An ultra-wideband system for measuring the dielectric properties of mineral compounds in a heat-reaction chamber at high temperatures

A measurement system for the measurement of microwave dielectric properties of mineral compounds at temperatures up to +1000°C is presented. It includes the simultaneous measurement of mass and temperature. Samples volumes in the range 0.01 to 0.1 m 3 can be studied. The system comprises a heat reaction chamber on a mass scale with mounted ultra-wideband (UWB) radio sensors and temperature probes. The complex refractive index is determined from the UWB signals using a technique with windowing to suppress interference and fitting of a modelled signal to the experimental ones. The developed method is validated by measuring the complex refractive index of water from +82°C down to +23°C and comparing with literature values. The systems is used to study calcination of limestone, i.e. the chemical decomposition of CaCO 3 to CaO and CO 2 when heated up to +1000°C. The chemical decomposition is clearly seen as a decrease in mass and as significant changes in the complex refractive index. The system could be used also for other mineral compounds and other types of materials.

TEKNIK OCH TEKNOLOGIER Elektroteknik och elektronik hsv//swe
ENGINEERING AND TECHNOLOGY Electrical Engineering, Electronic Engineering, Information Engineering hsv//eng
calcination; dielectric permittivity; heat-chamber; High-temperature techniques; radio measurement; thermogravimetry; ultra-wideband; UWB

Ingår i:IEEE Transactions on Instrumentation and Measurement: IEEE720018-94561557-9662

Av författaren/redakt...: Ottosson, Patrik; Andersson, Danie ...; Choudhary, Vipin; Rönnow, Daniel

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