| 1. |
- Dimitrios, Nikas, et al.
(författare)
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Effect of annealing on microstructure in railway wheel steel
- 2022
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Ingår i: 42Nd Riso International Symposium On Materials Science. - : Institute of Physics Publishing (IOPP). ; 1249
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Konferensbidrag (refereegranskat)abstract
- Railway wheels are commonly made from medium carbon steels (similar to 0.55 wt.% C), heat treated to a near pearlitic microstructure with 5-10% pro-eutectoid ferrite. During the operation of freight trains, where block brakes are used, high thermal loads occur together with the high contact stresses, which combined can affect the mechanical properties of the material. In this study, the effects of annealing on local microstructure and mechanical properties in pearlitic railway wheel steel were investigated using electron microscopy and micro-hardness. It is found that after annealing at 650 degrees C, the room temperature hardness reduces about 25%, accompanied by significant spheroidization of cementite in the pearlitic colonies, though the size and the orientation gradients of the pearlitic colonies have not changed much. The relationship between the microstructural changes and the mechanical properties are discussed.
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| 2. |
- Hosseini, Seyedehsan, 1994
(författare)
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Additive-Driven Improvements in Interfacial Properties and Processing of TMP-Polymer Composites
- 2023
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Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Efforts to address environmental concerns have resulted in new regulations designed to plan the reduction of plastic and synthetic polymer usage, necessitating the search for sustainable natural alternatives with comparable cost-effectiveness and mechanical performance. Thermomechanical pulp (TMP) fibres are one of the most affordable natural fibres that have no chemical refining in production, production have a high yield of 90-98% and TMP fibres have been demonstrated to improve the mechanical characteristics (strength, stiffness and toughness) of wood-polymer composites (WPCs) compared to the pure polymer. The integration of TMP fibres with non-polar synthetic polymers remains a challenge due to surface polarity differences. This PhD thesis aims to ease the processing of TMP fibre composites through the incorporation of additives. The hypothesis posits that incorporating magnesium stearate (MgSt), molybdenum disulfide (MoS2) and alkyl ketene dimer (AKD) as additives in TMP composites will enhance interfacial properties, resulting in improved processability and flow behaviour at high temperatures. MoS2 is known for its interaction with lignin, which exists in TMP and MgSt is recognised for its ability to improve flow in pharmaceutical processing when combined with cellulose, also a component of TMP. AKD modifies the hydrophilic properties of lignocellulosic surfaces. The experimental work explores the effect of these additives on the properties of TMP composites of ethylene acrylic acid copolymer (EAA) and polypropylene (PP) matrices. The dynamic mechanical analysis (DMA) and mechanical analysis results reveal that MoS2 exhibits superior interaction with TMP fibres, yielding enhanced interfacial properties compared to MgSt in between EAA and TMP fibres. Rheological studies elucidate the transition from a fluid-like state to a network-like structure upon the incorporation of TMP into the PP matrix. The incorporation of AKD with C18 reduces the viscosity of TMP-PP composites and PP itself, and, as determined through theoretical Hansen solubility parameter (HSP) calculations, increases compatibility between cellulose in TMP fibres and PP. The addition of AKD influences both the colour (lighter) and shape (smoother surface) of the extrudate filaments in the TMP-PP composites, indicative of improved processing. In addition, frictional analysis demonstrates the reduction of the coefficient of friction (COF) between metal and TMP fibre by MgSt and AKD treatments.
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| 3. |
- Guldris Leon, Lorena, 1983, et al.
(författare)
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Understanding Mineral Liberation during Crushing Using Grade-by-Size Analysis - A Case Study of the Penuota Sn-Ta Mineralization, Spain
- 2020
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Ingår i: Minerals. - : MDPI AG. - 2075-163X. ; 10:2
-
Tidskriftsartikel (refereegranskat)abstract
- Coarse comminution test-work and modeling are powerful tools in the design and optimization of mineral processing plants and provide information on energy consumption. Additional information on mineral liberation characteristics can be used for assessing the potential of pre-concentration stages or screens in the plant design. In ores of high-value metals (e.g., Ta, W), standard techniques-such as the mineralogical quantification of grain mounts by quantitative evaluation of minerals by scanning electron microscopy (QEMSCAN) or chemical analysis by X-ray fluorescence (XRF) can be challenging, due to the low relative abundance of such valuable minerals. The cost of QEMSCAN is also a limiting factor, especially considering the large number of samples required for the optimization of coarse comminution. In this study, we present an extended analytical protocol to a well-established mechanical test of interparticle breakage to improve the assessment of coarse mineral liberation characteristics. The liberation of ore minerals is a function of the rock texture and the difference in size and mechanical properties of the valuable minerals relative to gangue minerals and they may fraction in certain grain sizes if they behave differently during comminution. By analyzing the bulk-chemistry of the different grain size fractions produced after compressional testing, and by generating element by size diagrams, it is possible to understand the liberation characteristics of an ore. We show, based on a case study performed on a tantalum ore deposit, that element distribution can be used to study the influence of mechanical parameters on mineral liberation. This information can direct further mineralogical investigation and test work.
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| 4. |
- Koptyug, Andrey, 1956-, et al.
(författare)
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Electron Beam Melting: from Shape Freedom to Materials Properties Control at Macro- and Microscale
- 2021
-
Ingår i: Proceedings of the THERMEC 2020, Graz, Austria. - : Trans Tech Publications. ; , s. 755-759
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Konferensbidrag (refereegranskat)abstract
- Electron beam melting (EBM) is one of the constantly developing powder bed fusion (PBF) additive manufacturing technologies (AM) offering advanced control over the manufacturing process. Freedom of component shapes is one of the AM competitive advantages already used at industrial and semi- industrial scale. Development of the additive manufacturing today is targeting both widening of the available materials classes, and introducing new enabling modalities. Present research is related to the new possibilities in tailoring different material properties within additively manufactured components effectively adding “fourth dimension to the 3D-printing”. Specific examples are given in relation to the electron beam melting, but majority of the conclusions are valid for the laser-based PBF techniques as well. Through manipulating beam energy deposition it is possible to tailor quite different material properties selectively within each manufactured component, including effective material density as well as thermal, mechanical, electrical and acoustic properties. It is also possible to acquire by choice both metal-metal composite and completely alloyed material, when blends of precursor powder are used together with the beam energy manipulation.
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| 5. |
- Shaikh, Abdul Shaafi, 1989, et al.
(författare)
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On the effect of building platform material on laser-powder bed fusion of a Ni-base superalloy HAYNES® 282®
- 2023
-
Ingår i: European Journal of Materials. - : Informa UK Limited. - 2688-9277. ; 3:1
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Tidskriftsartikel (refereegranskat)abstract
- Additive manufacturing (AM) by laser powder bed fusion (LPBF) involves melting of layers of powder onto a substrate, called a building platform. Due to cost or convenience considerations, building platform materials rarely match the LPBF material, especially for high temperature materials. To ensure tolerances in component geometries, AM components are often stress-relieved/heat-treated while still attached to the building platform. It is therefore important to understand the effect of dissimilar building platform materials on the properties of the built-up material. These effects may be particularly important for high performance materials such as Ni-base superalloys used for critical applications in the aerospace and energy industries. To investigate this effect, samples of a Ni-base superalloy HAYNES® 282® were built onto a carbon steel building platform in several configurations. The samples were removed from the building platform after heat treatment and subjected to detailed composition analysis and microstructural characterization to investigate the effect of the building platform material on the properties of the additively manufactured part. Room temperature and high temperature tensile testing were used to characterize the material. Results showed no risk of large-scale chemical composition change, or mechanical property degradation of built-up material from on-platform heat treatment.
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| 6. |
- Vilardell, A. M., et al.
(författare)
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B2-structured Fe3Al alloy manufactured by laser powder bed fusion : Processing, microstructure and mechanical performance
- 2023
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Ingår i: Intermetallics (Barking). - : Elsevier. - 0966-9795 .- 1879-0216. ; 156
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Tidskriftsartikel (refereegranskat)abstract
- Prealloyed Fe3Al was successfully manufactured by laser powder bed fusion. The best set of process parameters led to parts with a relative density of 99.5 %, a surface roughness, Sa, of 31.5 ± 5.6 μm and a hardness of 319 ± 14 HV0.1. Its microstructure as well as its mechanical properties at room and high temperatures were analyzed. The results of the chemical composition showed minor variations in aluminum content oscillating between 21 and 28 at.% along the melt pool. Additionally, elongated grains were observed to grow parallel to the building direction, as well as the development of a weak 001 texture along the building direction. The mechanical properties were influenced by the temperature. Compression tests showed a loss in strength with the increase in temperature, from a yield strength of 621 ± 40 MPa at room temperature to 89 ± 20 MPa at 650 °C. Reciprocating sliding wear tests showed that fragmentation of the intermetallic at room temperature occurs, whereas plastic deformation dominated at higher temperatures. For all temperatures, tribochemical wear was also present due to the oxidation of wear debris.
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| 7. |
- Zhang, Yubin, et al.
(författare)
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Stress relief during annealing of railway wheel steel characterized by synchrotron X-ray micro-diffraction
- 2022
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Ingår i: 42nd Risø International Symposium on Materials Science. - : Institute of Physics Publishing (IOPP). ; 1249
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Konferensbidrag (refereegranskat)abstract
- Railway wheels in service experience rolling contact fatigue loading, but also need to resist frictional heating on braking, yielding temperatures up to 500 degrees C. The combination of mechanical and thermal loads leads to changes in the mechanical properties of the material. The focus of this study is to investigate the effect of annealing on local microstructure and residual stresses in railway wheel pearlitic steel (medium carbon steels, similar to 0.55 wt.% C) using synchroton X-ray Laue micro-diffraction. It is found that the local residual stress releases to a large extent after annealing at 500 degrees C. The stress formation and relief mechanisms and their relationship to the local microstructure are discussed.
