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Influence of heat pretreatment on ultrafiltration of a solution containing hemicelluloses extracted from wheat bran

Arkell, Anders (author)
Lund University,Lunds universitet,Avdelningen för kemiteknik,Institutionen för processteknik och tillämpad biovetenskap,Institutioner vid LTH,Lunds Tekniska Högskola,Division of Chemical Engineering,Department of Process and Life Science Engineering,Departments at LTH,Faculty of Engineering, LTH
Krawczyk, Holger (author)
Lund University,Lunds universitet,Avdelningen för kemiteknik,Institutionen för processteknik och tillämpad biovetenskap,Institutioner vid LTH,Lunds Tekniska Högskola,Division of Chemical Engineering,Department of Process and Life Science Engineering,Departments at LTH,Faculty of Engineering, LTH
Jönsson, Ann-Sofi (author)
Lund University,Lunds universitet,Avdelningen för kemiteknik,Institutionen för processteknik och tillämpad biovetenskap,Institutioner vid LTH,Lunds Tekniska Högskola,Division of Chemical Engineering,Department of Process and Life Science Engineering,Departments at LTH,Faculty of Engineering, LTH
 (creator_code:org_t)
Elsevier BV, 2013
2013
English.
In: Separation and Purification Technology. - : Elsevier BV. - 1873-3794 .- 1383-5866. ; 119, s. 46-50
  • Journal article (peer-reviewed)
Abstract Subject headings
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  • Hemicelluloses extracted from wheat bran can be concentrated and purified by ultrafiltration. However, the viscosity of the process solution is rather high (about 5 mPa s at 80 C and a shear rate of 100 s1), which results in a relatively low flux. The solution was subjected to heat pretreatment in an attempt to decrease the viscosity and increase the flux. Pretreatment of the solution at 80 C for 72 h was found to reduce the viscosity by 25%. The flux during ultrafiltration with a 10 kDa ceramic membrane increased from 48 l/m2 h, for the untreated solution, to 62 l/m2 h. The increase in flux was lower than expected, and this was attributed to the formation of a fouling layer of acid-insoluble compounds on the membrane. Both hemicelluloses and lignin were partly degraded. The retention of lignin was reduced from about 30% to 18%, whereas the retention of hemicelluloses was above 95%, and was not affected by heat pretreatment. The decrease in lignin retention after heat pretreatment results in improved separation of hemicelluloses and lignin, facilitating the purification of hemicelluloses.

Subject headings

TEKNIK OCH TEKNOLOGIER  -- Kemiteknik (hsv//swe)
ENGINEERING AND TECHNOLOGY  -- Chemical Engineering (hsv//eng)

Keyword

Ultrafiltration
Ceramic membrane
Hemicelluloses
Wheat bran
Heat pretreatment

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