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Liquid-liquid/solid...
Liquid-liquid/solid three-phase high-speed counter-current chromatography, a new technique for separation of polyphenols from Geranium wilfordii Maxim
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Liu, Dan (author)
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Ma, Yan (author)
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Gu, Ming (author)
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- Janson, Jan-Christer (author)
- Uppsala universitet,Analytisk kemi
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Wang, Changhai (author)
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Xiao, Hongbin (author)
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(creator_code:org_t)
- 2012-07-20
- 2012
- English.
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In: Journal of Separation Science. - : Wiley. - 1615-9306 .- 1615-9314. ; 35:16, s. 2146-2151
- Related links:
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Subject headings
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- High-speed counter-current chromatography using a new liquidliquid/solid three-phase system was used for the separation of the polyphenols corilagin and geraniin from a crude extract of Geranium wilfordii Maxim in one step. The optimized three-phase system was composed of n-hexane/ethyl acetate/methanol/acetic acid/water and to which was added 10-mu m average diameter microspheres of cross-linked 12% agarose at the ratio of 0.2:10:2:1:5 and 0.1 g/mL, respectively. The purities of geraniin and corilagin were 82 and 90%, which were determined by HPLC at 280 nm. A 14.5 and 7 mg of geraniin and corilagin were purified from 160 mg crude extract with the yields of 70 and 78%, respectively.
Subject headings
- NATURVETENSKAP -- Kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences (hsv//eng)
Keyword
- Corilagin
- Geraniin
- High-speed counter-current chromatography
- Liquid-liquid
- solid three-phase system
- Polyphenols
Publication and Content Type
- ref (subject category)
- art (subject category)
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