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| 8. |
- Edin, Emil, et al.
(författare)
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Rapid method for comparative studies on stress relief heat treatment of additively manufactured 316L
- 2022
-
Ingår i: Materials Science & Engineering. - : Elsevier. - 0921-5093 .- 1873-4936. ; 847
-
Tidskriftsartikel (refereegranskat)abstract
- The additive manufacturing method laser powder bed fusion (L-PBF) is known to introduce large residual stresses in the built component. Optimization of process parameters and subsequent heat treatment is crucial to relieve these residual stresses. However, many of the available tools used to analyze these residual stresses are either prohibitively expensive, or too time consuming for initial prototyping stages.A qualitative method for rapid evaluation of the effectiveness of stress relief heat treatment of L-PBF manufactured 316L has been tested. Residual stress induced distortion has been measured with contact and non-contact methods to study the effect of different stress relief heat treatment temperatures (600 – 950 °C, fixed holding time: 1 h). Over the examined temperature interval, at which deformation was measured, distinct differences were observable at each temperature with both methods. Based on the distortion, shape stability was considered reached after subjecting the test geometry to a heat treatment temperature of 900 °C for 1 hour. Complementary mechanical testing and microstructural characterization were carried out to provide a more general understanding of the implications of each heat treatment temperature. Microstructural characterization revealed that complete dissolution of the cellular sub-grain features occurred at the same temperature as where the minimum magnitude of distortion was obtained.
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| 9. |
- Andersson, Anton, et al.
(författare)
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Ground granulated iron silicate slag as supplementary cementitious material: Effect of prolonged grinding and granulation temperature
- 2023
-
Ingår i: Cleaner Materials. - : Elsevier. - 2772-3976. ; 10
-
Tidskriftsartikel (refereegranskat)abstract
- The metallurgical and cement industries contribute significantly to anthropogenic carbon dioxide emissions. Utilizing oxidic by-products from the metallurgical industry as supplementary cementitious materials (SCMs) can improve resource efficiency and reduce emissions from cement production. Iron silicate copper slags have been studied as SCMs, but mainly in systems where Portland cement is used as an activator. There is limited research on the inherent reactivity of the slag under changing processing conditions. The present study offers insight into the effect of granulation temperature and grinding on the inherent reactivity of an industrially produced iron silicate copper slag. The results showed that granulation temperature had an insignificant effect on reactivity, while grinding generated substantial improvements. The latter effect was concluded to stem from the increased specific surface area, increased number of sites for nucleation and growth of hydrates, and changes in the inherent reactivity owing to structural changes induced by the grinding.
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| 10. |
- Krakhmalev, Pavel, 1973-, et al.
(författare)
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Influence of heat treatment under hot isostatic pressing (HIP) on microstructure of intermetallic-reinforced tool steel manufactured by laser powder bed fusion
- 2020
-
Ingår i: Materials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing. - : Elsevier BV. - 0921-5093 .- 1873-4936. ; 772
-
Tidskriftsartikel (refereegranskat)abstract
- Microstructure and properties of as-built laser powder bed fusion (LPBF) steels differ from the conventional ones, and they may contain some porosity and lack of fusion. Therefore, post-treatments, including hot isostatic pressing (HIP), are used to density the material, and tailor the properties of the final product. Usually, HIP is performed as an operation separate from heat treatment. In the present investigation a new approach was used, in which the whole cycle of the heat treatment was carried out in HIP under pressure, and the influence of HIP on microstructure of an advanced stainless maraging tool steel manufactured by LPBF was investigated. For a comparison, a conventional steel grade of the same chemical composition, after a heat treatment at the same temperature-time conditions, was also characterized. The microstructure of the steel was investigated by means of advanced microscopy and atom probe tomography. The influence of the manufacturing route, heat treatment and HIP on microstructure, austenitic phase fraction and size distribution of precipitates was investigated, and the role of high pressure in stabilization of austenite in the microstructure was discussed. It was concluded that since HIP influences phase transformations, a fundamental understanding of the influence of HIP on microstructure is nececcary, and development of new post processing regimes guaranteeing the best performance of the material is required.
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| 11. |
- Xu, Jinghao, et al.
(författare)
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On the strengthening and embrittlement mechanisms of an additively manufactured Nickel-base superalloy
- 2020
-
Ingår i: Materialia. - : Elsevier BV. - 2589-1529. ; 10
-
Tidskriftsartikel (refereegranskat)abstract
- The γ′ phase strengthened Nickel-base superalloy is one of the most significant dual-phase alloy systems for high-temperature engineering applications. The tensile properties of laser powder-bed-fused IN738LC superalloy in the as-built state have been shown to have both good strength and ductility compared with its post-thermal treated state. A microstructural hierarchy composed of weak texture, sub-micron cellular structures and dislocation cellular walls was promoted in the as-built sample. After post-thermal treatment, the secondary phase γ′ precipitated with various size and fraction depending on heat treatment process. For room-temperature tensile tests, the dominated deformation mechanism is planar slip of dislocations in the as-built sample while dislocations bypassing the precipitates via Orowan looping in the γ′ strengthened samples. The extraordinary strengthening effect due to the dislocation substructure in the as-built sample provides an addition of 372 MPa in yield strength. The results of our calculation are in agreement with experimental yield strength for all the three different conditions investigated. Strikingly, the γ′ strengthened samples have higher work hardening rate than as-built sample but encounter premature failure. Experimental evidence shows that the embrittlement mechanism in the γ′ strengthened samples is caused by the high dislocation hardening of the grain interior region, which reduces the ability to accommodate further plastic strain and leads to premature intergranular cracking. On the basis of these results, the strengthening micromechanism and double-edge effect of strength and ductility of Nickel-base superalloy is discussed in detail.
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| 12. |
- Zia, Shafaq, et al.
(författare)
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Estimating manufacturing parameters of additively manufactured 316L steel cubes using ultrasound fingerprinting
- 2023
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Ingår i: Research and Review Journal of Nondestructive Testing (ReJNDT). - : NDT.net. - 2941-4989. ; 1:1
-
Tidskriftsartikel (refereegranskat)abstract
- Metal based additive manufacturing techniques such as laser powder bed fusion (LPBF) can produce parts with complex designs as compared to traditional manufacturing. The quality is affected by defects such as porosity or lack of fusion that can be reduced by online control of manufacturing parameters. The conventional way of testing is time consuming and does not allow the process parameters to be linked to the mechanical properties. In this paper, ultrasound data along with supervised learning is used to estimate the manufacturing parameters of 316L steel cubes. Nine cubes with varying manufacturing parameters (speed, hatch distance and power) are examined with ultrasound using focused transducers. The volumetric energy density (VED) is calculated from the process parameters for each cube. The ultrasound scans are performed in a dense grid in the built and transverse direction. The ultrasound data is used in partial least square regression algorithm by labelling the data with speed, hatch distance and power and then by labelling the same data with the VED. These models are computed for both measurement directions and as the samples are anisotropic, we see different behaviours of estimation in each direction. The model is then validated with an unknown set from the same 9 cubes. The manufacturing parameters are estimated and validated with a good accuracy making way for online process control.
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| 13. |
- Hanning, Fabian, et al.
(författare)
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The Effect of Grain Size on theSusceptibility Towards Strain Age Crackingof Wrought Haynes® 282®
- 2020
-
Ingår i: SPS 2020. - Amsterdam : IOS Press. - 9781643681467 - 9781643681474 ; 13, s. 407-416
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Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- The effect of grain size on the suceptibility towards strain age cracking (SAC) has been investigated for Haynes® 282® in the tempeature range of 750 to 950°C after isothermal exposure up to 1800s. Grain growth was induced by heattreating the material at 1150°C for 2h, resulting in a fourfold increase in grain size. Hardness was significanlty reduced after heat treatment as compared to millannealed material. Large grain size resulted in intergranular fracture over a widertemperature range than small grain size material. Ductility was lowest at 850°C, while lower values were observed to be correlated to increased grain size. The rapid formation of grain boundary carbide networks in Haynes® 282® is found to be notable to compensate for higher local stresses on grain boundaries due to incresedgrain size.
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| 14. |
- Qin, Xiao, 1993, et al.
(författare)
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Microstructure and texture evolutions in FeCrAl cladding tube during pilger processing
- 2023
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Ingår i: Journal of Materials Research and Technology. - 2238-7854. ; 25, s. 5506-5519
-
Tidskriftsartikel (refereegranskat)abstract
- The microstructure of FeCrAl cladding tubes depends on the fabricating process history. In this study, the microstructural characteristics of wrought FeCrAl alloys during industrial pilger processing into thin-walled tubes were investigated. The hot extruded tube showed ∼100 μm equiaxed grains with weak α∗-fiber in {h11}<1/h12> texture, while pilger rolling process change the microstructure to fragmented and elongated grains along the rolling direction. The pilgered textures could be predicted with the VPSC model. The inter-pass annealing at 800–850 °C for 1 h results in recovery and recrystallization of the ferric matrix and restoration of ductility. The final finished tube shows fine recrystallized grains (∼11 μm) with dominant γ-fiber in three dimensions. Pilger rolling enhanced α-fiber while annealing reduced α-fiber and enhanced γ-fiber. Microstructural evolution in the Laves precipitates followed the sequence of faceted needle-like → spherical → faceted ellipsoidal. Thermomechanical processing resulted in cladding tubes with an area fraction of ∼5% and a number density of 5 × 10−11 m−2 in Laves precipitates, which is half that of the first-pilgered tube. Laves precipitates pin the grain boundaries to control the microstructure and prevent grain coarsening.
