnaissance & Org Mol & Biomol, F-69622 Villeurbanne, France (creator_code:org_t)

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In:Journal of Materials Chemistry11:12, s. 3014-30170959-94281364-5501

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By the author/editor: Desroches, C; Parola, S; Vocanson, F; Ehlinger, N; Miele, P; Lamartine, R; show more...; Bouix, J; Eriksson, A; Lindgren, M; Lopes, C; show less...

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