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Spatial structure o...
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Blokhin, D.S.Institute of Physics, Kazan (Volga Region) Federal University, Kazan, Russia
(författare)
Spatial structure of the decapeptide Val-Ile-Lys-Lys-Ser-Thr-Ala-Leu-Leu-Gly in water and in a complex with sodium dodecyl sulfate micelles
- Artikel/kapitelEngelska2011
Förlag, utgivningsår, omfång ...
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2011-09-06
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Springer Science and Business Media LLC,2011
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printrdacarrier
Nummerbeteckningar
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LIBRIS-ID:oai:DiVA.org:ltu-3109
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https://urn.kb.se/resolve?urn=urn:nbn:se:ltu:diva-3109URI
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https://doi.org/10.1007/s00723-011-0257-xDOI
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Språk:engelska
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Sammanfattning på:engelska
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Klassifikation
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Ämneskategori:ref swepub-contenttype
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Ämneskategori:art swepub-publicationtype
Anmärkningar
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Validerad; 2011; 20110926 (ysko)
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We have studied the spatial structure of the decapeptide Val-Ile-Lys-Lys-Ser-Thr-Ala-Leu-Leu-Gly in aqueous solution and in a complex with sodium dodecyl sulfate (SDS) micelles by 1H nuclear magnetic resonance (NMR) spectroscopy and two-dimensional (2-D) NMR spectroscopy (total correlation spectroscopy and nuclear Overhauser effect spectroscopy (NOESY)). The approach used to determine the decapeptide spatial structure was based on analysis of the 1H–13C residual dipolar couplings in the molecules partially aligned in lyotropic liquid crystalline media. Analysis of the interproton distances obtained from the 2-D NOESY NMR spectrum was used to reveal the spatial structure of the decapeptide in a complex with SDS micelles. Complex formation was confirmed by analysis of 1H chemical shifts in the NMR spectrum of the decapeptide and analysis of the signs and values of NOEs in a solution with SDS micelles.
Ämnesord och genrebeteckningar
Biuppslag (personer, institutioner, konferenser, titlar ...)
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Efimov, S.V.Institute of Physics, Kazan (Volga Region) Federal University, Kazan, Russia
(författare)
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Klochkov, A.V.Institute of Physics, Kazan (Volga Region) Federal University, Kazan, Russia
(författare)
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Yulmetov, A.R.Institute of Physics, Kazan (Volga Region) Federal University, Kazan, Russia
(författare)
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Filippov, AndreiInstitute of Physics, Kazan (Volga Region) Federal University, Kazan, Russia(Swepub:ltu)andfil
(författare)
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Antzutkin, OlegLuleå tekniska universitet,Industriell miljö- och processteknik,Department of Physics, Warwick University, Coventry, UK(Swepub:ltu)olan
(författare)
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Aganov, A.G.Institute of Physics, Kazan (Volga Region) Federal University, Kazan, Russia
(författare)
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Klochkov, V.V.Institute of Physics, Kazan (Volga Region) Federal University, Kazan, Russia
(författare)
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Institute of Physics, Kazan (Volga Region) Federal University, Kazan, RussiaIndustriell miljö- och processteknik
(creator_code:org_t)
Sammanhörande titlar
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Ingår i:Applied Magnetic Resonance: Springer Science and Business Media LLC41:2-4, s. 267-2820937-93471613-7507
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