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| 15. |
- Shoja, Siamak, 1980
(författare)
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Microstructure and plastic deformation of textured CVD alumina coatings
- 2020
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Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- It is known that the wear performance of α-alumina coatings produced by chemical vapor deposition (CVD) is significantly influenced by the type and degree of texture. However, the main reasons behind this behavior are not fully understood. This thesis contains studies of two related topics for increasing the understanding of α-alumina coatings. The first topic concerns the microstructure and texture development of CVD α-Al2O3 coatings, and the second topic concerns calculations and analysis of the Schmid factors ( m ) for coatings with different textures. By combining different analysis methods (such as XRD, SEM, FIB/SEM, TKD, TEM, STEM, XEDS), and theoretical and experimental Schmid factor analysis by MATLAB and EBSD, the microstructure and plastic deformation of α-alumina coatings were investigated. The microstructures of three different CVD α-Al2O3 layers deposited onto a Ti(C,N,O) bonding layer were studied. Grain boundary diffusion of heavy elements from the substrate to the bonding layer/α-Al2O3 interface was observed. This may be the cause of a disturbance in the early growth of α-Al2O3. Additionally, it was found that the number of interfacial pores at the bonding layer/α-Al2O3 interface increased by introducing the H2S gas. The H2S gas also promoted an earlier development of the (0001) texture. The orientation of the grains was developed to the desired texture both as a gradual change over several grains and as an abrupt transformation from one grain to another. The probability of plastic deformation in different wear zones on the rake face of a cutting tool was investigated theoretically and experimentally by analyzing Schmid factors for textured α-Al2O3 coatings. Schmid factor diagrams were constructed using MATLAB/MTEX and used to extract frequency distributions for different slip systems and textures. The results were compared with lateral distribution maps of Schmid factors obtained from experimental coatings. It was observed that basal slip is most easily activated in the transition zone, followed by prismatic slip systems 1 and 2 in coatings with an (0001)-texture. The homogeneous plastic deformation behavior observed in this coating is also connected to mostly high Schmid factors in the m -value distribution. The differences between the m -value distributions for the three slip systems are not that pronounced in the (01-12) and (11-20) textures, and the distributions are relatively wide. The low wear rate and more homogeneous deformation of the coating with (0001) texture compared to the other coating textures may be the result of the high plasticity, offered by the easy activation of basal slip and prismatic 1 slip, and the low spread of Schmid factor values at the transition zone. In conclusion, the results presented in this thesis form a knowledge platform that can be used to understand the microstructure and wear mechanisms of textured CVD α-alumina coatings.
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| 16. |
- Alvi, Sajid, et al.
(författare)
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Enhanced mechanical, thermal and electrical properties of high‐entropy HfMoNbTaTiVWZr thin film metallic glass and its nitrides
- 2022
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Ingår i: Advanced Engineering Materials. - : John Wiley & Sons. - 1438-1656 .- 1527-2648. ; 24:9
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Tidskriftsartikel (refereegranskat)abstract
- The inception of high-entropy alloy promises to push the boundaries for new alloy design with unprecedented properties. This work reports entropy stabilisation of an octonary refractory, HfMoNbTaTiVWZr, high-entropy thin film metallic glass, and derived nitride films. The thin film metallic glass exhibited exceptional ductility of ≈60% strain without fracture and compression strength of 3 GPa in micro-compression, due to the presence of high density and strength of bonds. The thin film metallic glass shows thermal stability up to 750 °C and resistance to Ar-ion irradiation. Nitriding during film deposition of HfMoNbTaTiVWZr thin film of strong nitride forming refractory elements results in deposition of nanocrystalline nitride films with compressive strength, hardness, and thermal stability of up to 10 GPa, 18.7 GPa, and 950 °C, respectively. The high amount of lattice distortion in the nitride films leads to its insulating behaviour with electrical conductivity as low as 200 S cm−1 in the as-deposited film. The design and exceptional properties of the thin film metallic glass and derived nitride films may open up new avenues of development of bulk metallic glasses and the application of refractory-based high entropy thin films in structural and functional applications.
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| 17. |
- Forouzan, Farnoosh, 1985-, et al.
(författare)
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Kinetics of Carbon Enrichment in Austenite during Partitioning Stage Studied via In-Situ Synchrotron XRD
- 2023
-
Ingår i: Materials. - : MDPI. - 1996-1944. ; 16:4
-
Tidskriftsartikel (refereegranskat)abstract
- The present study reveals the microstructural evolution and corresponding mechanisms occurring during different stages of quenching and partitioning (Q&P) conducted on 0.6C-1.5Si steel using in-situ High Energy X-Ray Diffraction (HEXRD) and high-resolution dilatometry methods. The results support that the symmetry of ferrite is not cubic when first formed since it is fully supersaturated with carbon at the early stages of partitioning. Moreover, by increasing partitioning temperature, the dominant carbon source for austenite enrichment changes from ongoing bainitic ferrite transformation during the partitioning stage to initial martensite formed in the quenching stage. At low partitioning temperatures, a bimodal distribution of low- and high-carbon austenite, 0.6 and 1.9 wt.% carbon, is detected. At higher temperatures, a better distribution of carbon occurs, approaching full homogenization. An initial martensite content of around 11.5 wt.% after partitioning at 280 °C via bainitic ferrite transformation results in higher carbon enrichment of austenite and increased retained austenite amount by approximately 4% in comparison with partitioning at 500 °C. In comparison with austempering heat treatment with no prior martensite, the presence of initial martensite in the Q&P microstructure accelerates the subsequent low-temperature bainitic transformation.
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| 18. |
- Javadzadeh Kalahroudi, Faezeh, et al.
(författare)
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High-Nitrogen PM Tool Steel : A Comparison Of Microstructure And Mechanical Properties Of As-HIPed And HIPed Followed By Hot Working
- 2022
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Ingår i: World PM 2022 Congress Proceedings. - : European Powder Metallurgy Association (EPMA). - 9781899072552
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Konferensbidrag (övrigt vetenskapligt/konstnärligt)abstract
- High-nitrogen-chromium alloyed powder metallurgy (PM) tool steels offer many attractive features including high strength and corrosion resistance. The PM route offers various advantages such as advanced alloy composition, high homogeneity, and well-defined size distribution of hard phase particles. This study presents microstructure and mechanical properties of a PM Cr-Mo-V-N alloy. The conventional manufacturing route for this alloy is hot isostatic pressing (HIP) followed by hot working. To investigate the possibility of near-net-shape manufacturing, a comprehensive comparison of the performance was made between steels produced by as-HIPed and HIPed followed by hot working. Both steel types were heat treated in the same way to obtain martensitic matrix with limited retained austenite. In the present investigation, microstructure and phase analyses were performed by X-ray diffraction and scanning electron microscopy. Mechanical tests were carried out by hardness measurements and tensile fatigue tests in the very high cycle fatigue regime using ultrasonic fatigue testing.
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| 19. |
- Kazantseva, N. V., et al.
(författare)
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Laser Additive 3D Printing of Titanium Alloys : Current Status, Problems, Trends
- 2021
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Ingår i: Physics of metals and metallography. - : Maik Nauka/Interperiodica. - 0031-918X .- 1555-6190. ; 122:1, s. 6-25
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Tidskriftsartikel (refereegranskat)abstract
- Features of 3D printing, including laser melting of metal powders, were considered in this work. The effect of laser operation mode on the structure, residual stresses, and properties of manufactured metals was reviewed. A method for choosing process parameters using single tracks as universal for all types of metal laser 3D printers was proposed. Structural characteristics and medical requirements for biocompatible materials were presented. The biocompatible Ti-6Al-4V alloy manufactured by selective laser melting was considered.
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| 20. |
- Neikter, Magnus, 1988-, et al.
(författare)
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Fatigue Crack Growth of Electron Beam Melted Ti-6Al-4V in High-Pressure Hydrogen
- 2020
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Ingår i: Materials. - : MDPI. - 1996-1944. ; 13:6
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Tidskriftsartikel (refereegranskat)abstract
- Titanium-based alloys are susceptible to hydrogen embrittlement (HE), a phenomenon that deteriorates fatigue properties. Ti-6Al-4V is the most widely used titanium alloy and the effect of hydrogen embrittlement on fatigue crack growth (FCG) was investigated by carrying out crack propagation tests in air and high-pressure H2 environment. The FCG test in hydrogen environment resulted in a drastic increase in crack growth rate at a certain Δ K, with crack propagation rates up to 13 times higher than those observed in air. Possible reasons for such behavior were discussed in this paper. The relationship between FCG results in high-pressure H2 environment and microstructure was investigated by comparison with already published results of cast and forged Ti-6Al-4V. Coarser microstructure was found to be more sensitive to HE. Moreover, the electron beam melting (EBM) materials experienced a crack growth acceleration in-between that of cast and wrought Ti-6Al-4V.
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| 21. |
- Pineda Huitron, Rosa Maria, et al.
(författare)
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Converging criteria to characterize crack susceptibility in a micro-alloyed steel during continuous casting
- 2020
-
Ingår i: Materials Science & Engineering. - : Elsevier. - 0921-5093 .- 1873-4936. ; 772
-
Tidskriftsartikel (refereegranskat)abstract
- The ductility drop and decrease in strength that lead to crack formation during continuous casting of steel is typically investigated by means of the hot ductility test. In this study, hot ductility tests are performed by using a thermo-mechanical Gleeble system to simulate the deformation of steels at high temperatures and low deformation rates similar to those during continuous casting. Thus, temperature was varied between 600 and 1000°C while strain rates covered a range from 0.001 to 0.1s−1. Tests are carried out to identify the temperature range at which the steel is susceptible to crack formation as well as the effect of strain rate. Characterization of fractured surfaces and phase transformation after thermo-mechanical tests are conducted in the SEM and Optical Microscope. The combination of these techniques makes possible to formulate cracking mechanisms during hot processing which show critical strain for failure at temperatures between 700 and 900°C based on the convergence of three different criteria: I) Reduction of area, II) True fracture strength-ductility and III) True total energy. This approach provides a better understanding of crack formation in steels at the high temperatures experienced during continuous casting. This information is key to productivity losses and avoid defect formation in the final cast products.
