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High-pressure transformations of NbO2F
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- Carlson, Stefan (author)
- Lund University,Lunds universitet,MAX IV-laboratoriet,MAX IV Laboratory,European Synchrotron Radiation Facility
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- Larsson, Ann Kristin (author)
- Stockholm University
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- Rohrer, Franziska E. (author)
- Stockholm University
- (creator_code:org_t)
- 2000
- 2000
- English 8 s.
- In: Acta Crystallographica. Section B: Structural Science. - 0108-7681. ; 56:2, s. 189-196
- Journal article (peer-reviewed)
Abstract
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- The ReO3-type structure NbO2F, niobium dioxyfluoride, has been studied at high pressures using diamond anvil cells and synchrotron X-ray radiation. High-pressure powder diffraction measurements have been performed up to 40.1 GPa. A phase transition from the cubic (Pm3m) ambient pressure structure to a rhombohedral (R3c) structure at 0.47 GPa has been observed. Rietveld refinements at 1.38, 1.96, 3.20, 6.23, 9.00 and 10.5 GPa showed that the transition involves an a-a-a- tilting of the cation-anion coordination octahedra and a change of the anion-anion arrangement to approach hexagonal close packing. Compression and distortion of the Nb(O/F)6 octahedra is also revealed by the Rietveld refinements. At 17-18 GPa, the diffraction pattern disappears and the structure becomes X-ray amorphous.
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