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- Hsu, Ying-JuiUmeå universitet,Institutionen för fysik (author)
Development of a high pressure stirring cell up to 2 GPa : a new window for chemical reactions and material synthesis
- Article/chapterEnglish2020
Publisher, publication year, extent ...
- 2020-06-05
- Informa UK Limited,2020
- printrdacarrier
Numbers
- LIBRIS-ID:oai:DiVA.org:su-183667
- https://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-183667URI
- https://doi.org/10.1080/08957959.2020.1775200DOI
- https://urn.kb.se/resolve?urn=urn:nbn:se:umu:diva-173446URI
Supplementary language notes
- Language:English
- Summary in:English
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- SwePubSwePub
Classification
Notes
- A new method for stirring under high pressure conditions has been developed and tested. The key component is a Teflon cell assembly equipped with magnetic stirring function, which is capable to operate across a wide pressure range, up to at least 2 GPa, in a large volume press. The setup enables adjustable stirrer rotation rate and detection of stirring in a sample,e.g.to observe liquid-solid phase transitions at high pressure. The viscosity limit of stirring is ca. 500 times that of water at room temperature (i.e.similar to 500 mPas). Moreover, we show that zinc oxide nanoparticles hydrothermally synthesized at 0.5 GPa and 100 degrees C under stirring conditions show an order of magnitude smaller size (100 nm) compared to those synthesized under non-stirring conditions (1 mu m). The wide pressure range for stirring of viscous media opens interesting possibilities to produce novel materials via hydrothermal synthesis and chemical reactions.
Subject headings and genre
- NATURVETENSKAP Kemi hsv//swe
- NATURAL SCIENCES Chemical Sciences hsv//eng
- NATURVETENSKAP Fysik hsv//swe
- NATURAL SCIENCES Physical Sciences hsv//eng
- NATURVETENSKAP Fysik Den kondenserade materiens fysik hsv//swe
- NATURAL SCIENCES Physical Sciences Condensed Matter Physics hsv//eng
- Magnetic stirring
- hydrothermal synthesis
- high pressure
- metal oxide
Added entries (persons, corporate bodies, meetings, titles ...)
- Gordeeva, AlisaStockholms universitet,Institutionen för material- och miljökemi (MMK)(Swepub:su)algo1633 (author)
- Antlauf, MathisUmeå universitet,Institutionen för fysik(Swepub:umu)maan1028 (author)
- Häussermann, UlrichStockholms universitet,Institutionen för material- och miljökemi (MMK)(Swepub:su)ulrich (author)
- Andersson, OveUmeå universitet,Institutionen för fysik(Swepub:umu)ovan0001 (author)
- Umeå universitetInstitutionen för fysik (creator_code:org_t)
Related titles
- In:High Pressure Research: Informa UK Limited40:3, s. 358-3680895-79591477-2299
Internet link
- https://doi.org/10.1080/08957959.2020.1775200Fulltext
- https://www.tandfonline.com/doi/pdf/10.1080/08957959.2020.1775200?needAccess=true
- https://umu.diva-portal.org/smash/get/diva2:1453466/FULLTEXT02.pdffulltext:print
- https://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-183667
- https://doi.org/10.1080/08957959.2020.1775200
- https://urn.kb.se/resolve?urn=urn:nbn:se:umu:diva-173446
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