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| 22. |
- Pineda Huitron, Rosa Maria
(författare)
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Cracking during Continuous Casting of Steels : Analysis tools and procedures to identify their causes on microalloyed steel slabs
- 2020
-
Doktorsavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Transverse corner cracks are one of the most common but complex defects formed in microalloyed steels during continuous casting (CC). Such cracks are detrimental because it leads to a loss in productivity with a great impact on environment, energy and economics for several steel making companies all over the world. If cracks are detected, a supplementary process has to be applied to remove these cracks (e.g. grinding and scarfing). If cracks cannot be detected due to oxide scales covering the cracks, then they propagate during subsequent processing (e.g. hot rolling), promoting breakouts, which consequently results in material rejection and yield loss.This thesis focuses on the study of different phenomena occurring during the secondary cooling zone combining the effect of the process parameters together with the material behaviour, which assembles four scientific articles that explains and identifies some of the risks for cracking formation during CC of a HSLA steel slab. This information is key to avoid productivity losses and defect formation in the final cast product. These made possible to address research gaps and better understanding of the steel failure during CC. Additionally, this work proposes the development of strategies for reducing/preventing the formation of cracks during continuous casting of a specific HSLA alloy and caster machine.Crack susceptibility of the steel was determined through the so called hot ductility method, this made possible to identify the temperature range at which the steel is more susceptible to crack between 700-800 °C. It was found that one of the causes for failure of the steel at high temperatures is the combination of different ferrite morphologies being Widmanstätten ferrite the predominant phase, which is considered unfavourable to toughness and ductility. This temperature range was considered detrimental for cracking formation, which was demonstrated by including real temperature measurements with pyrometers and numerical modelling, that by avoiding the low ductility zone, the quality of the slabs could improve significantly. Outcomes of this work demonstrated that the control of the cooling is beneficial for the process in order to decrease the risk for crack susceptibility of the steel during processing.Oxide scale formation was considered another important factor that influences the cooling and final quality of steel slabs during CC. The formation of oxide films during cooling of the strand has industrial implications in terms of crack formation and the overall yield of the continuous casting machine since this reduces the cooling efficiency of the strand. Accurate insights in this particular work provides an understanding of oxide scale morphology, type and mechanisms leading to an accurate control of its formation during casting. Some of the findings revealed that oxidation rate and scale thickness is much higher under water vapour than in dry air. The presence of different oxides (i.e. wüstite, magnetite and hematite) change the oxidation behaviour due to micro-mechanical properties that shown higher plasticity for wüstite in comparison to magnetite and hematite. Furthermore, it was demonstrated that the oxide scale not only is influenced by temperature and environmental condition but by the surface of the substrate. These factors are considered one of the reason for uneven cooling during CC process, thus affecting the heat transfer coefficient resulting in undesired surface quality of steel slabs.
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| 23. |
- Stekovic, Svjetlana, 1967-, et al.
(författare)
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Effect of Nitriding on Microstructure and Mechanical Properties on a Ti64Alloy for Aerospace Applications
- 2022
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Ingår i: ICAS PROCEEDINGS. - Bonn.
-
Konferensbidrag (refereegranskat)abstract
- Titanium is 40% lighter than steel and is very strong in relation to its low weight, which makes it veryinteresting for lightweight applications. However, the use of titanium in certain aircraft components islimited because titanium is a relatively soft metal that quickly deteriorates when mechanically stressed.In this research, a nitriding heat treatment has been developed for Ti64 (Grade 5) alloy with the aimto improve wear properties without negative effect on fatigue and strength. The mechanical propertieswere studied through hardness and wear tests performed at room temperature in laboratory air onuntreated and treated Ti64. Different measurements techniques were used to evaluate hardness onsurface as well as polished cross-sections due to uncertainties in hardness measurements of thinfilms. The wear properties were investigated with pin-on-disc tests. The microstructures and nitridedsurfaces were also investigated by optical microscopy, scanning electron microscopy (SEM) andsurface profilometry. The analysis has shown that the nitriding process has led to the formation of anuneven compound layer and a diffusion zone beneath it. The energy dispersive X-ray spectroscopy(EDS) mapping showed a high concentration of nitrogen in the compound layer and aluminium in thediffusion zone. The microhardness measurements and nanoindentation have revealed the formationof an approximately 2.5 μm thick diffusion zone. The wear tests results showed a large difference infriction behaviour between the nitrided specimens, which has been associated with the failure of thenitrided layer and the wear rate.
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| 24. |
- Talebi, Nasrin, 1992, et al.
(författare)
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CRACK INITIATION CRITERIA FOR DEFORMED ANISOTROPIC R260 RAIL STEEL
- 2022
-
Ingår i: CM 2022 - 12th International Conference on Contact Mechanics and Wear of Rail/Wheel Systems, Conference Proceedings. ; , s. 857-864
-
Konferensbidrag (refereegranskat)abstract
- Rail material selection and maintenance planning require accurate material failure criteria. While many of these criteria consider low-cycle fatigue of virgin materials, rail failure is known to occur after severe plastic deformations. It is, therefore, relevant to consider the applicability of such criteria during large plastic deformations. In this study, we simulate previously performed high-shear tension-torsion experiments using finite strain theory to evaluate the local stresses and strains. Based on these results, failure criteria are calibrated and validated. The Jiang-Sehitoglu criterion accurately fits and predicts failure. However, the identified parameter values are different from literature values for similar materials.
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| 25. |
- Vuorinen, Esa, associate professor, 1956-, et al.
(författare)
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Mechanical and microstructural evaluation of high performance steel (S700MC) for road restraint systems
- 2020
-
Ingår i: Engineering Failure Analysis. - : Elsevier. - 1350-6307 .- 1873-1961. ; 108
-
Tidskriftsartikel (refereegranskat)abstract
- The suitability of using high performance steel (S700MC) for road restraint systems (RRS) under very high containment level was evaluated in this study. To investigate the influence of the crash on the mechanical behaviour of the steel, different test pieces were tested by tensile and hardness testing, and examined by scanning electron microscopy (SEM). The tensile test results of S700MC showed a noticeable increase in yield strength at 0.2% elongation (Rp0.2) from 744 to 935 MPa, and ultimate tensile strength (UTS) from 810 to 1017 MPa, before and after crash tests (BC and AC, respectively). S700MC showed ~9% lower elongation at fracture value in comparison with S275JR and S355JR steels. Besides, fracture toughness, was significantly higher for S700MC (133 and 148 MJ/m3 for BC and AC, respectively) compared to conventional mild steels (108–118 MJ/m3). Microstructural observations of head-part of all S700MC samples revealed equi-axed grains. The fracture surface of tensile tested samples before crash, showed elongated grains accompanied by pore formation. Among after crash samples, one test piece showed intergranular cracks while no intergranular cracks were observed for the other crashed pieces which resulted in the lower Rp0.2 (813 MPa) and UTS strength (847 MPa) and fracture toughness (125 MJ/m3). The results showed that although RRS manufactured with S700MC undergoes severe mechanical deformation, the risk of brittle fracture is very low and this is beneficial from industrial as well as social point of view.
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| 26. |
- Lang, Victoria Ashley, et al.
(författare)
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Hand Temperature Is Not Consistent With Illusory Strength During the Rubber Hand Illusion.
- 2021
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Ingår i: Annual International Conference of the IEEE Engineering in Medicine and Biology Society. IEEE Engineering in Medicine and Biology Society. Annual International Conference. - 2694-0604. ; 2021, s. 1416-1418
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Tidskriftsartikel (refereegranskat)abstract
- The rubber hand illusion is known to invoke a sense of ownership of a rubber hand when a person watches the stroking of the rubber hand in synchrony with their own hidden hand. Quantification of the sense of ownership is traditionally performed with the rubber hand illusion questionnaire, but the search for reliable physiological measurements persists. Skin temperature has been previously suggested and debated as a biomarker for ownership. We investigated hand temperature as a measure of rubber hand illusory strength via thermal imaging of the hand during the rubber hand experiment. No relationship was found between reported illusory strength and skin temperature.Clinical Relevance- Our results indicate that skin temperature is not a suitable biomarker for rubber hand illusory strength.
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| 27. |
- Singh, Sukhdeep, 1988, et al.
(författare)
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Influence of Hot Isostatic Pressing on the Hot Ductility of Cast Alloy 718 : The Effect of Niobium and Minor Elements on the Liquation Mechanism
- 2020
-
Ingår i: Metallurgical and Materials Transactions. A. - : Springer. - 1073-5623 .- 1543-1940. ; 51:12, s. 6248-6257
-
Tidskriftsartikel (refereegranskat)abstract
- The influence of two hot isostatic pressing (HIP) treatments on liquation behavior was investigated and compared with regard to the extent of heat-affected zone liquation cracking in cast Alloy 718. The extent of liquation was seen to increase after HIP treatment at 1190 °C due to solute changes caused by the homogenization of Nb, which contributed to extensive grain boundary melting. The HIP treatment at 1120 °C exhibited lower liquation with contributions from particle liquation of the Laves phase and constitutional liquation of NbC carbides. This was also reflected in a lower ductility recovery temperature, with slower recovery for the former due to the extensive liquation. Interestingly, the nil ductility temperatures were both below the predicted equilibrium solidus of the alloy, which suggests that the ductility drop is related to liquation caused by solute segregation at the grain boundaries. © 2020, The Author(s).
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| 28. |
- Holmberg, Jonas, 1976-, et al.
