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- Banerjee, Srutarshi, et al.
(författare)
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3D imaging of magnetic domains in Nd2Fe14B using scanning hard X-ray nanotomography
- 2024
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Ingår i: Journal of Synchrotron Radiation. - 0909-0495. ; 31:Pt 4, s. 877-887
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Tidskriftsartikel (refereegranskat)abstract
- Nanoscale structural and electronic heterogeneities are prevalent in condensed matter physics. Investigating these heterogeneities in 3D has become an important task for understanding material properties. To provide a tool to unravel the connection between nanoscale heterogeneity and macroscopic emergent properties in magnetic materials, scanning transmission X-ray microscopy (STXM) is combined with X-ray magnetic circular dichroism. A vector tomography algorithm has been developed to reconstruct the full 3D magnetic vector field without any prior noise assumptions or knowledge about the sample. Two tomographic scans around the vertical axis are acquired on single-crystalline Nd2Fe14B pillars tilted at two different angles, with 2D STXM projections recorded using a focused 120 nm X-ray beam with left and right circular polarization. Image alignment and iterative registration have been implemented based on the 2D STXM projections for the two tilts. Dichroic projections obtained from difference images are used for the tomographic reconstruction to obtain the 3D magnetization distribution at the nanoscale.
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| 2. |
- Hase, Thomas P. A., et al.
(författare)
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Proximity effects on dimensionality and magnetic ordering in Pd/Fe/Pd trialyers
- 2014
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Ingår i: Physical Review B. Condensed Matter and Materials Physics. - 1098-0121 .- 1550-235X. ; 90:10, s. 104403-
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Tidskriftsartikel (refereegranskat)abstract
- The element-specific magnetization and ordering in trilayers consisting of 0.3-1.4 monolayer (ML) thick Fe layers embedded in Pd(001) has been determined using x-ray resonant magnetic scattering. The proximity to Fe induces a large moment in the Pd which extends similar to 2 nm from the interfaces. The magnetization as a function of temperature is found to differ significantly for the Fe and Pd sublattices: The Pd signal resembles the results obtained by magneto-optical techniques with an apparent three-dimensional (3D) to two-dimensional (2D) transition in spatial dimensionality for Fe thickness below similar to 1 ML. In stark contrast, the Fe data exhibits a 2D behavior. No ferromagnetic signal is obtained from Fe below the 2D percolation limit in Fe coverage (similar to 0.7 ML), while Pd shows a ferromagnetic response for all samples. The results are attributed to the temperature dependence of the susceptibility of Pd and a profound local anisotropy of submonolayered Fe.
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