id:"swepub:oai:DiVA.org:ltu-12752"
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- Engström, V.Luleå tekniska universitet (author)
The effect of seed size on the growth of silicalite-1 films on gold surfaces
- Article/chapterEnglish2000
Publisher, publication year, extent ...
- 2000
- printrdacarrier
Numbers
- LIBRIS-ID:oai:DiVA.org:ltu-12752
- https://urn.kb.se/resolve?urn=urn:nbn:se:ltu:diva-12752URI
- https://doi.org/10.1016/S1387-1811(99)00299-1DOI
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- Language:English
- Summary in:English
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- SwePubSwePub
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Notes
- Validerad; 2000; 20060929 (bajo)
- Silicalite-1 films grown on gold surfaces seeded with colloidal crystals with a size of 60, 165 and 320 nm were investigated by reflection–absorption infrared spectroscopy, scanning electron microscopy and X-ray diffraction in order to follow up the formation of nano-scale defects and to determine the optimal synthesis conditions for preparation of silicalite-1 films with a low concentration of defects. Using 60-nm-sized colloidal crystals, the seeding method was capable of producing silicalite-1 films with low concentrations of defects and with thicknesses ranging from 100 to 300 nm, which are predominantly oriented with the a-axis perpendicular to the surface. Hydrothermal treatment times of the 60-nm-seeded surfaces longer than 36 h as well as the seeding with 165 or 320 nm colloidal crystals substantially enhanced the formation of defects in the films.
Subject headings and genre
- TEKNIK OCH TEKNOLOGIER Kemiteknik Kemiska processer hsv//swe
- ENGINEERING AND TECHNOLOGY Chemical Engineering Chemical Process Engineering hsv//eng
- NATURVETENSKAP Kemi Fysikalisk kemi hsv//swe
- NATURAL SCIENCES Chemical Sciences Physical Chemistry hsv//eng
- Chemical Technology
- Kemisk teknologi
- Physical Chemistry
- Fysikalisk kemi
Added entries (persons, corporate bodies, meetings, titles ...)
- Mihailova, BorianaCentral Laboratory of Mineralogy and Crystallography, Bulgarian Academy of Sciences, Sofia, Bulgaria (author)
- Hedlund, JonasLuleå tekniska universitet,Industriell miljö- och processteknik(Swepub:ltu)johe (author)
- Holmgren, AllanLuleå tekniska universitet(Swepub:ltu)alho (author)
- Sterte, JohanLuleå tekniska universitet(Swepub:ltu)jost (author)
- Luleå tekniska universitetCentral Laboratory of Mineralogy and Crystallography, Bulgarian Academy of Sciences, Sofia, Bulgaria (creator_code:org_t)
Related titles
- In:Microporous and Mesoporous Materials38:1, s. 51-601387-18111873-3093
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