(författare)
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Selection of milling strategy based on surface integrity investigations of highly deformed Alloy 718 after ceramic and cemented carbide milling
- 2020
-
Ingår i: Journal of Manufacturing Processes. - : Elsevier Ltd. - 1526-6125. ; 58, s. 193-207
-
Tidskriftsartikel (refereegranskat)abstract
- High speed milling with ceramic indexable inserts is a current practice for manufacturing of gas turbine components in superalloys since it allows for high material removal rates. Ceramic milling is used for rough milling, which is followed by cemented carbide semi- and finish milling. The tool motion play an important role on the resulting surface integrity. The machining strategy of up or down milling will induce different degree of residual stresses and deformations. Increased knowledge of selecting the machining strategy with lowest impact will promote improved productivity by using ceramic milling to a greater extent based on the affected depth. The main objective in this work has been to correlate the residual stresses and deformations to promote a greater utilization of ceramic milling while still producing surfaces with acceptable properties. Prior investigations have shown that ceramic milling induce very high tensile stresses in the surface, exceeding the material's nominal yield strength. A second objective has been to explain these stress levels by thorough investigations of the deformation after milling. In this study, milling tests with new and worn ceramic and cemented carbide inserts have been performed in Alloy 718. The topography, residual stresses, deformation and hardness have been investigated for up, centre and down milling. Residual stress measurements were performed using X-ray diffraction, followed by evaluation of hardness and deformation, using hardness testing, light optical microscopy as well as electron back scattering diffraction (EBSD). These results have been used to determine an appropriate milling strategy based on lowest possible impact in respect to residual stresses and deformation. The results show a high degree of deformation after milling that differs for the up, centre and down milling. Based on these results, it is shown that up milling is preferable for new inserts but as the inserts wear out, down milling becomes more suitable since a lower degree of deformation and residual stress impact was observed. EBSD and hardness testing showed that the milling, especially ceramic milling, caused severe deformation of the surfaces resulting in grain refinement to a nano-crystalline level. This is most likely the explanation for the prevalence of the high tensile stresses without distorting or causing failure. © 2020 The Authors
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| 29. |
- Jabir Hussain, Ahmed Fardan, 1996, et al.
(författare)
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Fine-Tuning Melt Pools and Microstructures: Taming Cracks in Powder Bed Fusion—Laser Beam of a non-weldable Ni-base Superalloy
- 2024
-
Ingår i: Materialia. - : ELSEVIER SCI LTD. - 2589-1529. ; 34
-
Tidskriftsartikel (refereegranskat)abstract
- Powder Bed Fusion – Laser Beam (PBF-LB) of high γ’ strengthened Ni-base superalloys, such as CM247LC, is of great interest for high temperature applications in gas turbines. However, PBF-LB of CM247LC is challenging due to the high cracking susceptibility during PBF-LB processing (solidification cracking) and heat treatment (strain age cracking, mostly caused by residual stresses). This study focuses on understanding the impact of process parameters on microstructure, residual stresses and solidification cracking. Laser power (P), speed (v) and hatch spacing (h) were varied while the layer thickness (t) was fixed. The melt pool size and shape were found to be key factors in minimizing solidification cracking. Narrower and shallower melt pools, achieved using a low line energy density (LED = P/v ≤ 0.1 J/mm), gave low crack densities (0.7 mm/mm2). A tight hatch spacing (h = 0.03 mm) resulted in reduced lack of fusion porosity. Electron backscatter diffraction investigations revealed that parameters giving finer microstructure with 〈100〉 crystallographic texture had low crack densities provided they were processed with a low LED. Atom probe tomography elucidated early stages of spinodal decomposition in the as-built condition, where Cr and Al cluster separately. The extent of spinodal decomposition was found to be affected by the LED and the hatch spacing. Samples with low LED and small hatch spacing showed higher degrees of spinodal decomposition. X-ray diffraction residual stress investigations revealed that the residual stress is proportional to the volumetric energy density (VED = P/(v. h. t)). Although low residual stresses can be achieved by using low VED, there is a high risk of lack of fusion. Hence, other parameters such as modified scan strategy, build plate pre-heating and pulsed laser mode, must be further explored to minimize the residual stresses to reduce the strain age cracking susceptibility.
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| 30. |
- Chantziara, Katerina, 1993-
(författare)
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Very HIgh Cycle Fatigue (VHCF) behavior of high strength alloys : A literature review
- 2023
-
Rapport (övrigt vetenskapligt/konstnärligt)abstract
- Very High Cycle Fatigue (VHCF) response of metallic materials is considered of significance importance, particularly for high- demanding applications. Since it is proved that most of the engineering materials do not exhibit a conventional fatigue limit, but rather display a continuously decreasing stress-life response at longer lifetimes. Consequently, the investigation of the various mechanisms are taking place during VHCF is essential. The primary object of the present effort is to explore and summarize recent developments and current status of the VHCF phenomenon in high strength alloys.The development of the new ultrasonic machines made the fatigue testing beyond 107 life cycles possible in a very shorter time, leading to fatigue fractures at stress levels lower than the traditionally proposed “fatigue limit”. Nowadays, a classification between Low Cycle Fatigue (LCF), High Cycle Fatigue (HCF) and Very High Cycle Fatigue (VHCF) is commonly used. The main reasons for this specific grading are: i) the need for safe design of components and ii) the fact that the failure mechanisms are particular in each of the LCF, HCF and VHCF regimes.Ultrasound machines, also called piezoelectric, are resonance fatigue testing machines reducing the testing time at least 400 times compared to the conventional machines operating at frequencies up to 20 kHz.The crack initiation stage is one of the most investigated subjects when it comes to VHCF. Usually, the fatigue initiates from a defect (inclusion, pore, grain boundary triple points), while up to 99% of fatigue life is consumed in that stage. Different models have been proposed in the literature regarding the evolution of events that contribute to the fatigue crack initiation and growth. Proposed models are such as the ODA, the polygonization, continuous grain refinement with local plasticity, the matrix fragmentation and the NCP numerous cyclic pressing. Several studies have assessed the different models and further enriched the knowledge in the VHCF field.In the present literature review effort, the main VHCF mechanisms of crack initiation and growth as well as the proposed models are presented and analyzed. Moreover, the VHCF response and the recent experimental results referring to the most used engineering alloys, e.g. steels, Ti, Ni, Al and Mg alloys, are described, with a main attention to steels. The different testing parameters and the way they affect the VHCF response are also presented.Finally, the literature review is concluded by presenting the new challenges and directions for future work in the field, especially under the light of the new low-carbon society.
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| 31. |
- Mishra, Pragya, 1989-, et al.
(författare)
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Microstructural Characterization and Mechanical Properties of L-PBF Processed 316 L at Cryogenic Temperature
- 2021
-
Ingår i: Materials. - : MDPI. - 1996-1944. ; 14:19
-
Tidskriftsartikel (refereegranskat)abstract
- Laser powder bed fusion (L-PBF) has attracted great interest in the aerospace and medical sectors because it can produce complex and lightweight parts with high accuracy. Austenitic stainless steel alloy 316 L is widely used in many applications due to its good mechanical properties and high corrosion resistance over a wide temperature range. In this study, L-PBF-processed 316 L was investigated for its suitability in aerospace applications at cryogenic service temperatures and the behavior at cryogenic temperature was compared with room temperature to understand the properties and microstructural changes within this temperature range. Tensile tests were performed at room temperature and at −196 °C to study the mechanical performance and phase changes. The microstructure and fracture surfaces were characterized using scanning electron microscopy, and the phases were analyzed by X-ray diffraction. The results showed a significant increase in the strength of 316 L at −196 °C, while its ductility remained at an acceptable level. The results indicated the formation of ε and α martensite during cryogenic testing, which explained the increase in strength. Nanoindentation revealed different hardness values, indicating the different mechanical properties of austenite (γ), strained austenite, body-centered cubic martensite (α), and hexagonal close-packed martensite (ε) formed during the tensile tests due to mechanical deformation.
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| 32. |
- Moretti, Marie Anna, 1995-
(författare)
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Microstructure and property models of alloy 718 applicable for simulation of manufacturing processes
- 2022
-
Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- This thesis focuses on experimental characterization, understanding and modelling of nickel-based alloy 718, for a large range of loading conditions. Alloy 718 is the most widely used nickel-based superalloy, due to its high strength, high corrosion resistance and excellent mechanical properties at high temperatures. In this work, the mechanical behavior and microstructure evolution of this alloy during high strain rate deformation is investigated. Compression tests using a Split-Hopkinson pressure bar (SHPB) device were performed and the microstructure of the deformed sample was observed using optical microscope (OM) and scanning-electron microscope (SEM) coupled with electron back-scattered diffraction (EBSD) technique. The microstructural evolution according to the deformation conditions was characterized. For high deformation temperatures (1000 C and above), recrystallisation is identifed as the main deformation mechanism. A physics-based model was employed to simulate the deformation behavior of alloy 718. This type of models accounts for the microstructural mechanisms taking place during deformation. Knowledge about the deformation mechanisms of alloy 718, acquired experimentally and from literature, enables to formulate mathematically the microstructural phenomena governing the deformation behavior of the alloy. The proposed model includes the effects of strain hardening, grain boundary strengthening (Hall-Petch), solid solution strengthening, phonon and electron drag and recovery by dislocation glide and cross-slip. It is calibrated and validated using data obtained from mechanical tests, as well as values captured by the microstructural analysis.
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| 33. |
- Sadek, Mohamed, 1986-, et al.
