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Diglycidylether of iso-eugenol : a suitable lignin-derived synthon for epoxy thermoset applications

Francois, Camille (author)
ICMUB Institute;Department of Electrochemistry;Molecular Materials and Devices;UMR-CNRS 6302;University of Bourgogne Franche-Comté
Pourchet, Sylvie (author)
ICMUB Institute;Department of Electrochemistry;Molecular Materials and Devices;UMR-CNRS 6302;University of Bourgogne Franche-Comté
Boni, Gilles (author)
ICMUB Institute;Department of Electrochemistry;Molecular Materials and Devices;UMR-CNRS 6302;University of Bourgogne Franche-Comté
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Fontaine, Stephane (author)
DRIVE Laboratory;Institut Supérieur de l'Automobile et des Transports;F-58027 Nevers;France
Gaillard, Yves (author)
FEMTO Institute;Applied Mechanics Department;UMR CNRS 6174;University of Franche-Comté;F-25000 Besançon
Placet, Vincent (author)
FEMTO Institute;Applied Mechanics Department;UMR CNRS 6174;University of Franche-Comté;F-25000 Besançon
Galkin, Maxim V. (author)
Stockholms universitet,Institutionen för organisk kemi,Department of Organic Chemistry;Arrhenius Laboratory;Stockholm University;S-106 91 Stockholm;Sweden
Orebom, Alexander (author)
Stockholms universitet,Institutionen för organisk kemi,Department of Organic Chemistry;Arrhenius Laboratory;Stockholm University;S-106 91 Stockholm;Sweden
Samec, Joseph (author)
Stockholms universitet,Institutionen för organisk kemi,Department of Organic Chemistry;Arrhenius Laboratory;Stockholm University;S-106 91 Stockholm;Sweden
Plasseraud, Laurent (author)
ICMUB Institute;Department of Electrochemistry;Molecular Materials and Devices;UMR-CNRS 6302;University of Bourgogne Franche-Comté
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 (creator_code:org_t)
2016
2016
English.
In: RSC Advances. - : Royal Society of Chemistry. - 2046-2069. ; 6:73, s. 68732-68738
Related links:
https://urn.kb.se/re...
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https://doi.org/10.1...
https://urn.kb.se/re...
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  • Journal article (peer-reviewed)
Abstract Subject headings
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  • A novel lignin-based synthon, diglycidylether of iso-eugenol (DGE-isoEu) is used as a prepolymer for the preparation of thermosetting resins. DGE-isoEu is synthesized in a two-step procedure with a satisfactory yield from bio-based iso-eugenol (isoEu, 2-methoxy-4-(1-propenyl)phenol) catalytically fragmented from lignin in an organosolv process. DGE-isoEu was fully characterized by NMR, MS and FTIR. Curing of the DGE-isoEu monomer has then been investigated in the presence of several carboxylic acid derivatives hardeners. The thermal and mechanical properties of each material were recorded showing, in particular, a high T-g and instantaneous modulus values in the range of 78-120 degrees C and 4.6-5.5 GPa, respectively. The lignin derived new materials give very attractive thermo-mechanical properties comparable to that of common BPA-containing epoxy resins.

Subject headings

NATURVETENSKAP  -- Kemi (hsv//swe)
NATURAL SCIENCES  -- Chemical Sciences (hsv//eng)
NATURVETENSKAP  -- Kemi -- Polymerkemi (hsv//swe)
NATURAL SCIENCES  -- Chemical Sciences -- Polymer Chemistry (hsv//eng)

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