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- Mintova, S.Luleå tekniska universitet (author)
Growth of silicalite-1 films on gold substrates
- Article/chapterEnglish1997
Publisher, publication year, extent ...
- 1997
- printrdacarrier
Numbers
- LIBRIS-ID:oai:DiVA.org:ltu-3563
- https://urn.kb.se/resolve?urn=urn:nbn:se:ltu:diva-3563URI
- https://doi.org/10.1016/S0927-6513(97)00037-0DOI
Supplementary language notes
- Language:English
- Summary in:English
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- SwePubSwePub
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Notes
- Godkänd; 1997; 20080529 (cira)
- The crystallization of thin continuous silicalite-1 films on modified gold surfaces prepared at 100°C in clear precursor solutions has been studied by grazing angle X-ray diffractometry, infrared spectroscopy, dynamic light scattering, scanning electron microscopy, Kr adsorption and ellipsometry. The gold surfaces were pre-treated with a silane coupling agent, gamma-mercaptopropyltrimethoxysilane, and hydrolysed in an acidic solution, pH < 4, to create a modified negatively charged interface on which positively charged colloidal silicalite-1 seed crystals were adsorbed. The colloidal seed crystals are believed to be preferentially adsorbed with their {010} face parallel to the Au surface. Continued growth of the oriented seed crystals in a following hydrothermal step results in the formation of a continuous thin oriented crystalline film. The mechanism for the formation of silicalite-1 films on Au is discussed
Subject headings and genre
- TEKNIK OCH TEKNOLOGIER Kemiteknik Kemiska processer hsv//swe
- ENGINEERING AND TECHNOLOGY Chemical Engineering Chemical Process Engineering hsv//eng
- Chemical Technology
- Kemisk teknologi
Added entries (persons, corporate bodies, meetings, titles ...)
- Valtchev, V.Bulgarian Academy of Sciences (author)
- Engström, V.Luleå tekniska universitet (author)
- Shoeman, Brian J.Luleå tekniska universitet (author)
- Sterte, Johan (author)
- Luleå tekniska universitetBulgarian Academy of Sciences (creator_code:org_t)
Related titles
- In:Microporous Materials11:3-4, s. 149-1600927-65131873-3107
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