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- Paskova, Tanja, 1961-, et al.
(författare)
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Characterization of mass-transport grown GaN by hydride vapour-phase epitaxy
- 2004
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Ingår i: Journal of Crystal Growth. - : Elsevier BV. - 0022-0248 .- 1873-5002. ; 273:1-2, s. 118-128
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Tidskriftsartikel (refereegranskat)abstract
- A comprehensive study of the morphological, optical and microstructural properties of mass-transport (MT) and conventionally grown GaN by hydride vapour-phase epitaxy is presented. Spatially resolved techniques have been utilized to reveal in a comparative way, the characteristics of the material grown either in predominant vertical or lateral growth modes. A strong donor-acceptor pair (DAP) emission is observed from the MT regions with a distinctive intensity contrast between the exciton and DAP emission bands from MT and nontransport regions. Secondary ion mass spectroscopy and imaging were employed to investigate the impurity incorporation into different regions. An increase of residual oxygen and aluminium impurity concentrations was found in the MT areas. In addition, positron annihilation spectroscopy showed a strong signal of Ga vacancy clusters in the MT grown material. The increase of the point defect concentrations of both Ga vacancy and oxygen impurity, most likely forming defect complexes, is related to the enhancement of the DAP emission.
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- Eriksson, Magnus, et al.
(författare)
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New semi-isostatic high velocity compaction method to prepare titanium dental copings
- 2004
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Ingår i: Powder Metallurgy. - : Informa UK Limited. - 0032-5899 .- 1743-2901. ; 47:4, s. 335-342
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Tidskriftsartikel (refereegranskat)abstract
- A new method to prepare titanium dental copings from titanium powder was tested, involving high velocity compaction and various elastic forms, which were used to achieve a semi-isostatic effect during the impact. The tooth preparation die (mandrel) and the powder were placed inside an elastic form. The impact struck the elastic form, and the powder was compacted against the tooth preparation die. Several different elastomers were tested to find the best one. Cross-sections of the powder bodies were studied for density variations. The soft, flexible elastomer worked best to compact the powder. The highest densification could be focused closest to the mandrel where the coping should be milled out. The density in the highest density areas could locally reach 98-99%. If the method with elastic forms could be optimised to give as high a density as without elastic forms, a lower shrinkage and possible deformation of the copings could be reached.
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