(författare)
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Fatigue Strength and Fracture Mechanisms in the Very-High-Cycle-Fatigue Regime of Automotive Steels
- 2020
-
Ingår i: Steel Research International. - : WILEY-V C H VERLAG GMBH. - 1611-3683 .- 1869-344X. ; 91:8
-
Tidskriftsartikel (refereegranskat)abstract
- Very-high-cycle-fatigue (VHCF) strength properties are of interest to several technical applications assessed globally at different laboratories with long-life fatigue testing capabilities. Also, VHCF failure mechanisms are a scientific topic with remaining open research questions. Herein, three automotive bar grade steels are studied with respect to VHCF strength and initiation mechanisms. A microalloyed ferritic-pearlitic steel (38MnSiV5, 870 MPa tensile strength), a quenched and tempered martensitic steel (50CrV4, 1410 MPa tensile strength), and a carburizing steel (16MnCr5, 1180 MPa core structure tensile strength) are studied to reveal characteristics regarding initiation and VHCF failure mechanisms. A 20 kHz ultrasonic fatigue testing instrument is used to obtain fatigue lives up to and above 10(9) load cycles in uniaxial loading. Hour-glass specimens, smooth or notched, are tested at R = -1 and R = 0.1. Fatigue strength and stress life (SN)-diagram data are achieved, and crack initiation and growth mechanisms are studied using primarily field-emission gun-scanning electron microscopy (FEG-SEM). Fatigue strengths are explained by a modified life-dependent Murakami-expression, the Haigh diagram, and notch sensitivity. Interior and surface crack initiations by surface defects, triple points, and inclusions are found. The fine granular area (FGA) to fish-eye crack growth transition conditions are explored and schematic descriptions are given.
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| 34. |
- Xu, C L, et al.
(författare)
-
Impact of local Si segregation on strain localization in ductile cast iron
- 2020
-
Ingår i: IOP Conference Series: Materials Science and Engineering. - : Institute of Physics Publishing (IOPP).
-
Konferensbidrag (refereegranskat)abstract
- The distribution of Si content in tensile deformed ductile cast iron has been characterized using electron microscopy and correlated to the strain distribution determined based on 3D tomography data collected before and after tensile deformation and digital volume correlation analysis. The results show that the high plastic strain regions localize in bands consisting of large graphite nodules and deformed matrix with high Si content connecting the graphite nodules in the first-to-solidify regions. The bands are aligned about 45° with respect to the loading direction, which is close to the maximum shear direction.
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| 35. |
- Ramesh Sagar, Vaishak, 1988, et al.
(författare)
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Investigating the sensitivity of particle size distribution on part geometry in additive manufacturing
- 2020
-
Ingår i: ASME International Mechanical Engineering Congress and Exposition, Proceedings (IMECE). ; 2B-2020
-
Konferensbidrag (refereegranskat)abstract
- Selective laser melting process is a powder bed fusion additive manufacturing process that finds applications in aerospace and medical industries for its ability to produce complex geometry parts. As the raw material used is in powder form, particle size distribution (PSD) is a significant characteristic that influences the build quality in turn affecting the functionality and aesthetics aspects of the end product. This paper investigates the effect of PSD on deformation for 316L stainless steel powder, where three coupled in-house simulation tools based on Discrete Element Method (DEM), Computational Fluid Dynamics (CFD), and Structural Mechanics are employed. DEM is used for simulating the powder distribution based on the different particle size distribution of the powder. The CFD is used as a virtual test bed to determine thermal parameters such as density, heat capacity and thermal conductivity of the powder bed viewed as a continuum. The values found as a stochastic function of the powder distribution is used to test the sensitivity of the melted zone and distortion using Structural Mechanics. Results showed significant influence of particle size distribution on the packing density, surface height, surface roughness, the stress state and displacement of the melted zone. The results will serve as a catalyst in developing geometry assurance strategies to minimize the effect of particle size distribution on the geometric quality of the printed part.
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| 36. |
- Liu, Yuqi, et al.
(författare)
-
Liquid Digital Twins Based on Magnetic Fluid Toys
- 2022
-
Ingår i: 2022 IEEE Conference on Virtual Reality and 3D User Interfaces Abstracts and Workshops (VRW). - : IEEE. - 9781665484022 ; , s. 988-989
-
Konferensbidrag (refereegranskat)abstract
- As a new type of functional material, magnetic fluid has both the fluidity of liquid and the magnetic properties of solid magnetic material. By controlling the magnets, one can simulate the effect of manipulating liquids like a sea emperor. This will provide new ideas for the multiverse of the metaverse. Not only that, magnetic fluids also have very important applications in astrophysics, controlled thermonuclear reactions and even the medical industry. Therefore, this paper hopes to provide a control idea for the future application of magnetic fluid by performing Digital Twins simulation of magnetic fluid.
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| 37. |
- Edin, Emil
(författare)
-
Effect of Stress Relief Annealing: Part Distortion, Mechanical Properties, and Microstructure of Additively Manufactured Austenitic Stainless Steel
- 2022
-
Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Additive manufacturing (AM) processes may introduce large residual stresses in the as-built part, in particular the laser powder bed fusion process (L-PBF). The residual stress state is an inherent consequence of the heterogeneous heating and subsequent cooling during the process. L-PBF has become renowned for its “free complexity” and rapid prototyping capabilities. However, it is vital to ensure shape stability after the component is removed from the build plate, which can be problematic due to the residual stress inducing nature of this manufacturing process. Residual stresses can be analyzed via many different characterization routes (e.g. X-ray and neutron diffraction, hole drilling, etc.), both quantitatively and qualitatively. From an industrial perspective, most of these techniques are either prohibitively expensive, complex or too slow to be implementable during the early prototyping stages of AM manufacturing.In this work a deformation based method employing a specific geometry, a so called “keyhole”-geometry, has been investigated to qualitatively evaluate the effect of different stress relief annealing routes with respect to macroscopic part deformation, mechanical properties and microstructure. Previous published work has focused on structures with open geometry, commonly referred to as bridge-like structures where the deformation required for analysis occurs during removal from the build plate. The proposed keyhole-geometry can be removed from the build plate without releasing the residual stresses required for subsequent measurement, which enables bulk manufacturing on single build plates, prior to removal and stress relief annealing. Two L-PBF manufactured austenitic stainless steel alloys were studied, 316L and 21-6-9. Tensile specimen blanks were manufactured and the subsequent heat treatments were carried out in pairs of keyhole and tensile blank. Both a contact (micrometer measurement), and a non-contact (optical profilometry) method were employed to measure the residual stress induced deformation in the keyholes. The annealing heat treatment matrix was iteratively expanded with input from the deformation analysis to find the lowest temperature at which approximately zero deformation remained after opening the structure via wire electrical discharge machining. The lowest allowable annealing temperature was sought after to minimize strength loss. After stress relief annealing at 900 ℃ for 1 hour, the 316L keyhole-geometry was considered shape stable. The lateral micrometer measurement yielded a length change of 1 µm, and a radius of 140 m (over the 22 mm top surface) was assigned from curve fitting the top surface height profiles. The complementary microstructural characterization revealed that this temperature corresponded to where the last remains of the cellular sub-grain structures disappears. Tensile testing showed that the specimen subjected to the 900 ℃ heat treatment had a marked reduction in yield stress (YS) compared to that of the as-built: 540 MPa → 402 MPa, whereas ultimate tensile strength (UTS) only reduced slightly: 595 MPa → 570 MPa. The ductility (4D elongation) was found to be ~13 % higher for the specimen heat treated at 900 ℃ than that of the as-built specimen, 76% and 67% respectively. For alloy 21-6-9 the residual stress induced deformation minimum (zero measurable deformation) was found after stress relief heat treatment at 850 ℃ for 1 hour. Slight changes in the microstructure were observable through light optical microscopy when comparing the different heat treatment temperatures. The characteristic sub-grain features associated with alloy 316L were not verified for alloy 21-6-9. Similar to the results for 316L, UTS was slightly lower for the tensile specimen subjected to the heat treatment temperature required for shape stability (850 ℃) compared to the as-built specimen: 810 MPa → 775 MPa. The measured ductility (4D elongation) was found to be approximately equal for the as-built (47%), and heat treated (48%) specimen. As-built material exhibited a YS of 640 MPa while the heat treated specimen had a YS of 540 MPa. For alloy 21-6-9, the lateral micrometer deformation measurements were compared with stress relaxation testing performed at 600 ℃, 700℃ and 800 ℃. Stress relaxation results were in good agreement with the results from the lateral deformation measurements. The study showed that for both steel alloys, the keyhole method could be successfully employed to rapidly find a suitable stress relief heat treatment route when shape stability is vital.
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| 38. |
- Edin, Emil, et al.
(författare)
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Stress relief heat treatment and mechanical properties of laser powder bed fusion built 21-6-9 stainless steel
- 2023
-
Ingår i: Materials Science and Engineering A. - : Elsevier. - 0921-5093 .- 1873-4936. ; 868
-
Tidskriftsartikel (refereegranskat)abstract
- In this work, the effectiveness of residual stress relief annealing on a laser powder bed fusion (L-PBF) manufactured austenitic stainless steel, alloy 21-6-9 was investigated. Residual stress levels were gauged using geometrical distortion and relaxation testing results. In the investigated temperature interval (600–850 °C), shape stability was reached after subjecting the as-built material to an annealing temperature of 850 °C for 1 h. Microstructural characterization and tensile testing were also performed for each annealing temperature to evaluate the alloy's thermal stability and the resulting tensile properties. In the as-built state, a yield strength (YS) of 640 MPa, ultimate tensile strength (UTS) of 810 MPa and 4D elongation of 47% were measured. Annealing at 850 °C for 1 h had little measurable effect on ductility (48% 4D elongation) while still having a softening effect (UTS = 775 MPa, YS = 540 MPa). From the microstructural characterization, cell-like features were observed sporadically in the annealed condition and appeared stable up until 800 °C after which gradual dissolution began, with the last remnants disappearing after subjecting the material to 900 °C for 1 h.
