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Time-of-Flight Thre...
Time-of-Flight Three Dimensional Neutron Diffraction in Transmission Mode for Mapping Crystal Grain Structures
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- Cereser, Alberto (author)
- Technical University of Denmark,European Spallation Source ESS AB
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- Strobl, Markus (author)
- Lund University,Lunds universitet,European Spallation Source ESS AB,Stiftelser och övriga anknutna verksamheter,Other Institutions and Utilities,University of Copenhagen
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- Hall, Stephen A. (author)
- Lund University,Lunds universitet,Hållfasthetslära,Institutionen för byggvetenskaper,Institutioner vid LTH,Lunds Tekniska Högskola,European Spallation Source ESS AB,Stiftelser och övriga anknutna verksamheter,Solid Mechanics,Department of Construction Sciences,Departments at LTH,Faculty of Engineering, LTH,Other Institutions and Utilities
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- Steuwer, Axel (author)
- Nelson Mandela Metropolitan University,University of Malta
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- Kiyanagi, Ryoji (author)
- Japan Atomic Energy Agency
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- Tremsin, Anton S (author)
- University of California, Berkeley
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- Knudsen, Knud Erik Bach (author)
- Technical University of Denmark
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- Shinohara, Takenao (author)
- Japan Atomic Energy Agency
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- Willendrup, Peter K. (author)
- Technical University of Denmark
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- Da Silva Fanta, Alice Bastos (author)
- Technical University of Denmark
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- Iyengar, Srinivasan (author)
- Lund University,Lunds universitet,Materialteknik,Institutionen för maskinvetenskaper,Institutioner vid LTH,Lunds Tekniska Högskola,Materials Engineering,Department of Mechanical Engineering Sciences,Departments at LTH,Faculty of Engineering, LTH,European Spallation Source ESS AB
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- Larsen, Peter Mose (author)
- Technical University of Denmark
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- Hanashima, Takayasu (author)
- Research Center for Neutron Science and Technology
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- Moyoshi, Taketo (author)
- Research Center for Neutron Science and Technology
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- Kadletz, Peter M. (author)
- Ludwig-Maximilian University of Munich
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- Krooß, Philipp (author)
- University of Kassel
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- Niendorf, Thomas (author)
- University of Kassel
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- Sales, Morten (author)
- Technical University of Denmark
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- Schmahl, Wolfgang W. (author)
- Ludwig-Maximilian University of Munich
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- Schmidt, Søren (author)
- Technical University of Denmark
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(creator_code:org_t)
- 2017-08-25
- 2017
- English.
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In: Scientific Reports. - : Springer Science and Business Media LLC. - 2045-2322. ; 7:1
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Abstract
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- The physical properties of polycrystalline materials depend on their microstructure, which is the nano- to centimeter scale arrangement of phases and defects in their interior. Such microstructure depends on the shape, crystallographic phase and orientation, and interfacing of the grains constituting the material. This article presents a new non-destructive 3D technique to study centimeter-sized bulk samples with a spatial resolution of hundred micrometers: time-of-flight three-dimensional neutron diffraction (ToF 3DND). Compared to existing analogous X-ray diffraction techniques, ToF 3DND enables studies of samples that can be both larger in size and made of heavier elements. Moreover, ToF 3DND facilitates the use of complicated sample environments. The basic ToF 3DND setup, utilizing an imaging detector with high spatial and temporal resolution, can easily be implemented at a time-of-flight neutron beamline. The technique was developed and tested with data collected at the Materials and Life Science Experimental Facility of the Japan Proton Accelerator Complex (J-PARC) for an iron sample. We successfully reconstructed the shape of 108 grains and developed an indexing procedure. The reconstruction algorithms have been validated by reconstructing two stacked Co-Ni-Ga single crystals, and by comparison with a grain map obtained by post-mortem electron backscatter diffraction (EBSD).
Subject headings
- TEKNIK OCH TEKNOLOGIER -- Materialteknik (hsv//swe)
- ENGINEERING AND TECHNOLOGY -- Materials Engineering (hsv//eng)
Publication and Content Type
- art (subject category)
- ref (subject category)
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- By the author/editor
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Cereser, Alberto
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Strobl, Markus
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Hall, Stephen A.
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Steuwer, Axel
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Kiyanagi, Ryoji
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Tremsin, Anton S
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show more...
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Knudsen, Knud Er ...
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Shinohara, Taken ...
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Willendrup, Pete ...
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Da Silva Fanta, ...
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Iyengar, Sriniva ...
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Larsen, Peter Mo ...
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Hanashima, Takay ...
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Moyoshi, Taketo
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Kadletz, Peter M ...
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Krooß, Philipp
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Niendorf, Thomas
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Sales, Morten
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Schmahl, Wolfgan ...
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Schmidt, Søren
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- ENGINEERING AND TECHNOLOGY
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ENGINEERING AND ...
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and Materials Engine ...
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Lund University