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Synthesis, crystal structure and NLO properties of a novel ruthenium(II) complex with unusual coordination mode

Tian, Yu-peng (author)
Department of Chemistry, Anhui University, China
Zhang, Ming-liang (author)
Department of Chemistry, Anhui University, China
Hu, Zhang-Jun (author)
Department of Chemistry, Anhui University, China
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Hu, Han-mei (author)
Department of Chemistry, Anhui University, China
Wu, Jie-Ying (author)
Department of Chemistry, Anhui University, China
Zhang, Xuanjun (author)
Department of Chemistry, Anhui University, China
Zhang, Sheng-YI (author)
Department of Chemistry, Anhui University, China
Tao, Xutang (author)
State Key Laboratory of Crystal Materials, Shandong University, China
Jiang, Minhua (author)
State Key Laboratory of Crystal Materials, Shandong University, China
Chen, He-ping (author)
Department of Physics, Anhui University, China
Chantrapromma, Suchada (author)
Crystallography Unit, School of Physics, Universiti Sain Malaysia
Fun, Hoong-Kun (author)
Crystallography Unit, School of Physics, Universiti Sain Malaysia
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 (creator_code:org_t)
2014-01-07
2005
English.
In: Transition metal chemistry (Weinheim). - : Kluwer Academic Publishers. - 0340-4285 .- 1572-901X. ; 30:7, s. 778-785
Related links:
https://urn.kb.se/re...
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https://doi.org/10.1...
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  • Journal article (peer-reviewed)
Abstract Subject headings
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  • A new Schiff base 4-[N-hydroxyethyl-N-(methyl)amino]benzaldehyde S-methyl dithiocarbazate (HL, where H is a dissociable proton) and the ruthenium complex [Ru(bpy)2L]PF6 (bpy = 2,2′-bipyridine) have been synthesized. The structural determinations of the ligand and its ruthenium complex, by X-ray crystallography, show that the ligand is coordinated as a monoanionic bidentate N, S-donor, forming a four-member chelate ring with a bite angle of 65.91°. The complex shows intense MLCT transitions in the visible region. Fluorescent and electrochemical properties have been also studied. The complex in DMF solution exhibited a strong two-photon absorption (t.p.a.) at 532 nm nanosecond laser pulses. The t.p.a. coefficient β, t.p.a. cross-section σ and the third-order optical nonlinearity χ(3) of the complex and the ligand have been determined by the Z-scan technique.

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