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| 39. |
- Gruber, Paul H., et al.
(författare)
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WC-Ni cemented carbides prepared from Ni nano-dot coated powders
- 2023
-
Ingår i: International journal of refractory metals & hard materials. - : Elsevier Ltd. - 0263-4368. ; 117
-
Tidskriftsartikel (refereegranskat)abstract
- This study presents a novel approach for the synthesis of WC-Ni cemented carbides with enhanced mechanical properties. A low-cost solution-based route was used to coat WC powders with well-distributed metallic nickel dots measuring between 17 nm and 39 nm in diameter. Varying compositions with loadings of 2, 6, and 14 vol% Ni were consolidated using spark plasma sintering (SPS) at 1350 °C under 50 MPa of uniaxial pressure giving relative densities of 99 ± 1 %. The sintered WC-Ni cemented carbides had an even distribution of the Ni binder phase in all compositions, with retained ultrafine WC grain sizes of 0.5 ± 0.1 μm from the starting powder. The enhanced sinterability of the coated powders allowed for consolidation to near theoretical densities, with a binder content as low as 2 vol%. This is attributed to the uniform distribution of nickel and an extensive Ni-WC interface existing prior to sintering. The small size of the Ni dots likely also contributed to the solid-state sintering starting temperatures of as low as 800 °C. The mechanical performance of the resulting cemented carbides was evaluated by measuring the hardness at temperatures between 20 °C and 700 °C and estimating toughness at room temperature using Vickers indentations. These results showed that the mechanical properties of the WC-Ni cemented carbides synthesised by our method were comparable to conventionally prepared WC-Co cemented carbides with similar grain sizes and binder contents and superior to conventionally prepared WC-Ni cemented carbides. In particular, the 2 vol% Ni composition had excellent hardness at room temperature of up to 2210HV10, while still having an indentation fracture toughness of 7 MPa·m0.5. Therefore, WC-Ni cemented carbides processed by this novel approach are a promising alternative to conventional WC-Co cemented carbides for a wide range of applications.
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| 40. |
- Harr Martinsen, Kristoffer, 1990
(författare)
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Preparation and characterization of graphene/metal composites
- 2021
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Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Since the isolation of graphene in 2004, much research has been conducted to understand this novel material and how its properties can be utilized in different applications. One type of venture involves graphene as a reinforcing filler in metal matrix composites (MMC) which is becoming increasingly prevalent in the automotive and aerospace industries. Such composites combine the machinability and processing flexibility of metals with the unique properties of graphene. In fact, copper-graphene composites have demonstrated ameliorated mechanical strength with thermal conductivities elevated beyond pristine copper. However, the challenges that remain to commercialize copper-graphene composites are numerous. The most challengeable one is that graphene must be uniformly dispersed in the matrix and adhere to copper through an industrially scalable and affordable process. Moreover, the volume fraction of graphene must be efficiently controlled, lest superfluous amounts lead to structural detriment. In this regard, the emphasis of this study was to investigate a scalable and simple method to obtain such MMC via powder metallurgy. Specifically, gas atomized copper powder was functionalized with 3-aminopropyl-triethoxysilane (APTES) in toluene (APTES-Cu), resulting in a positively charged surface; then aqueously dispersed and negatively charged graphene oxide (GO) could then be self-assembled on the surface APTES@Cu via electrostatic interaction (Cu@APTES-Cu). The thickness of GO layers and morphology on the powder was controlled by modulating APTES grafting duration and APTES concentration in toluene. Cu@APTES-Cu powders were thermally annealed before compaction and sintering in inert atmosphere. The results show that surface modification of metal powders serves as a scalable and versatile approach to coat graphene on metal particles for the preparation of graphene/metal composites. Surface modification of copper with 0.2 vol% APTES in toluene for 30 minutes was sufficient to obtain composite powders with incomplete GO coating, which nonetheless demonstrated improved hardness. However, cold working of sintered composites was essential to densify the porous structure created by reduced GO during sintering. On the other hand, sintered composite samples that exhibited higher thermal conductivity than copper was obtained with higher APTES and GO loading. After thermal annealing, these thicker GO coatings were found to improve thermal conductivity in sintered composites by acting as thermal bridges between individual composite particles. Despite incomplete sintering of these composites, a 20% increase in thermal conductivity was attainable. Finally, both polarization scans and etching measurements in concentrated HCl and ammonium persulfate (APS) indicate that the GO coating decomposes on the outer surface during sintering. However, the reduced GO coating can retard corrosion of the internal composite structure by diffusion inhibition.
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| 41. |
- Hemati, N., et al.
(författare)
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Effect of Rare Earth Elements on the Microstructural and Mechanical Properties of ZK60 Alloy after T5 Treatment
- 2022
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Ingår i: Russian Journal of Non-Ferrous Metals = Izvestiya VUZ. Tsvetnaya Metallurgiya. - : Springer Nature. - 1067-8212 .- 1934-970X. ; 63:2, s. 223-236
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Tidskriftsartikel (refereegranskat)abstract
- In this study, the microstructure and mechanical properties of ZK60 extruded alloy were investigated after adding 3 wt % of Ce and Y and T5 operation. The microstructure of the base alloy consists of alpha-Mg and Mg7Zn3. In addition to these phases, MgZn2Ce and Mg3Y2Zn3 phases are formed by adding Ce and Y, respectively. The addition of rare earth elements reduces the grain size of the base alloy from 6.1 mu m to less than 3 mu m. The volume fraction of precipitates also increases because of the additions. After T5 operation for different times, it was observed that the hardness peak (88 HV) for the base alloy is achieved after 18 hours. However, the peak hardness of alloys containing rare earth elements occurred in 24 hours. Increasing the aging time results in an increase in the grain size of the base alloy, while it led to a slight increase in the grain size of alloys containing rare earth elements. The higher hardness at the peak age of all studied alloys is explained based on the increase in the volume fraction of precipitates during this operation. The delay in the peak age in alloys containing rare earth elements is due to the delay in the formation of beta(2’) precipitates. The shear punch test results of extruded alloys show that in alloys containing Ce and Y the shear strength is 156 and 160 MPa, respectively. While this value is about 148 MPa for the base alloy. At the peak age, this strength for ZK60-Ce and ZK60-Y alloys increases by 11% and 13%, respectively. Higher strength and hardness in Y-containing alloys are due to the simultaneous strengthening of solid solution and precipitates along with the formation of precipitates with high thermal stability.
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| 42. |
- Hentschel, Oliver, et al.
(författare)
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Experimental Investigations in the Processing of AISI H11 Powder Blends Enriched with Tungsten Carbide Nanoparticles for the Additive Manufacturing of Tailored Hot Working Tools in the Directed Energy Deposition (DED-LB/M)—Impact of Tungsten Carbide Nanoparticles on Microstructural and Mechanical Characteristics
- 2024
-
Ingår i: Metals. - : MDPI. - 2075-4701. ; 14:2, s. 188-188
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Tidskriftsartikel (refereegranskat)abstract
- In this study, the DED-LB/M process of AISI H11 tool steel powder blends modified by adding WC nanoparticles (WC-np) in concentrations of 1, 2.5 and 5 wt.-% was the object of scientific investigations. For this, 30-layer cuboid specimens were manufactured. The overall scientific aim was to examine how the WC-np interact with the steel melt and in the end, influence the processability, microstructure and mechanical properties of produced specimens. The examinations were carried out on both as-built and thermally post-processed specimens. An advanced microstructural analysis (SEM, EDS, EBSD and XRD) revealed that due to the high solubility of WC-np in the molten steel, most of the WC-np appear to have dissolved during the ongoing laser process. Furthermore, the WC-np favor a stronger distortion and finer grain size of martensite in the manufactured specimens. An increase in hardness from about 650 HV1 for the H11 specimen to 780 HV1 for the one manufactured using the powder blend containing 5 wt.-% of WC-np was observed in as-built conditions. In the same way, the compression yield strength enhanced from 1839 MPA to 2188 MPA. The hardness and strength increasing effect of WC-np remained unchanged even after heat treatments similar to those used in industry.
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| 43. |
- Hoier, Philipp, 1988, et al.
