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Revealing Three-Dimensional Structure of an Individual Colloidal Crystal Grain by Coherent X-Ray Diffractive Imaging

Shabalin, A. G. (author)
P.N. Lebedev Physical Institute of the Russian Academy of Sciences,German Electron Synchrotron (DESY)
Meijer, J. M. (author)
Lund University,Lunds universitet,Fysikalisk kemi,Enheten för fysikalisk och teoretisk kemi,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Physical Chemistry,Physical and theoretical chemistry,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH,Utrecht University
Dronyak, R. (author)
German Electron Synchrotron (DESY)
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Yefanov, O. M. (author)
German Electron Synchrotron (DESY)
Singer, A. (author)
University of California, San Diego,German Electron Synchrotron (DESY)
Kurta, R. P. (author)
German Electron Synchrotron (DESY),European XFEL GmbH
Lorenz, U. (author)
German Electron Synchrotron (DESY)
Gorobtsov, O. Y. (author)
Russian Research Center 'Kurchatov Institute',German Electron Synchrotron (DESY)
Dzhigaev, D. (author)
National Research Nuclear University MEPhI,German Electron Synchrotron (DESY)
Kalbfleisch, S. (author)
University of Göttingen
Gulden, J. (author)
German Electron Synchrotron (DESY)
Zozulya, A. V. (author)
German Electron Synchrotron (DESY)
Sprung, M. (author)
German Electron Synchrotron (DESY)
Petukhov, A. V. (author)
Eindhoven University of Technology,Utrecht University
Vartanyants, I. A. (author)
National Research Nuclear University MEPhI,German Electron Synchrotron (DESY)
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PN. Lebedev Physical Institute of the Russian Academy of Sciences German Electron Synchrotron (DESY) (creator_code:org_t)
2016
2016
English.
In: Physical Review Letters. - 0031-9007. ; 117:13
  • Journal article (peer-reviewed)
Abstract Subject headings
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  • We present results of a coherent x-ray diffractive imaging experiment performed on a single colloidal crystal grain. The full three-dimensional (3D) reciprocal space map measured by an azimuthal rotational scan contained several orders of Bragg reflections together with the coherent interference signal between them. Applying the iterative phase retrieval approach, the 3D structure of the crystal grain was reconstructed and positions of individual colloidal particles were resolved. As a result, an exact stacking sequence of hexagonal close-packed layers including planar and linear defects were identified.

Subject headings

NATURVETENSKAP  -- Fysik -- Atom- och molekylfysik och optik (hsv//swe)
NATURAL SCIENCES  -- Physical Sciences -- Atom and Molecular Physics and Optics (hsv//eng)
NATURVETENSKAP  -- Kemi -- Fysikalisk kemi (hsv//swe)
NATURAL SCIENCES  -- Chemical Sciences -- Physical Chemistry (hsv//eng)

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