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Rhodium as efficien...
Rhodium as efficient additive for boosting acetone sensing by TiO2 nanocrystals : Beyond the classical view of noble metal additives
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- Epifani, Mauro (author)
- Istituto per la Microelettronica e i Microsistemi, IMM-CNR, Via Monteroni, Lecce, Italy
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- Kaciulis, Saulius (author)
- Istituto per lo Studio dei Materiali Nanostrutturati, ISMN–CNR, Roma, Italy
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- Mezzi, Alessio (author)
- Istituto per lo Studio dei Materiali Nanostrutturati, ISMN–CNR, Roma, Italy
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- Zhan, Ting (author)
- Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC BIST, Campus UAB, Bellaterra, Barcelona, Catalonia, Spain
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- Arbiol, Jordi (author)
- Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC BIST, Campus UAB, Barcelona, Catalonia, Spain. ICREA, Barcelona, Catalonia, Spain
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- Siciliano, Pietro (author)
- Istituto per la Microelettronica e i Microsistemi, IMM-CNR, Via Monteroni, Lecce, Italy
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- Landström, Anton (author)
- Luleå tekniska universitet,Materialvetenskap
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- Concina, Isabella (author)
- Luleå tekniska universitet,Materialvetenskap
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- Moumen, Abderrahim (author)
- Department of Information Engineering, Brescia University, Brescia, Italy
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- Comini, Elisabetta (author)
- Department of Information Engineering, Brescia University, Brescia, Italy
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- Xiangfeng, Chu (author)
- School of Chemistry and Chemical Engineering, Anhui University of Technology, Maanshan, Anhui, PR China
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(creator_code:org_t)
- Elsevier, 2020
- 2020
- English.
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In: Sensors and actuators. B, Chemical. - : Elsevier. - 0925-4005 .- 1873-3077. ; 319
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https://urn.kb.se/re...
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https://doi.org/10.1...
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Abstract
Subject headings
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- Anatase TiO2 nanocrystals were prepared by solvothermal synthesis and modified by in- situ generated Rh nanoparticles, with a starting nominal Rh:Ti atomic concentration of 0.01 and 0.05. After heat-treatment at 400 °C the TiO2 host was still in the anatase crystallographic phase, embedding Rh nanoparticles homogeneously distributed and whose surface had been oxidized to Rh2O3, as established by X-ray diffraction, Transmission Electron Microscopy and X-ray Photoelectron spectroscopy. Moreover, Rh seemed also homogeneously distributed in elemental form or as Rh2O3 nanoclusters. The acetone sensing properties of the resulting materials were enhanced by Rh addition, featuring a response increase of one order of magnitude at the best operating temperature of 300 °C. Moreover, Rh addition enlarged the detection range down to 10 ppm whereas pure TiO2 was not able of giving an appreciable response already at a concentration as high as 50 ppm. From the sensing data, the enhancement of the sensor response was attributed to the finely dispersed Rh species and not to the oxidized Rh nanocrystals.
Subject headings
- NATURVETENSKAP -- Fysik -- Annan fysik (hsv//swe)
- NATURAL SCIENCES -- Physical Sciences -- Other Physics Topics (hsv//eng)
Keyword
- TiO2 nanocrystals
- Acetone sensing
- Rhodium
- Noble metal additives
- Solvothermal synthesis
- Experimentell fysik
- Experimental Physics
Publication and Content Type
- ref (subject category)
- art (subject category)
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Epifani, Mauro
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Kaciulis, Sauliu ...
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Mezzi, Alessio
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Zhan, Ting
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Arbiol, Jordi
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Siciliano, Pietr ...
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show more...
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Landström, Anton
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Concina, Isabell ...
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Moumen, Abderrah ...
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Comini, Elisabet ...
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Xiangfeng, Chu
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- NATURAL SCIENCES
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NATURAL SCIENCES
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and Physical Science ...
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Sensors and actu ...
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Luleå University of Technology