(författare)
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Influence of batch-to-batch material variations on grindability of a medium‑carbon steel
- 2022
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Ingår i: Journal of Manufacturing Processes. - : Elsevier Ltd. - 1526-6125. ; 73, s. 463-470
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Tidskriftsartikel (refereegranskat)abstract
- This study addresses the influence of material variations on the grindability of crankshaft steel. Most previous studies on the effect of material microstructure on grindability involve comparisons of significantly different steel grades. This study, in contrast, is focused on batch-to-batch grindability variations for one steel grade, a scenario frequently occurring in industry where batches from different steel makers are fed into a production line. For this purpose, a batch made of recycled steel and a batch made of ore-based steel were compared with regards to microstructure and grindability under identical grinding and dressing conditions. Although both batches met the same material specifications, microstructural variations were identified in terms of grain size and micro-constituents (inclusions, carbonitrides). While specific grinding energy, residual stress and full-width at half-maximum profiles of ground surfaces were the same for both batches, the recycled batch showed different and unfavorable variation in wheel wear and Barkhausen noise (BN) response. Larger fractions of oxide inclusions and larger grain sizes (affected by carbonitrides) were present in the recycled batch, which were the likely reasons for the differences in wheel wear and BN response, respectively. These findings may aid grindability improvement by steel-grade adjustments, e.g. modification of the distribution and type of inclusions and/or amount of elements forming carbonitrides. Furthermore, the results highlight the importance of understanding and controlling material microstructure, as existing in-line quality by BN control may not always be able to correctly indicate surface integrity, which could lead to misinterpretations (e.g. false part-rejection on the assumption of grinding burn). © 2021 The Authors
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| 44. |
- Javadzadeh Kalahroudi, Faezeh
(författare)
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Microstructure and Fatigue Analysis of PM-HIPed Alloys : A Focus on Inconel 625 and High-Nitrogen Tool Steel
- 2024
-
Licentiatavhandling (övrigt vetenskapligt/konstnärligt)abstract
- Nickel-based superalloys and tool steels are well-known high-performance alloys due to their extensive use in many different industries. Nickel-based superalloys have found their way into aircraft, aerospace, marine, chemical, and petrochemical industries owing to their excellent high-temperature corrosion and oxidation resistance. On the other hand, tool steels could provide a combination of outstanding corrosion and wear resistance. They can play an important role in cutting and wear applications and manufacturing plastic extrusion and food processing components.Near-net shape manufacturing using powder metallurgy (PM) and hot isostatic pressing (HIP) can serve as an efficient manufacturing process to produce these alloys. This technology can successfully tackle conventional manufacturing challenges of highly alloyed materials i.e. segregation during the casting process or cracks during hot working processes of Ni-based superalloys, and carbide segregation and formation of large and irregularly shaped carbides in wrought and hot rolled tool steels. However, the presence of precipitates on prior particle boundaries (PPBs) in Ni-based superalloys, and metallurgical defects like non-metallic inclusions in both Ni-based superalloys and tool steels may affect the fatigue performance of these PM-HIPed products.This licentiate thesis aims to investigate the microstructure and fatigue behavior of two PM-HIPed alloys i.e. Inconel 625 and high-nitrogen tool steel. The results confirm precipitation along PPBs in PM-HIPed Inconel 625; however, no effect was detected in the fractography studies of the high cycle fatigue samples, and tensile properties were comparable with wrought materials reported in the literature. On the other hand, the microstructure of PM-HIPed high-nitrogen tool steel displayed dispersed precipitates and no traces of PPBs. Moreover, in both cases, i.e. very high cycle fatigue of PM-HIPed high-nitrogen tool steel and high cycle fatigue of PM-HIPed Inconel 625, fatigue crack initiation was attributed to the presence of non-metallic inclusions, either individually or agglomerated with precipitates. This underscores the significance of the manufacturing process in fatigue performance.
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| 45. |
- Krakhmalev, Pavel, 1973-, et al.
(författare)
-
Microstructure of L-PBF alloys : Chapter 8.
- 2021
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Ingår i: Fundamentals of Laser Powder Bed Fusion of Metals. - : Elsevier. - 9780128240908 ; , s. 215-243
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Bokkapitel (refereegranskat)abstract
- Laser powder bed fusion (L-PBF) of metallic alloys results in the formation of solid metallic material with microstructure different from the conventional analogs. The differences are the result of high temperature of the molten pool, high cooling rates, steep temperature gradient, thermal cycling during manufacturing, and other factors. Since the microstructure affects the physical and mechanical properties of materials and influences the performance of L-PBF parts, microstructural analysis is critical. Understanding of the formation of microstructure, therefore, is necessary to predict the final properties of the material, and it creates a strong basis for the microstructure control and manufacturing of components with tailored properties. This chapter outlines the main principles of the formation of microstructure in the L-PBF process and presents some examples of microstructures of the most common L-PBF alloys.
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| 46. |
- Krakhmalev, Pavel, 1973-, et al.
(författare)
-
Structural integrity I: static mechanical properties : Chapter 13
- 2021
-
Ingår i: Fundamentals of Laser Powder Bed Fusion of Metals. - : Elsevier. - 9780128240908 ; , s. 349-376
-
Bokkapitel (refereegranskat)abstract
- Laser powder bed fusion (L-PBF) is one of the additive manufacturing methods to produce metallic parts. The layer-by-layer manufacturing nature results in the formation of specific microstructure, achieving different properties compared to conventional analogs. In this chapter, the mechanical properties of the main classes of materials such as steels, aluminum and titanium alloys, as well as nickel-base superalloys manufactured by L-PBF are overviewed. The focus is on the static mechanical properties obtained by tensile tests as the most common standard method for the measurement of mechanical characteristics. A correlation between manufacturing, microstructure, and mechanical properties of these L-PBF materials is highlighted.
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| 47. |
- Kuzminova, Yulia O., et al.
(författare)
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Structural and mechanical properties of the additive manufactured CrFeCoNi(Al,Ti) high-entropy alloys produced using powder blends
- 2023
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Ingår i: Materialia. - : Elsevier. - 2589-1529. ; 32
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Tidskriftsartikel (refereegranskat)abstract
- High-entropy Alloys (HEAs) are considered prospective materials demonstrating the new approach of alloy design creating new compositions for harsh conditions. However, searching for alloy chemical composition providing the best material properties is a costly process. Additive manufacturing (AM) can be an effective technique for adjusting the alloy composition by using several initial materials. The powder bed fusion (PBF) AM process allows the printing of solid parts using powder blends. In the present study, the CrFeCoNi(Al,Ti) HEAs were printed by the PBF technique using the blends of three powders. The structural and phase investigations revealed the chemical inhomogeneity in the materials that led to the new phase formations affecting the mechanical characteristics. The high-temperature annealing at 1200 °C can be considered a post-treatment process for the printed alloys as a homogenization process while the annealing at a lower temperature of 800 °C initiates the decomposition of the initially formed f.c.c. phase.
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| 48. |
- Maurya, Himanshu Singh, et al.
(författare)
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Synergistic effect of Nb and Mo on the microstructural formationof the Ti(C,n)-high chromium ferrous-based cermets
- 2024
-
Ingår i: International journal of refractory metals & hard materials. - : Elsevier. - 0263-4368. ; 122
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Tidskriftsartikel (refereegranskat)abstract
- In this study, Ti(C,N)-Fe-based green cermets with different metallic alloying elements have been consolidated by pressureless liquid-phase sintering. The addition of different metallic binders on Ti(C,N)-based cermet such as Nb and Mo on high chromium Ferrous based binder has been investigated. Detailed analysis of the phase constitution was conducted using thermodynamic calculations and experiments, as well as a systematic study of the microstructure evolution and room temperature mechanical properties including hardness and fracture toughness was conducted. The Nb and Mo addition to the binder system affects the sintering temperatures and can significantly affect the phase formation and microstructural development. Scanning electron microscope (SEM) and Energy dispersive spectroscopy (EDS) technique were used to examine the microstructure, composition, and fracture surface of cermets. The addition of the Mo, and Nb reveals lower porosity and finer microstructure as compared to the reference material (Ti(C,N)-Fe-Cr). The refinement of microstructure improves mechanical properties such as hardness and fracture toughness of Ti(C,N)-Fe-Cr-Mo-Nb-based cermets. Further, the addition of these binder elements may reduce the formation of Fe-Cr-based intermetallic complex carbides, allowing cermets to perform better in terms of toughness and corrosion resistance. As a result of the experiments, it is evident that Nb and Mo dissolve in Ti(C,N) and form solid solutions during sintering. The increased number of coreless grains, spinodal decomposition, and crack deflection in cermet further enhance the fracture toughness.
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| 49. |
- Mishra, Pragya, 1989-, et al.
(författare)
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Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications
- 2023
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Ingår i: Journal of Materials Research and Technology. - : Elsevier. - 2238-7854. ; 25, s. 1483-1494
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Tidskriftsartikel (refereegranskat)abstract
- The alloy 21-6-9 is a nitrogen-strengthened austenitic stainless steel often used in aerospace applications due to its high strength, good fabrication properties, and toughness at cryogenic temperatures. However, minimal research has been conducted on alloy 21-6-9 using the additive manufacturing process laser powder-bed fusion (L-PBF). The L-PBF technique has been seen as a key to reducing production time and avoiding costly machining. Therefore, there is an interest in investigating L-PBF-processed 21-6-9 to determine the effects of L-PBF on properties at elevated and cryogenic temperatures. In this study, prior to tensile testing the alloy 21-6-9 underwent heat treatments that simulated aerospace applications and the alloy was analyzed and characterized to evaluate phase stability. The effects of elevated and cryogenic temperatures (77K) on the tensile behavior and microstructure were investigated using X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). The tensile tests showed that the yield strength and ultimate tensile strength improved, while ductility varied depending on the conditions and test environment. The ultimate tensile strength was approximately 80% higher at 77K than at room temperature, although the elongation decreased by around 90%, possibly due to the formation of strain-induced martensite.
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| 50. |
- Mussa, Abdulbaset, et al.
(författare)
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Development of a new PM tool steel for optimization of cold working of advanced high-strength steels
- 2020
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Ingår i: Metals. - : MDPI AG. - 2075-4701. ; 10:10
-
Tidskriftsartikel (refereegranskat)abstract
- In the present study, Uddeholm Vancron SuperClean cold work tool steel was investigated concerning wear resistance and fatigue strength, using laboratory and semi-industrial tests. The Uddeholm Vancron SuperClean was designed with the help of ThermoCalc calculations to contain a high amount of a carbonitride phase, which was suggested to improve tribological performance of this tool steel. In order to investigate the tested steel, galling tests with a slider-on flat-surface tribotester and semi-industrial punching tests were performed on an advanced high-strength steel, CP1180HD. Uddeholm Vanadis 8 SuperClean containing only a carbide phase and Uddeholm Vancron 40 containing a mixture of carbides and carbonitrides were also tested to compare the performance of the tool steels. The microstructure and wear mechanisms were characterized with scanning electron microscopy. It was found that the carbonitrides presented in Uddeholm Vancron SuperClean improved its resistance to material transfer and galling. Semi-industrial punching tests also confirmed that Uddeholm Vancron SuperClean cold work tool steel also possesses enhanced resistance to chipping and fatigue crack nucleation, which confirms the beneficial role of the carbonitride phase in wear resistance of cold work tool steel.
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